CC BY-NC-ND 4.0 · Eur J Dent 2020; 14(01): 152-156
DOI: 10.1055/s-0040-1705075
Original Article

In Vitro Evaluation of Physical and Mechanical Properties of Light-Curing Resin Cement: A Comparative Study

Luís Felipe Espíndola-Castro
1   Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil
,
Oscar Felipe Fonseca de Brito
1   Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil
,
Larissa Gabrielle Assis Araújo
1   Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil
,
Izabella Luiza Aragão Santos
1   Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil
,
Gabriela Queiroz De Melo Monteiro
1   Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil
› Author Affiliations

Abstract

Objective The aim of study was to evaluate in vitro the surface hardness, sorption, solubility, and color stability of three light-cured resin cements, namely RelyX Veneer (RLX), Variolink Veneer (VLK), and All Cem Veneer (ACV).

Materials and Methods Cylindrical samples (15 × 1 mm) were made for each group using a metallic mold (n = 10). Vickers microhardness test was performed, and average hardness was calculated from three indentations (300 gf/15s) per sample. The sorption and solubility of the materials were evaluated according to ISO 4049:2009 based on three samples weighing: initial (m 1), after immersion in distilled water for 7 days (m 2), and final (after removal of all moisture [m 3]). The color change was observed using a digital spectrophotometer, at three different time points, baseline, 1 day, and 1 week of immersion in coffee and distilled water (control).

Statistical Analysis Shapiro–Wilk test was used to analyze the normality of the data, and groups were compared using Kruskal–Wallis and Mann–Whitney tests. A significance level of 5% was used.

Results RLX showed the highest microhardness mean values (36.96 VHN), but higher sorption (23.2 µg/mm3) and solubility (2.40 µg/mm3), with statistically significant differences with the other groups. For color stability, higher ∆E was observed for the samples immersed in coffee (p = 0.009). The VLK resin cement presented statistically significant differences from the other groups, with higher color changes in coffee at 1 day (15.14) and after 1 week (23.65).

Conclusion RLX resin cement showed better hardness results. All materials tested performed satisfactorily for sorption and solubility according to ISO 4049:2009. All materials showed high-staining values after 1 week of immersion in coffee.



Publication History

Article published online:
13 March 2020

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Thieme Medical and Scientific Publishers Private Ltd.
A-12, Second Floor, Sector -2, NOIDA -201301, India

