Synthesis

Issue 20 · October 2023

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table of contents
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short review
3239
Tibbetts, Joshua D.; Askey, Hannah E.; Cao, Qiao; Grayson, James D.; Hobson, Sophie L.; Johnson, George D.; Turner-Dore, Jacob C.; Cresswell, Alexander J.:
Decarboxylative, Radical C–C Bond Formation with Alkyl or Aryl Carboxylic Acids: Recent Advances
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feature
3251
Homer, Amal; Seitz, Oliver:
New Thiazole Orange Derivatives for Improved Fluorescence Signaling of DNA FIT Probes

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psp
3263
Broudic, Nathan; Pacheco-Benichou, Alexandra; Fruit, Corinne; Besson, Thierry:
Synthesis of Trifunctional Thiazole-Fused Anthranilonitrile and Anthranilic Acid Derivatives

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paper
3272
Alizadeh, Abdolali; Rostampoor, Azar; Hasanpour, Hamidreza:
Green Synthesis of Five-Membered Hetarene N-Oxides: A Designed Approach to the Synthesis of Substituted Chromeno[3,4-c]pyrrole-2-oxides

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CIF File (OTHER)
3281
Enagandhula, Damodar; Adepu, Raju; Mainkar, Prathama S.:
Proline-Catalyzed Diastereoselective Synthesis of Dihydroquinolinyl-Spirooxindole via Aza-Michael/Aldol Reaction

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3289
García-Santos, William H.; Quiroz-Mendoza, Ariadna M.; Mayorquín-Torres, Martha C.; Flores-Álamo, Marcos; Iglesias-Arteaga, Martin A.:
Palladium-Catalyzed Synthesis of Benzofuran Spiroketals Derived from Cholesterol; NMR and X-ray Characterization

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3297
Wong, Yuk Fai; Pettus, Thomas R. R.:
Synthesis of Naturally Racemic Marilines B & C through Multicomponent Reactions Involving ortho-Quinone Methides and Various Nitrogen Nucleophiles

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3303
Sarkar, Rumpa; Samanta, Surya Kanta; Menon, Anila M.; Chopra, Deepak; Ganguly, Debabani; Bera, Mrinal K.:
Synthesis of Quinoline and Quinolin-2(1H)-one Derivatives via Nickel Boride Promoted Reductive Cyclization

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Supplementary Material

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3315
Basceken, Sinan:
Synthesis of N-Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH₄

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3329
Singh, Manpreet; Vaishali, Vaishali; Deepika, Deepika; Jyoti, Jyoti; Sharma, Shubham; Banyal, Naveen; Kumar, Prashant; Budhalakoti, Bharti; Malakar, Chandi C.; Singh, Virender:
Transition-Metal-Free Cascade C–N Bond Formation: An Effective Strategy for the Synthesis of β-Carboline N-Fused Imidazolium Acetates and Estimation of their Light-Emitting Properties

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3342
Sato, Yu; Ukei, Takahiro; Tsugeno, Hiromasa; Suga, Takuya; Soeta, Takahiro; Ukaji, Yutaka:
Asymmetric Hetero-Diels–Alder Reaction of 4-Phenyl-1,2,4-triazole-3,5-dione with 2,4-Dienyl Carboxylic Acids

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3349
Bian, Chuan-Cai; Li, Yong-Qiang; Yang, Hao-ran; Yu, Xiao-Ming:
Scalable, Stereocontrolled, Total Synthesis of Carolacton

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3364
Zhang, Xinqin; Wu, Qiong; Yang, Qin; Fu, Yang; Peng, Yiyuan:
Rhodium-Catalyzed C–H Activation of 2-Arylquinazolinones and Cyclization with Elemental Sulfur via C–S/S–N Bond Formation to Access 7H-Benzo[4,5]isothiazolo[3,2-b]quinazolinones

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3373
Tao, Xiang-Feng; Qin, Hua-Li:
A General Protocol for the Chemo- and Stereoselective Construction of α,β-Unsaturated γ-Amino Sulfonyl Fluorides

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3382
Zaheer, Mohd Khalid; Vaishanv, Narendra Kumar; Kumar, Awadhesh; Mishra, Sameer; Kant, Ruchir; Mohanan, Kishor:
Efficient α-Arylation of α-Fluoro-α-nitrosulfonylmethanes Employing Diaryliodonium Salts

