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Synthesis 1990; 1990(2): 140-141
DOI: 10.1055/s-1990-26813
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Studies on Organophosphorus Compounds XL. An One-Pot Procedure for the Mono-O-Alkylation of Phosphonic Acid: A Facile Synthesis of Alkyl Hydrogen p-Substituted Phenylphosphonates

Chengye Yuan* , Hanzhen Feng
  • *Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Linglin Lu, Shanghai 200032, People's Republic of China
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Publication Date:
17 September 2002 (online)

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A one-pot procedure is described for the synthesis of hexyl hydrogen p-substituted phenylphosphonates 4 in moderate yield based on the mono-O-alkylation of bis(tetramethylammonium) salts of dibasic phosphonic acids 3.

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