 
  • References

  • 1 Almohareb T, Alkatheeri MS, Vohra F, Alrahlah A. Influence of experimental staining on the color stability of indirect computer-aided design/computer-aided manufacturing dental provisional materials. Eur J Dent 2018; 12 (02) 269-274
  • 2 Blum IR, Nikolinakos N, Lynch CD, Wilson NH, Millar BJ, Jagger DC. An in vitro comparison of four intra-oral ceramic repair systems. J Dent 2012; 40 (11) 906-912
  • 3 Novais VR, Raposo LH, Miranda RR, Lopes CC, Simamoto PC, Soares CJ. Degree of conversion and bond strength of resin-cements to feldspathic ceramic using different curing modes. J Appl Oral Sci 2017; 25 (01) 61-68
  • 4 Leal CL, Queiroz A, Foxton RM, Argolo S, Mathias P, Cavalcanti AN. Water sorption and solubility of luting agents used under ceramic laminates with different degrees of translucency. Oper Dent 2016; 41 (05) E141-E148
  • 5 Petropoulou A, Vrochari AD, Hellwig E, Stampf S, Polydorou O. Water sorption and water solubility of self-etching and self-adhesive resin cements. J Prosthet Dent 2015; 114 (05) 674-679
  • 6 Silva EM, Noronha-Filho JD, Amaral CM, Poskus LT, Guimarães JG. Long-term degradation of resin-based cements in substances present in the oral environment: influence of activation mode. J Appl Oral Sci 2013; 21 (03) 271-277
  • 7 Pan Y, Xu X, Sun F, Meng X. Surface morphology and mechanical properties of conventional and self-adhesive resin cements after aqueous aging. J Appl Oral Sci 2018; 27 (01) e20170449
  • 8 Alshali RZ, Salim NA, Satterthwaite JD, Silikas N. Long-term sorption and solubility of bulk-fill and conventional resin-composites in water and artificial saliva. J Dent 2015; 43 (12) 1511-1518
  • 9 de Brito O, de Oliveira I, Monteiro G. Hydrolytic and biological degradation of bulk-fil and self-adhering resin composite. Oper Dent 2019; 44 (05) E223-E233
  • 10 Martin N, Jedynakiewicz N. Measurement of water sorption in dental composites. Biomaterials 1998; 19 (1-3) 77-83
  • 11 Marghalani HY. Sorption and solubility characteristics of self-adhesive resin cements. Dent Mater 2012; 28 (10) e187-e198
  • 12 Ramos NC, Luz JN, Valera MC, Melo RM, Saavedra G, Bresciani E. Color stability of resin cement exposed to aging. Oper Dent 2019; 44 (06) 609-614
  • 13 Salgado VE, Cavalcante LM, Moraes RR, Davis HB, Ferracane JL, Schneider LF. Degradation of optical and surface properties of resin-based composites with distinct nanoparticle sizes but equivalent surface area. J Dent 2017; 59 (01) 48-53
  • 14 Shiozawa M, Takahashi H, Asakawa Y, Iwasaki N. Color stability of adhesive resin cements after immersion in coffee. Clin Oral Investig 2015; 19 (02) 309-317
  • 15 Malchiodi L, Zotti F, Moro T, De Santis D, Albanese M. Clinical and Esthetical Evaluation of 79 Lithium Disilicate Multilayered Anterior Veneers with a Medium Follow-Up of 3 Years. Eur J Dent 2019; 13 (04) 581-588
  • 16 International Organization for Standardization. ISO 4049: Dentistry polymer – based filling, restorative and luting materials. Switzerland, 2009. Available at: https://www.iso.org/standard/42898.html. Accessed February 5, 2020
  • 17 Monteiro, GQM, Oliveira ILM, Brito, OFF. Guedes BP, Amorim MSML, Maia AMA. Chromatic and surface alterations in enamel subjected to brushing with desensitizing whitening toothpaste. Eur J Gen Dent 2016; 5 (03) 115-121
  • 18 Venter SAS, Fávaro AL, Radovanovic E, Girotto EM. Hardness and degree of conversion of dental restorative composites based on an organic-inorganic hybrid. Mater Res 2013; 16 (04) 898-902
  • 19 De Souza G, Braga RR, Cesar PF, Lopes GC. Correlation between clinical performance and degree of conversion of resin cements: a literature review. J Appl Oral Sci 2015; 23 (04) 358-368
  • 20 Demarco FF, Corrêa MB, Cenci MS, Moraes RR, Opdam NJ. Longevity of posterior composite restorations: not only a matter of materials. Dent Mater 2012; 28 (01) 87-101
  • 21 Nayyer M, Zahid S, Hassan SH. et al. Comparative abrasive wear resistance and surface analysis of dental resin-based materials. Eur J Dent 2018; 12 (01) 57-66
  • 22 Arocha MA, Mayoral JR, Lefever D, Mercade M, Basilio J, Roig M. Color stability of siloranes versus methacrylate-based composites after immersion in staining solutions. Clin Oral Investig 2013; 17 (06) 1481-1487
  • 23 Falkensammer F, Arnetzl GV, Wildburger A, Freudenthaler J. Color stability of different composite resin materials. J Prosthet Dent 2013; 109 (06) 378-383
  • 24 Malekipour MR, Sharafi A, Kazemi S, Khazaei S, Shirani F. Comparison of color stability of a composite resin in different color media. Dent Res J (Isfahan) 2012; 9 (04) 441-446
  • 25 Ertaş E, Güler AU, Yücel AC, Köprülü H, Güler E. Color stability of resin composites after immersion in different drinks. Dent Mater J 2006; 25 (02) 371-376
  • 26 Bagheri R, Burrow MF, Tyas M. Influence of food-simulating solutions and surface finish on susceptibility to staining of aesthetic restorative materials. J Dent 2005; 33 (05) 389-398
  • 27 Johnston WM, Kao EC. Assessment of appearance match by visual observation and clinical colorimetry. J Dent Res 1989; 68 (05) 819-822
  • 28 Zafa MS, Khan E, Aversa R, Petrescu RV, Apicella A, Petrescu FI. Influence of curing light type and staining medium on the discoloring stability of dental restorative composite. Am J Biochem Biotechnol 2017; 13 (01) 42-50
  • 29 Ferracane JL, Condon JR. Rate of elution of leachable components from composite. Dent Mater 1990; 6 (04) 282-287
  • 30 Ortengren U, Wellendorf H, Karlsson S, Ruyter IE. Water sorption and solubility of dental composites and identification of monomers released in an aqueous environment. J Oral Rehabil 2001; 28 (12) 1106-1115
  • 31 Zhang Y, Xu J. Effect of immersion in various media on the sorption, solubility, elution of unreacted monomers, and flexural properties of two model dental composite compositions. J Mater Sci Mater Med 2008; 19 (06) 2477-2483