Synfacts
Issue 03 · March 2014
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SYNFORM
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Synthesis of Natural Products and Potential Drugs
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Synthesis of (–)-Oseltamivir
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Total Synthesis of (–)-Angiolam A
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Synthesis of (–)-Calyciphylline N
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Total Synthesis of (±)-Yezo’otogirin C
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Synthesis of (–)-Ophiodilactones A and B
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Synthesis of a Bile Acid Transporter Inhibitor
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Synthesis of the β-Lactamase Inhibitor MK-7655
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Syntheses of Leuconolam–Leuconoxine–Mersicarpine Group Indole Alkaloids
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Total Synthesis of Sandresolide B and Amphilectolide
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0234
Synthesis of a TRPV1 Antagonist
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Synthesis of (–)-Lasonolide A
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0236
Synthesis of an HCV Replicase Inhibitor
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0237
Synthesis of the Four Stereoisomers of Mefloquine
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Synthesis of Heterocycles
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0239
Intramolecular Ene Synthesis of 3-Pyrrolines
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0240
Spiroaminals and Spiroketals via Au/La and Au/Y Relay Catalysis
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0241
Synthesis of Pyrazoles via Nickel-Catalyzed Cyclotrimerization
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0242
Synthesis of Oxazolones by a β-Selective Oxidative Heck Coupling
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0243
Iridium-Catalyzed Route to Enantioenriched Tertiary Alcohols and Thioethers
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0244
Synthesis of Dihydroimidazoles and Quinazolinones via C–H Amination
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0245
Multicomponent Synthesis of Aza-Dibenzazepines Catalyzed by Rh/Pd
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0246
Synthesis of 3,5-Diphenyl-1
H
-pyrazoles by Mechanochemical Ball Milling
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0247
Synthesis of 1,3-Oxazin-6-ones from Enamides Catalyzed by Palladium
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0248
1,3-Cycloaddition Route to 1,2,3-Triazoles Catalyzed by Copper
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0249
Variation of the Pictet–Spengler Synthesis of Tetrahydrocarbolines
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0250
Gold-Catalyzed Synthesis of Tetrazoles from Alkynes
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0251
Synthesis of 3
H
-Pyrrolo[2,3-
c
]quinolin-4(5
H
)-ones Using ToSMIC Derivatives
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0252
Substituted α-Amino-β-Lactams via Sequential C–H Arylation/C–H Amidation
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0253
Diastereoselective Synthesis of Dibenzo[
c
,
e
]azepines
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Synthesis of Materials and Unnatural Products
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0255
‘Chalc’ing up a New Sumanene
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0256
Stable Boranes with a Thiophene Linker
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0257
Triarylmethanes Made to Order
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0258
An ‘Ene’-credible Cascade
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0259
A New SF
4
-Building Block
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0260
A Radical Protection
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0261
Terazulene: A Head-to-Tail Oligomer of Azulene
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0262
A Cascade Cycloaddition Approach to Perylenes
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0263
Can You
exo
-dig It? Radical-Cascade Synthesis of Polycyclic Frameworks
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0264
Nothing Azaborine About It: One Step to Functionalized Azaborines
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0265
Site-Selective Polycyclic Thiophenes From Alkynes via C–H Activation
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0266
Gigantic Cyclic Poly(carbosiloxane)s
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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z267
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0267
trans
-Selective Hydroboration of Internal Alkynes Catalyzed by Ruthenium
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0268
Chiral Pyridazines via Copper-Catalyzed Asymmetric Hetero-Diels–Alder Reaction
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0269
Tandem Enantioselective Zinc-Promoted Reaction
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0270
Allylsilanes via Tandem C–H Insertion–Decarboxylative Rearrangement
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0271
Asymmetric Sonogashira Coupling Catalyzed by a Palladium Complex
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0272
Synthesis of Tropanes through Asymmetric [3+2] Cycloaddition
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0273
β-Tetralones and Benzobicyclo-[2.2.2]octanones via C–C Bond Cleavage
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0274
Enantioselective Synthesis of Quaternary Succinimides Catalyzed by Palladium(II)
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0275
Enantioselective Cyclative Acetoxylation Catalyzed by Palladium
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0276
Palladium-Catalyzed Asymmetric Allylic Alkylation of Ketones
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0277
Palladium-Catalyzed Enantioselective Desymmetrization of Bicyclic Hydrazines
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0278
Magnesium-Catalyzed Asymmetric 1,3-Dipolar Cycloaddition
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0279
Domino Rhodium(III)-Catalyzed Hydroarylation–Lactonization
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0280
Asymmetric Hydrogenolysis of
