Synfacts

Issue 02 · February 2015

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Synthesis of (+)-Linoxepin

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Synthesis of NVP-HSP990

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Synthesis of Rubriflordilactone A

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Synthesis and Structural Revision of (+)-Uprolide G Acetate

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Total Synthesis of Disorazole C₁

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Copper-Promoted Synthesis of Pyrimidines by Dimerization of Amino Esters

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Indolines by Heck Reaction, C–H Activation, and Amination with Diaziridinones

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Synthesis of 1,6-Annulated 2-Pyridones by Nickel-Catalyzed Hydroarylation

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0126
Rhodium(II)-Catalyzed Synthesis of Fused Azepine Derivatives

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0127
Preparation of 2,5-Dihydroazepines from Dienyltriazoles by [4+3] Cycloaddition

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0128
Dihydrofurans and Dihydroindoles by Annulation of Tethered Triazoles

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0129
Rhodium(III)-Catalyzed Synthesis of 2H-Chromenes

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0130
Prins Reaction–Pinacol Rearrangement Route to Oxaspiro[4.5]decan-1-one

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0131
Quinolines from the Reaction of o-Halo N-Arylhydroxylamines with Olefins

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0132
Cu(I)- and Pd(II)-Catalyzed Synthesis of Functionalized Imidazo[1,2-a]pyridines

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0133
Copper/NHC-Catalyzed Synthesis of 1,4-Diarylimidazoles from Isocyanides

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0134
Palladium-Catalyzed Synthesis of Oxazoles and Thiazoles

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0135
Synthesis of 7-Trifluoromethylpyrazolo[1,5-a]pyrimidines

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0136
Synthesis of Octahydro-2H-chromenes via Prins Reaction–Arylthiolation

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Stereoselective Synthesis of l-Rhamnose-Derived Fused Triazoles

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Synthesis of Materials and Unnatural Products
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0139
Lights,…and Action! Photoisomerism Control of Redox Properties

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Lithium Chloride Carbenoid Mediated Dehydrocoupling of Phosphines

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0141
Synthesis of Radially π-Conjugated Thiophene-Based Macrocycles

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0142
Dyeing of Laughter

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0143
Fluoride Activation for Mild Etherification

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0144
Azobenzene Stars in a Disappearing Act

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A Superacid Serves Up Benzo[c]thiophenes

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Biaryl Macrocycles via Metal-Free Coupling

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Traceless Cage Catalysis

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Regioselective, Late-Stage Decarboxylative Direct Arylation of BODIPYs

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Synthesis of Nylon 11 and 12 Precursors from a Renewable Feedstock

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12 nm Soluble Wheel from c. 1878
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Boranes Teach Old rr-P3HT New Tricks

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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Asymmetric Alkylation via Photoredox Pathway Using a Chiral Iridium Complex
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Asymmetric Scandium-Catalyzed Aza-Michael Reaction of Pyrazoles

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0155
Copper(I)-Mediated Asymmetric Boryl Substitution of Allyl Acetals
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0156
Palladium-Catalyzed Enantioselective C–H Iodination at Room Temperature

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0157
Copper(II)-Containing Bistetracarboline Amides in Enantioselective Henry Reactions

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0158
Asymmetric Propargylic Alkylation of Enamines Catalyzed by Copper

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0159
One-Pot Multicomponent Synthesis of NHC Ligands

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0160
Enantioselective Epoxidation of α,β-Unsaturated Esters by Iron(II) Catalysis

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0161
Palladium-Catalyzed Asymmetric Decarboxylative Allylation

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0162
Allylation of Ketones and Aldehydes with Allenes and Silylboranes

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0163
Enantioselective Diboration of Vinyl Boronates

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0164
Carbotrifluoromethylation of Alkynes Catalyzed by Copper

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0165
Enantioselective Ruthenium-Catalyzed Oxidation of Spirocyclic Oxindoles

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0166
Pd-Mediated Enantioselective Hayashi–Miyaura Reaction Using Chiral Palladacycles

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0167
Gold-Catalyzed Stereocontrolled Synthesis of Enamides

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0168
Gold/Chiral Phosphoric Acid Catalyzed Hydroamination–Hydroarylation of Alkynes

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0169
Stereoselective Macrocyclic Ring-Closing Metathesis

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0170
Asymmetric Propargylation of Benzofuranones Catalyzed by Copper

