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Synlett 1994; 1994(7): 535-536
DOI: 10.1055/s-1994-22919
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PeSeNPhth-TMSOTf as a Promotor of Thioglycoside

Hiroki Shimizu* , Yukishige Ito, Tomoya Ogawa
  • *The Institute of Physical and Research (RIKEN), Wako-shi, Saitama, 351-01, JAPAN
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Publication Date:
18 September 2002 (online)

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A new method to activate thioglycosides is described. The combined use of PhSeNPhth and TMSOTf was demonstrated to be a powerful promoter of thioglycoside. The reaction proceeds rapidly even at low temperature to give O-glycoside in a high yield. The effects of solvents and reaction temperature were also investigated.

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