Synfacts

Ausgabe 10 · Oktober 2021

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Ausgabe
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A157
SYNFORM ISSUE 2021/10 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
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1071
Synthesis of Sotorasib FREIER ZUGRIFF

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1072
Synthesis of (+)-Davisinol

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1073
Synthesis of (–)-Talatisamine and (–)-Liljestrandisine FREIER ZUGRIFF

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1074
Synthesis of Anti-Malarial MMV390048

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1075
Total Synthesis (+)-Pepluanol A

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1076
Synthesis of Pemigatinib

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1077
Total Synthesis of (+)-Ambiguine G

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1078
Synthesis of (+)-Mannolide C

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1079
Total Synthesis of (+)-Prostratin

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1080
Synthesis of (±)-Pentacycloanammoxic Acid Methyl Ester FREIER ZUGRIFF

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Synthesis of Heterocycles
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1081
Synthesis of Silazacycles from the Elusive 3-Silaazetidine

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1082
Synthesis of 2,1-Benzisoxazoles via Decyanative Cyclization

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1083
Direct Preparation of N-Substituted Pyrazoles from Primary Aliphatic or Aromatic Amines

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1084
Dithioesters as Thiocarbonyl Precursors in Thorpe–Ziegler-Type Cyclization

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1085
Regiospecific Three-Component Synthesis of 2-Aminothiophenes

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1086
Rh-Catalyzed Synthesis of Thienoacenes from Thiophenes

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1087
Direct C–H Functionalization of N-Heteroaromatics with Cyclic Ethers

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Synthesis of Materials and Unnatural Products
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1089
Dendritic Donor for Good π-Stacking

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1090
A Tetrathia[8]circulene–Azaborine Fusion

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1091
Living Helix

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1092
Synthesis of Stereogenic Fluoroborate as a Fluorophore with an Increased Stokes Shift

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1093
Nitrogen Incorporation in a Nanographene through Direct Oxidative Cyclization

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1094
A Benzene- Bridged Bismacrocycle

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1095
Metal-Free Oxidative Decarboxylative Coupling

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1096
Easy Access to a Nitrogen- Doped Aromatic Belt with a [6]Cycloparaphenylene Skeleton

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1097
Efficient Synthesis of a Novel Benzo-Incorporated Smallest Expanded Calix[4]pyrrole

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1098
A New Meta in meta-Halophenol Synthesis

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1099
Thiolated Pillar[5]arene and Its Supramolecular-Complexation-Accelerated Dimerization

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1100
Calix[3]-Type Macrocycles: The Missing Family Member

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Metals in Synthesis
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1101
Denitrogenative Ring Shrinkage of Heterocycles FREIER ZUGRIFF

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1102
Synthesis of Chiral Cyclopropane-1-Carboxylates

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1103
One-Pot α,α′-Difunctionalization of Cyclic Amines

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1104
Trifluoroacetylation of Styrenes

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1105
Copper-Catalyzed Arene Ring Cleavage

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1106
Enantioselective Rhodium-Catalyzed Synthesis of Fluorinated Allenes

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1107
Iron-Catalyzed Cross-Coupling of Propargyl Ethers with Grignard Reagents

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1108
Stereoselective Synthesis of (E)-δ-Vinyl-Homoallylic Alcohols from α-Vinyl Allylboronate

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1109
Preparation of Chiral Allylic Alcohols by Asymmetric Reduction of Substituted Cycloalkenones

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1110
Vinylation of Aldehydes through Twofold C–H Functionalization

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1111
Rhodium-Catalyzed Alkynylcyclopropanation of Alkenes Using Alkynylcycloheptatrienes

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1112
Iridium-Catalyzed Alkenylation of Enamides

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1113
Preparation of (Het)arylgermanes

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1114
Palladium and Ammonium Halide Catalysis for Enantioselective [4+2] Annulations

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1115
Enantio- and Diastereoselective Synthesis of Trifluoromethyl-Cyclopropylboronates

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1116
Directed Nickel-Catalyzed Hydrofunctionalization of Alkenes

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1117
Synthesis of gem-Difluorohomoallylic Alcohols by Reductive Defluorinative Coupling

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1118
Palladium-Catalyzed Benzylic C(sp³)–H Carbonylative Arylation of Azaarylmethyl Amines

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1119
Nickel-Catalyzed Ring-Opening Allylation of Cyclopropanols with Allylic Carbonates

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1120
Rhodium-Catalyzed Stereoselective Synthesis of Enones and Enals from 2,3-Allenols and Organoboronic Acids FREIER ZUGRIFF

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1121
Copper-Catalyzed Amination of Secondary Alkyl Iodides

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1122
Stereodivergent Aldehyde α-Allylation with 1,3-Dienes

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1123
Palladium-Catalyzed Dearomatization of Nitroindoles

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1124
Palladium-Catalyzed Carbonylative-Amination Reaction Generating Fluorinated β-Lactams

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1125
Regiodivergent Hydroalkenylation of 1,6-Enynes with Acrylates and Alkenes

