DOI:
10.1055/s-00000084
Synthesis
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Determination of the concentration: In a dried and argon-flushed Schlenk flask with gas inlet and rubber septum, an exactly known amount of menthol (approx. 0.8 mmol) and a few mg of 1,10-phenanthroline were dissolved in anhyd THF (2.5 mL). The -PrMgBr solution was added dropwise until blue color appeared. See: Watson SC, Eastham JF,
J. Organomet. Chem.. 1967; 9 165
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