N
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0281
Isochromenes Synthesis by Cyclization and Asymmetric Transfer Hydrogenation
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0282
Intramolecular Allylic Alkylation by Iridium Catalysis
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0283
Trisubstituted Monofluoroalkenes via Rh-Catalyzed Allylic C–F Bond Activation
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0284
Asymmetric Monoborylation of Alkenylsilanes by Copper Catalysis
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0285
Asymmetric Arylation of α-Keto Esters by Rhodium Catalysis
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0286
Asymmetric O-Arylation by Palladium Catalysis
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0287
Thiourea-Catalyzed Enantioselective Monofluoromethylation of Aldehydes
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0288
Hydroalkynylation of Norboradienes by Rhodium Catalysis
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0289
Asymmetric Addition of Acetonitrile to
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-Thiophosphinoylimines by Copper Catalysis
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0290
Chiral Amino Alcohols via a Palladium-Catalyzed Asymmetric Allylic Amination
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0291
C–H Functionalization of Pyrroles Catalyzed by Palladium(II) and Phosphate
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0292
Highly Stereoselective Manganese-Catalyzed Epoxidation of Styrenes and Δ
5
-Steroids
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0293
Enantioenriched Cyclic Compounds by Allylic Alkylation and Metathesis
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0294
Ruthenium-Catalyzed Asymmetric Hydrogenation of α,β-Unsaturated Ketones
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0295
Transfer of Chirality for Synthesis of Bicyclo[5.3.0]decatrienes
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0296
Direct C–O Arylation Catalyzed by Nickel
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Metal-Mediated Synthesis
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0297
Palladium-Catalyzed Linear-Selective Negishi Cross-Coupling of Allylzinc Halides
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0298
Tandem Asymmetric Conjugate Addition –Enolate Trapping with Cyclic Enones
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0299
α-Trifluoromethylated Alkylboron Compounds: Synthesis and Applications
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0300
Titanium Ethoxide Mediated Synthesis of
N
-Acyl-
N
,
O
-acetals
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0301
Synthesis of Acridine Derivatives by ZnCl
2
-Promoted Intramolecular Cyclization
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0302
Methylation and
meta
Arylation of 3-Phenylpropanoic Acid Derivatives
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0303
AgF-Mediated Homocoupling Reaction of β,β-Difluorostyrene Derivatives
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0304
Arylthio–Metal Exchange Alkylation of α-Arylthioalkanenitriles
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0305
Zinc-Initiated Addition and Cascade Reactions of Alkynes
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0306
Zinc-Catalyzed Borylation of Aryl Halides and Borylzincation of Benzynes
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0307
Coupling of Arylzinc Reagents with Aryl and Alkenyl Halides
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0308
Azomethine Imines by Intramolecular Cycloaddition Reaction
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0309
Aldol Reaction with Super Silyl Haloacetate
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0310
Preparation of a Trifluoromethyl Copper Reagent from Trifluoromethyl Ketones
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0311
Chelation-Controlled Addition of Dialkylzinc Reagents to Aldehydes
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Organo- and Biocatalysis
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0313
Organocatalysis with Carbocations
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0314
Oxidative Cross-Coupling in Asymmetric Aminocatalysis
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0315
Arylation of Benzylic Ethers Using a Thiol Catalyst
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0316
Enantioselective trans-Dihydroxylation of Styrenes via Cascade Biocatalysis
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0317
Chiral DMAP Catalyzed Desymmetrization of
meso
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0318
Organocatalytic Enantioselective Cascade Aza-Michael–Michael Addition
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0319
A General Aminocatalytic Protocol for the Synthesis of Aldimines
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Polymer-Supported Synthesis
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0321
A Silicon Nanowire Array Stabilized Palladium-Nanoparticle Catalyst
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0322
α-Aminoxylation of Ketones with TEMPO Using Cu/SiO
2
-Fe
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0323
Asymmetric Oxidation of Sulfides Using a Chiral Copper MOF
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0324
Suzuki–Miyaura Coupling with Silia
Cat
DPP-Pd
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0325
Oxidative Amidation of Primary Alcohols and Amines Using Au/HAP
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0326
Synthesis of Benzoquinazolinones Using a Brønsted Acidic Ionic Liquid
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0327
Pd/Al
2
O
3
-Catalyzed Hydrogenation Using H
2
Micro- and Nanobubbles
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0328
Synthesis of Imidazole, Thiazole, and Oxazole Derivatives with Nano-CeO
2
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0329
Asymmetric 1,3-Dipolar Cycloaddition with Imidazolidinone–Fe
3
O
4
NPs
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0330
Solvent-Free Ring Opening of Epoxides Using a Bismuth Complex
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0331
The Crystal Plane Effect in the Au/CeO
2
-Catalyzed Alcohol Oxidation
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0332
Disilylation of Terminal Alkynes with Au/TiO
2
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