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0171
Desymmetrization of meso-Epoxides Using Thiols

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0172
Asymmetric Three-Component Reaction Catalyzed by Rhodium

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0173
Synthesis of Cyclopropylboronates via Desymmetrization

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Enantioselective Pd-Catalyzed Cycloaddition of Vinylethylene Carbonates and Isocyanates

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0175
Enantioselective Scandium-Catalyzed 1,5-Hydride Shift/Ring Closure of Oxindoles

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Asymmetric Hydrogenation via Capture of Active Intermediates

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0177
Asymmetric Synthesis of 2,3-Dihydropyrroles Catalyzed by Scandium(III)

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0178
Palladium-Catalyzed C(sp³)–H Stereoretentive Olefination with Vinyl Iodides

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Intramolecular Asymmetric Allylic Amidation via Iridium Catalysis

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Metal-Mediated Synthesis
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Carbonylation of Organolithiums Using Serially Connected Flow Reactors

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0182
Conjugate Alkynylation–Silver(I)-Catalyzed Lactonization

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Directed Regioselective 2,5- and 3,5-Dimagnesiations of Substituted Arenes
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Zinc Reagents for the Copper-Catalyzed Perfluoroalkylation of Aryl Iodides

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Iron-Catalyzed Hydromagnesiation

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0187
Sandmeyer Difluoromethylation

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0188
Fluorinative Cross-Coupling of Olefins

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0189
Asymmetric Alkylation of Acylsilanes

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0190
Regioselective Tandem Synthesis of 3-Halo-5-Substituted Isoxazoles

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0191
1,4-Addition of Heteroaryl Boronates to Enones

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0192
Dibromination of Alkynes

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0193
Copper-Mediated Direct Alkoxylation

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0194
Formation of Silylated Hydrazones from Dimethylalkynylaluminum Reagents

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0195
TMP-Magnesium Bases for the Preparation of Cyanopyrazoles

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Organo- and Biocatalysis
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0197
NHC-Catalyzed α-Fluorination of Aldehydes

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0198
Biocatalytic Gram-Scale Halogenation of Tryptophan

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0199
Metal-Free Carbonylations by Photoredox Catalysis
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0200
Phosphoric Acid Catalyzed Dearomative α-Amination of 2-Naphthols

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0201
[4+2] Annulation of Allenones and β,γ-Unsaturated α-Keto Esters

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0202
Asymmetric 1,6-Conjugate Addition of Aldehydes to p-Quinone Methides

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0203
Enantioselective Selenocyclization via Dynamic Kinetic Resolution

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0204
Catalytic, Enantioselective Sulfenofunctionalization of Alkenes

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0205
Organocatalytic N-Methylation with Carbon Dioxide

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0206
The Catalytic Asymmetric Abramov Reaction

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Polymer-Supported Synthesis
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0207
Asymmetric Conjugate Addition of ArB(OH)₂ to Enones with Chiral Rh-POF
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0208
Pd@PDEB: An Efficient Catalyst for Cross-Coupling Reactions

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0209
An Expedient Synthesis of 3,3′-Diaryl H₈-BINOLs

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0210
Bifunctional RuNPs@SILP for the Deoxygenation of Biomass Substrates

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0211
Hydrogenation of Phenylacetylene with Platinum Nanoparticles/ZTC

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0212
Hydroalkoxylation with Highly Oxidized Pd NPs

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0213
One-Pot Synthesis of Dihydropyrano[2,3-c]Pyrazoles with 4 Å MS

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0214
Huisgen Cycloaddition with Graphene Oxide Supported Copper Nanoparticles

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0215
Transamidation of Amides with Amines Using [PyPS]₃PW₁₂O₄₀

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0216
Nucleophilic Substitution Using Polystyrene-Supported Ionic Liquid Catalysts

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0217
Pd/CeO₂-Mediated Synthesis of N-(2-Pyridyl)-indoles via C–H Activation

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0218
Synthesis of Pyrroles Using [RuCl₂(p-cymene)]₂ in PEG-400

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0219
Copper-Free Sonogashira Reaction Using PVC-Supported Pd Complex

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0220
Alcoholysis of Epoxides Using Graphite Oxide

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0221
Solid-Supported Iron Catalysts for C–H Functionalization Reactions

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0222
Alkyne Semihydrogenation Using First-Row Transition-Metallated POPs

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Erratum
223
Copper-Catalyzed Silylation of Aldehydes

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