Synfacts

Issue 03 · March 2014

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Iridium-Catalyzed Route to Enantioenriched Tertiary Alcohols and Thioethers

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Synthesis of 3,5-Diphenyl-1H-pyrazoles by Mechanochemical Ball Milling

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1,3-Cycloaddition Route to 1,2,3-Triazoles Catalyzed by Copper

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Variation of the Pictet–Spengler Synthesis of Tetrahydrocarbolines

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Gold-Catalyzed Synthesis of Tetrazoles from Alkynes

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Synthesis of 3H-Pyrrolo[2,3-c]quinolin-4(5H)-ones Using ToSMIC Derivatives

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Substituted α-Amino-β-Lactams via Sequential C–H Arylation/C–H Amidation

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Diastereoselective Synthesis of Dibenzo[c,e]azepines

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Stable Boranes with a Thiophene Linker

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Triarylmethanes Made to Order

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An ‘Ene’-credible Cascade

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A New SF₄-Building Block

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A Radical Protection

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Terazulene: A Head-to-Tail Oligomer of Azulene

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A Cascade Cycloaddition Approach to Perylenes

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Can You exo-dig It? Radical-Cascade Synthesis of Polycyclic Frameworks

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0264
Nothing Azaborine About It: One Step to Functionalized Azaborines

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0265
Site-Selective Polycyclic Thiophenes From Alkynes via C–H Activation

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Gigantic Cyclic Poly(carbosiloxane)s

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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trans-Selective Hydroboration of Internal Alkynes Catalyzed by Ruthenium FREE ACCESS

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Chiral Pyridazines via Copper-Catalyzed Asymmetric Hetero-Diels–Alder Reaction

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Tandem Enantioselective Zinc-Promoted Reaction FREE ACCESS

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Allylsilanes via Tandem C–H Insertion–Decarboxylative Rearrangement

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Asymmetric Sonogashira Coupling Catalyzed by a Palladium Complex

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Synthesis of Tropanes through Asymmetric [3+2] Cycloaddition

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β-Tetralones and Benzobicyclo-[2.2.2]octanones via C–C Bond Cleavage

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Enantioselective Synthesis of Quaternary Succinimides Catalyzed by Palladium(II)

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Enantioselective Cyclative Acetoxylation Catalyzed by Palladium

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Palladium-Catalyzed Asymmetric Allylic Alkylation of Ketones

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Palladium-Catalyzed Enantioselective Desymmetrization of Bicyclic Hydrazines

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Magnesium-Catalyzed Asymmetric 1,3-Dipolar Cycloaddition

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Domino Rhodium(III)-Catalyzed Hydroarylation–Lactonization

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Asymmetric Hydrogenolysis of N-Sulfonyl Amino Alcohols Catalyzed by Palladium

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Isochromenes Synthesis by Cyclization and Asymmetric Transfer Hydrogenation

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0282
Intramolecular Allylic Alkylation by Iridium Catalysis

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Trisubstituted Monofluoroalkenes via Rh-Catalyzed Allylic C–F Bond Activation

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Asymmetric Monoborylation of Alkenylsilanes by Copper Catalysis

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Asymmetric Arylation of α-Keto Esters by Rhodium Catalysis

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Asymmetric O-Arylation by Palladium Catalysis

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0287
Thiourea-Catalyzed Enantioselective Monofluoromethylation of Aldehydes

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Hydroalkynylation of Norboradienes by Rhodium Catalysis

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Asymmetric Addition of Acetonitrile to N-Thiophosphinoylimines by Copper Catalysis

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0290
Chiral Amino Alcohols via a Palladium-Catalyzed Asymmetric Allylic Amination

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C–H Functionalization of Pyrroles Catalyzed by Palladium(II) and Phosphate

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0292
Highly Stereoselective Manganese-Catalyzed Epoxidation of Styrenes and Δ₅-Steroids

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0293
Enantioenriched Cyclic Compounds by Allylic Alkylation and Metathesis

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0294
Ruthenium-Catalyzed Asymmetric Hydrogenation of α,β-Unsaturated Ketones

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0295
Transfer of Chirality for Synthesis of Bicyclo[5.3.0]decatrienes

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0296
Direct C–O Arylation Catalyzed by Nickel

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Metal-Mediated Synthesis
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Palladium-Catalyzed Linear-Selective Negishi Cross-Coupling of Allylzinc Halides FREE ACCESS

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Tandem Asymmetric Conjugate Addition –Enolate Trapping with Cyclic Enones

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0299
α-Trifluoromethylated Alkylboron Compounds: Synthesis and Applications

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0300
Titanium Ethoxide Mediated Synthesis of N-Acyl-N,O-acetals

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0301
Synthesis of Acridine Derivatives by ZnCl₂-Promoted Intramolecular Cyclization

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0302
Methylation and meta Arylation of 3-Phenylpropanoic Acid Derivatives

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0303
AgF-Mediated Homocoupling Reaction of β,β-Difluorostyrene Derivatives

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0304
Arylthio–Metal Exchange Alkylation of α-Arylthioalkanenitriles

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0305
Zinc-Initiated Addition and Cascade Reactions of Alkynes

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0306
Zinc-Catalyzed Borylation of Aryl Halides and Borylzincation of Benzynes

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0307
Coupling of Arylzinc Reagents with Aryl and Alkenyl Halides

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0308
Azomethine Imines by Intramolecular Cycloaddition Reaction

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0309
Aldol Reaction with Super Silyl Haloacetate

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0310
Preparation of a Trifluoromethyl Copper Reagent from Trifluoromethyl Ketones

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0311
Chelation-Controlled Addition of Dialkylzinc Reagents to Aldehydes

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Organo- and Biocatalysis
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Organocatalysis with Carbocations

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0314
Oxidative Cross-Coupling in Asymmetric Aminocatalysis

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0315
Arylation of Benzylic Ethers Using a Thiol Catalyst

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0316
Enantioselective trans-Dihydroxylation of Styrenes via Cascade Biocatalysis

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0317
Chiral DMAP Catalyzed Desymmetrization of meso Primary Diols

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0318
Organocatalytic Enantioselective Cascade Aza-Michael–Michael Addition

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0319
A General Aminocatalytic Protocol for the Synthesis of Aldimines

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Polymer-Supported Synthesis
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A Silicon Nanowire Array Stabilized Palladium-Nanoparticle Catalyst FREE ACCESS

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α-Aminoxylation of Ketones with TEMPO Using Cu/SiO₂-Fe

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Asymmetric Oxidation of Sulfides Using a Chiral Copper MOF

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Suzuki–Miyaura Coupling with SiliaCat DPP-Pd

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0325
Oxidative Amidation of Primary Alcohols and Amines Using Au/HAP

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0326
Synthesis of Benzoquinazolinones Using a Brønsted Acidic Ionic Liquid

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0327
Pd/Al₂O₃-Catalyzed Hydrogenation Using H₂ Micro- and Nanobubbles

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Synthesis of Imidazole, Thiazole, and Oxazole Derivatives with Nano-CeO₂

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Asymmetric 1,3-Dipolar Cycloaddition with Imidazolidinone–Fe₃O₄ NPs

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Solvent-Free Ring Opening of Epoxides Using a Bismuth Complex

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The Crystal Plane Effect in the Au/CeO₂-Catalyzed Alcohol Oxidation

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Disilylation of Terminal Alkynes with Au/TiO₂

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