Subscribe to RSS
Please copy the URL and add it into your RSS Feed Reader.
https://www.thieme-connect.de/rss/thieme/en/10.1055-s-00000084.xml
Synthesis 2015; 47(17): 2677-2679
DOI: 10.1055/s-0034-1380217
DOI: 10.1055/s-0034-1380217
paper
Synthesis of a Cyclic 3-Methylsulfonyl Enol Ether
Further Information
Publication History
Received: 25 March 2015
Accepted after revision: 24 April 2015
Publication Date:
17 June 2015 (online)
Dedicated to Professor Hans-Ulrich Reissig on the occasion of his 66th birthday
Abstract
Electrophilic introduction of a methylmercapto group into dihydropyran gives 3-methylmercaptodihydropyran, which is readily oxidized to 3-methylsulfonyldihydropyran.
Supporting Information
- Supporting information for this article is available online at http://dx.doi.org/10.1055/s-0034-1380217.
- Supporting Information
-
References
- 1 Present address: Institut Für Chemie und Biochemie, Freie Universität Berlin, Takustr. 3, 14195 Berlin, Germany.
- 2 Skuballa W, Raduechel B, Vorbrueggen H. Tetrahedron Lett. 1988; 29: 4285
- 3 Meerwein H, Zenner KF, Gipp R. Liebigs Ann. Chem. 1965; 688: 67
- 4 Baldwin MJ, Brown RK. Can. J. Chem. 1967; 45: 1195
- 5 Brintzinger H, Pfannstiehl K, Koddebusch H. Chem. Ber. 1950; 83: 87
- 6 Freeman F, Angeletakis CN. J. Am. Chem. Soc. 1983; 105: 4039
- 7 de Lucchi O, Miotti U, Modena G. Org. React. 1991; 40: 157
- 8 Opitz O, Rieth KG, Walz G. Tetrahedron Lett. 1966; 5269
- 9 Opitz O, Bluecher D. Tetrahedron Lett. 1966; 5263
- 10 Beagley B, James M, Pritchard RG, Raynor CM, Smith C, Stoodley RJ. J. Chem. Soc., Perkin Trans. 1 1992; 2371
- 11 Skuballa W, Vorbrueggen H. Angew. Chem., Int. Ed. Engl. 1981; 20: 1046
- 12 Skuballa W, Schillinger E, Stuerzebecher CSt, Vorbrueggen H. J. Med. Chem. 1986; 29: 313