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CIF File (OTHER)
3393
Zhu, Yue-Lu; Yan, Jie; Xu, Xiu-Xuan; Sun, Zong-Yu; Chen, Jiao:
Copper-Catalyzed Coupling of N-Phenoxyacetamides and 2H-Azirines for Synthesis of α-Amino Oxime Ethers

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3402
Bondarenko, Andriy V.; Kozyriev, Yevhenii K.; Vashchenko, Bohdan V.; Grygorenko, Oleksandr O.:
Synthesis of 2,2-Disubstituted and 2,2,3-Trisubstituted 1,4-Dioxane-Derived Building Blocks

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errata
e1
Singh, Manpreet; Vaishali, Vaishali; Deepika, Deepika; Jyoti, Jyoti; Sharma, Shubham; Banyal, Naveen; Kumar, Prashant; Budhalakoti, Bharti; Malakar, Chandi C.; Singh, Virender:
Erratum - Transition-Metal-Free Cascade C–N Bond Formation: An Effective Strategy for the Synthesis of β-Carboline N-Fused Imidazolium Acetates and Estimation of their Light-Emitting Properties
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e2
Basceken, Sinan:
Erratum - Synthesis of N-Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH₄
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D’Amaral, Melissa C.; Andrews, Keith G.; Denton, Ross; Adler, Marc J.:
Silyl Esters as Reactive Intermediates in Organic Synthesis

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Synthesis

Linked PDF of Table of Contents

Decarboxylative, Radical C–C Bond Formation with Alkyl or Aryl Carboxylic Acids: Recent Advances

New Thiazole Orange Derivatives for Improved Fluorescence Signaling of DNA FIT Probes

Synthesis of Trifunctional Thiazole-Fused Anthranilonitrile and Anthranilic Acid Derivatives

Green Synthesis of Five-Membered Hetarene N-Oxides: A Designed Approach to the Synthesis of Substituted Chromeno[3,4-c]pyrrole-2-oxides

Proline-Catalyzed Diastereoselective Synthesis of Dihydroquinolinyl-Spirooxindole via Aza-Michael/Aldol Reaction

Palladium-Catalyzed Synthesis of Benzofuran Spiroketals Derived from Cholesterol; NMR and X-ray Characterization

Synthesis of Naturally Racemic Marilines B & C through Multicomponent Reactions Involving ortho-Quinone Methides and Various Nitrogen Nucleophiles

Synthesis of Quinoline and Quinolin-2(1H)-one Derivatives via Nickel Boride Promoted Reductive Cyclization

Synthesis of N-Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH₄

Transition-Metal-Free Cascade C–N Bond Formation: An Effective Strategy for the Synthesis of β-Carboline N-Fused Imidazolium Acetates and Estimation of their Light-Emitting Properties

Asymmetric Hetero-Diels–Alder Reaction of 4-Phenyl-1,2,4-triazole-3,5-dione with 2,4-Dienyl Carboxylic Acids

Scalable, Stereocontrolled, Total Synthesis of Carolacton

Rhodium-Catalyzed C–H Activation of 2-Arylquinazolinones and Cyclization with Elemental Sulfur via C–S/S–N Bond Formation to Access 7H-Benzo[4,5]isothiazolo[3,2-b]quinazolinones

A General Protocol for the Chemo- and Stereoselective Construction of α,β-Unsaturated γ-Amino Sulfonyl Fluorides

Efficient α-Arylation of α-Fluoro-α-nitrosulfonylmethanes Employing Diaryliodonium Salts

Copper-Catalyzed Coupling of N-Phenoxyacetamides and 2H-Azirines for Synthesis of α-Amino Oxime Ethers

Synthesis of 2,2-Disubstituted and 2,2,3-Trisubstituted 1,4-Dioxane-Derived Building Blocks

Erratum - Transition-Metal-Free Cascade C–N Bond Formation: An Effective Strategy for the Synthesis of β-Carboline N-Fused Imidazolium Acetates and Estimation of their Light-Emitting Properties

Erratum - Synthesis of N-Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH₄

Silyl Esters as Reactive Intermediates in Organic Synthesis