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Synthesis 1995; 1995(11): 1411-1414
DOI: 10.1055/s-1995-4124
DOI: 10.1055/s-1995-4124
paper
© Georg Thieme Verlag, Rüdigerstr. 14, 70469 Stuttgart, Germany. All rights reserved.
This journal, including all individual contributions and illustrations published therein,
is legally protected by copyright for the duration of the copyright period. Any use,
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without the publisher's consent, is illegal and liable to criminal prosecution. This
applies in particular to photostat reproduction, copying, cyclostyling, mimeographing
or duplication of any kind, translating, preparation of microfilms, and electronic
data processing and storage.Synthesis and Reactivity of Cyanotetrathiafulvalenes: X-ray Crystal Structure of 4-Cyanotetrathiafulvalene
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Publikationsverlauf
Publikationsdatum:
31. Dezember 2000 (online)
The synthesis of cyanotetrathiafulvalenes is described using tetrathiafulvaleneyllithium intermediates to afford the desired products both conveniently and in good yield. 4-Cyanotetrathiafulvalene (2) has been used as a building block to synthesize new derivatives with potentially interesting solid-state structures. The X-ray crystal structure of 2 reveals that neither hydrogen-bonding interactions nor cyano-cyano dipole interactions are implicated in the overall packing.
tetrathiafulvalene - organolithium - cyano- - X-ray crystal structure