 |
| PAPER | Synthesis 2007: 363-366
DOI: 10.1055/s-2007-965873 |
© Georg Thieme Verlag Stuttgart · New York
|
 |
A Novel and Efficient Synthesis of Unsymmetrical Disulfides
|
| Sylwia Antoniow, Dariusz Witt* |
Department of Organic Chemistry, Chemical Faculty, Gdansk University of Technology, Narutowicza 11/12, 80-952 Gdansk, Poland
Fax: +48(58)3472694; e-Mail: dwitt@chem.pg.gda.pl;
|
|
Received
17 October 2006 |
Abstract
Unsymmetrical disulfides have been prepared from the corresponding thiols and bis-(5,5-dimethyl-2-thiono-1,3,2-dioxaphosphorinanyl)disulfide under mild conditions with good to excellent yields. The method can be applied to thiols bearing neutral, aromatic, basic or acidic functionalities with variable length of carbon chain. Key words
unsymmetrical disulfides - alkanethiols - l-cysteine - thiophenol
| |