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1126
Nickel-Catalyzed Cross-Coupling of α-Magnesiated Nitriles by Using a Benzonitrile Ligand

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Polymer-Supported Synthesis
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1127
Selective Synthesis of Imines and Secondary Amines by Homocoupling of Primary Amines

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1128
Cobalt-Catalyzed Synthesis of Tetrahydropyridine Derivatives and Oxidation of Benzylic Alcohols

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1129
Zirconium Metal–Organic Framework Catalyzed Direct Amide-Bond Formation FREIER ZUGRIFF

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1130
Hydrogenation of Quinolines Catalyzed by Tungsten- Doped Cobalt Nanoparticles

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1131
N-Alkylation of Amines with Aldehydes Catalyzed by a Graphene-Co-Shelled Ni/NiO@C Nanocatalyst

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1132
Synthesis of Pyrans by a Zirconium-Catalyzed Three-Component Condensation

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1133
Ruthenium-Catalyzed Transformations of 2,5-Hexanediones into Furans or Pyrrolidines

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1134
Controlled Hydrogenation of Azoarenes to Hydrazoarenes on Palladium/Carbon

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1135
Aerobic Oxidation of α-Diazo Esters Catalyzed by Charcoal-Supported Copper Nanoparticles

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1136
Palladium-Catalyzed α-Arylation of Ketones in Water

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Organo- and Biocatalysis
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1137
Biocatalytic Directed Cationic Cyclization Cascades toward Fragrance Ingredients FREIER ZUGRIFF

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1138
Carbon-Bonding Interaction Catalyst

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1139
Organocatalytic Enantiodivergent Bromolactonizations

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1140
Development of a Novel Chiral Framework: The SPHENOL Backbone

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1141
Synthesis of Chiral Cyclazines by Aminocatalytic Stereoselective [8+2] Cycloaddition

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1142
Protecting Group-Free Late-Stage S-Glycosylation of Peptides

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1143
Visible-Light Photoredox-Catalytic Coupling of Aryl Chlorides via Radical Anions

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1144
Organocatalytic Kinetic Resolution of Amido Tertiary Allylic Alcohols

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1145
Cinchona-Alkaloid-Catalyzed Annulation Enables an Asymmetric Synthesis of Chiral Oxacycles

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1146
Chiral Triazolium Salt-Catalyzed Asymmetric Cyanoalkylation of Electron-Deficient Olefins

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Chemistry in Medicine and Biology
z1147
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1147
Aziridines Cross-Dimerize to Larger N-Heterocycles FREIER ZUGRIFF

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1148
Photocatalyzed Site-Selective Tyrosine Bioconjugation

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1149
Doubly Caged Puromycin

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1150
A Novel P(V)-Based Reagent for Asymmetric Synthesis of Thiophosphoramidates

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1151
Eschenmoser Sulfide Contraction in the Synthesis of Kinase Inhibitors

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1152
Gram-Scale Synthesis of Iboxamycin

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1153
Optical Control of Phosphatidic Acid Signaling

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1154
Beating Resistant Plasmodium Parasites with the Antimalarial MMV688533

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1155
Potent and Selective Orphan GPCR Agonist for the Treatment of Schizophrenia

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1156
Activity-Based Probe for Monitoring Ethylene

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1157
Optical Control of Sodium Channels

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1158
A Rigid Vitamin Diet: Allenic derivatives of Vitamin D

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Peptide Chemistry
z1159
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1159
Organoboron-Catalyzed Synthesis of Serine- and Threonine-Derived Weinreb Amides

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1160
Palladium-Catalyzed C–H Functionalization of Cyclic-Aminal-Protected Peptides

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1161
Synthesis of Sulfonyl Fluoro Peptides by an Ugi Reaction FREIER ZUGRIFF

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1162
Unnatural Peptide Synthesis by Photochemical Acyl Radical Addition of Dehydroalanine

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1163
Palladium-Catalyzed Modification of Aspartic Acid-Containing Peptides

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1164
Electrochemical Synthesis of α-Amino Esters

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1165
Enantioselective Synthesis of 2-Chloroaziridines

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1166
Chiral Phosphoric Acid-Catalyzed Synthesis of α-Amino Esters

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1167
Ruthenium-Catalyzed Dehydrogenative Amidation of Alcohols by Amines

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1168
Unnatural α-Amino Acid Synthesis by Photoinduced Alkylation of Dehydroalanine

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1169
Synthesis of a Side-Chain-Tethered Solid Support for Peptide Synthesis FREIER ZUGRIFF

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1170
Synthesis of γ-Oxo-α-Amino Acids by Iridium Catalysis

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Flow Chemistry
z1171
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1171
Photocatalytic C(sp³)–H Heteroarylation in Flow

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1172
Decarboxylation and Decarboxylative Deuteration of Carboxylic Acids by Using a Ag–Bi Hybrid Material

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1173
A Fixed-Bed Approach for Wittig-Type Olefinations in Continuous Flow

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1174
Ozone-Mediated Oxidation of Amines and Pyridines under Flow Conditions

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