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Synthesis 1990; 1990(9): 755-756
DOI: 10.1055/s-1990-27005
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2,3-Dihydro-1,4-dioxin in Organic Chemistry; Part II.1 Palladium-Catalyzed Acylations of 5-Tributylstannyl-2,3-dihydro-1,4-dioxin: Preparation of 5-Acyl-2,3-dihydro-1,4-dioxins

Valérie Blanchot* , Marcel Fétizon, Issam Hanna
  • *Laboratoire de Synthèse Organique, Ecole Polytechnique, F-91128 Palaiseau Cedex, France
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Publication Date:
17 September 2002 (online)

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5-Tributylstannyl-2,3-dihydro-1,4-dioxin, readily prepared from 5-lithio-2,3-dihydro-1,4-dioxin and chlorotributyltin, smoothly undergoes palladium-catalyzed coupling reactions with acid chlorides, affording 5-acyl- 2,3-dihydro-1,4-dioxin in high yield.

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