Synthesis

Issue 21 · November 2020

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Synform
A153
Zanda, Matteo:
SYNFORM ISSUE 2020/11
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review
3095
Loska, Rafał; Mąkosza, Mieczysław:
Introduction of Carbon Substituents into Nitroarenes via Nucleophilic Substitution of Hydrogen: New Developments

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short review
3111
Mateus-Ruiz, Jeferson B.; Cordero-Vargas, Alejandro:
Visible-Light-Mediated Photoredox Reactions in the Total Synthesis of Natural Products

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3129
Moberg, Christina:
Silylboranes as Powerful Tools in Organic Synthesis: Stereo- and Regioselective Reactions with 1,n-Enynes

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feature
3140
Rehan, Mohammad; Flegel, Jana; Heitkamp, Franziska; Pergomet, Jorgelina L.; Otte, Felix; Strohmann, Carsten; Kumar, Kamal:
Asymmetric Synthesis of 3,3′-Piperidinoyl Spirooxindoles and Discovery of Stereospecific Cycloadducts as Novel Hedgehog Pathway Modulators

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psp
3153
Kadari, Lingaswamy; Roisnel, Thierry; Erb, William; Krishna, Palakodety Radha; Mongin, Florence:
Remote Deprotometalation-Iodolysis of N,N-Diisopropyl-2-trimethylsilylferrocenecarboxamide: A New Route Toward 1,1′-Disubstituted Ferrocenes
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special topic
Recent Advances in Amide Bond Formation
3162
Shiri, Morteza; Farajinia-Lehi, Noushin; Salehi, Parvin; Tanbakouchian, Zahra:
Transition Metal and Inner Transition Metal Catalyzed Amide Derivatives Formation through Isocyanide Chemistry

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PDF (1583 kb)
3189
Manne, Srinivasa Rao; de la Torre, Beatriz G.; El-Faham, Ayman; Albericio, Fernando:
OxymaPure Coupling Reagents: Beyond Solid-Phase Peptide Synthesis

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3211
Zhao, Baoli; Liu, Yunyun:
Step-Economical C–H Activation Reactions Directed by In Situ Amidation

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PDF (451 kb)
3219
Spiliopoulou, Nikoleta; Constantinou, Constantinos T.; Triandafillidi, Ierasia; Kokotos, Christoforos G.:
Synthetic Approaches to Acyl Hydrazides and Their Use as Synthons in Organic Synthesis

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PDF (491 kb)
3231
Kolympadi Marković, Maria; Marković, Dean; Laclef, Sylvain:
Amide Synthesis by Transamidation of Primary Carboxamides

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PDF (697 kb)
3243
Shiri, Morteza; Gholami-Koupaei, Zahra; Bandehali-Naeini, Farzaneh; Tonekaboni, Maryam-Sadat; Soheil-Moghaddam, Saeedeh; Ebrahimi, Delaram; Karami, Sima; Notash, Behrouz:
Highly Selective Synthesis of α-Hydroxy, α-Oxy, and α-Oxo Amides by a Post-Passerini Condensation Transformation

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PDF (345 kb)

Supplementary Material

Supporting Information (PDF)

CIF File (OTHER)
3253
Movahed, Farzaneh Soleymani; Sawant, Dinesh N.; Bagal, Dattatraya B.; Saito, Susumu:
Tris(o-phenylenedioxy)cyclotriphosphazene as a Promoter for the Formation of Amide Bonds Between Aromatic Acids and Amines

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3263
Smolobochkin, Andrey V.; Gazizov, Almir S.; Otegen, Nazerke K.; Voronina, Julia K.; Strelnik, Anna G.; Samigullina, Aida I.; Burilov, Alexander R.; Pudovik, Michail A.:
Nucleophilic Cyclization/Electrophilic Substitution of (2,2-Dialkoxyethyl)ureas: Highly Regioselective Access to Novel 4-(Het)arylimidazolidinones and Benzo[d][1,3]diazepinones

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3272
Verma, Saumya; Kumar, Puneet; Khatana, Anil K.; Chandra, Dinesh; Yadav, Ajay K.; Tiwari, Bhoopendra; Jat, Jawahar L.:
Zinc(II)-Catalyzed Synthesis of Secondary Amides from Ketones via Beckmann Rearrangement Using Hydroxylamine-O-sulfonic Acid in Aqueous Media
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Supplementary Material

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3277
Kabes, Connor Q.; Gunn, Jack H.; Selbst, Maximilian A.; Lucas, Reagan F.; Gladysz, John A.:
Syntheses of Enantiopure 1,2-Ethylenediamines with Tethered Secondary Amines of the Formula H₂NCH₂CH[(CH₂)_nNHMe]NH₂ (n = 1–4) from α-Amino Acids: New Agents for Asymmetric Catalysis

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Supplementary Material

Supporting Information (PDF)
Recent Advances in Amide Bond Formation
3286
Zhang, Rui; Zhang, Jun-Chao; Zhang, Wei-Yi; He, Yu-Qing; Cheng, Hua; Chen, Cheng; Gu, Yu-Cheng:
A Practical Approach for the Transamidation of N,N-Dimethyl Amides with Primary Amines Promoted by Sodium tert-Butoxide under Solvent-Free Conditions

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Synthesis

Linked PDF of Table of Contents

SYNFORM ISSUE 2020/11

Introduction of Carbon Substituents into Nitroarenes via Nucleophilic Substitution of Hydrogen: New Developments

Visible-Light-Mediated Photoredox Reactions in the Total Synthesis of Natural Products

Silylboranes as Powerful Tools in Organic Synthesis: Stereo- and Regioselective Reactions with 1,n-Enynes

Asymmetric Synthesis of 3,3′-Piperidinoyl Spirooxindoles and Discovery of Stereospecific Cycloadducts as Novel Hedgehog Pathway Modulators

Remote Deprotometalation-Iodolysis of N,N-Diisopropyl-2-trimethylsilylferrocenecarboxamide: A New Route Toward 1,1′-Disubstituted Ferrocenes

Transition Metal and Inner Transition Metal Catalyzed Amide Derivatives Formation through Isocyanide Chemistry

OxymaPure Coupling Reagents: Beyond Solid-Phase Peptide Synthesis

Step-Economical C–H Activation Reactions Directed by In Situ Amidation

Synthetic Approaches to Acyl Hydrazides and Their Use as Synthons in Organic Synthesis

Amide Synthesis by Transamidation of Primary Carboxamides

Highly Selective Synthesis of α-Hydroxy, α-Oxy, and α-Oxo Amides by a Post-Passerini Condensation Transformation

Tris(o-phenylenedioxy)cyclotriphosphazene as a Promoter for the Formation of Amide Bonds Between Aromatic Acids and Amines

Nucleophilic Cyclization/Electrophilic Substitution of (2,2-Dialkoxyethyl)ureas: Highly Regioselective Access to Novel 4-(Het)arylimidazolidinones and Benzo[d][1,3]diazepinones

Zinc(II)-Catalyzed Synthesis of Secondary Amides from Ketones via Beckmann Rearrangement Using Hydroxylamine-O-sulfonic Acid in Aqueous Media

Syntheses of Enantiopure 1,2-Ethylenediamines with Tethered Secondary Amines of the Formula H₂NCH₂CH[(CH₂)_nNHMe]NH₂ (n = 1–4) from α-Amino Acids: New Agents for Asymmetric Catalysis

A Practical Approach for the Transamidation of N,N-Dimethyl Amides with Primary Amines Promoted by Sodium tert-Butoxide under Solvent-Free Conditions