Synfacts

Issue 08 · August 2016

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SYNFORM ISSUE 2016/08
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Synthesis of Natural Products and Potential Drugs
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Total Synthesis of (−)-6-epi-Ophiobolin N
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Synthesis of Darunavir

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Synthesis of PDE4 Inhibitors
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Large Scale Synthesis of Eupalinilide E

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Synthesis of (+)-Dictyoxetane

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Synthesis of an Inhibitor of Influenza Virus Replication

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Syntheses of Decinnamoyltaxinine E and Taxabaccatin III

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Synthesis of (R)-JM 1232 by Asymmetric Alkynylation

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0775
Synthesis of a Glucocorticoid Receptor Modulator

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Synthesis of a tRNA–Guanine Transglycosylase Inhibitor

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Total Syntheses of Erythrina Alkaloids

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0778
Synthesis of LpxC Inhibitor LP-058

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0779
Synthesis of Strongylophorine-2

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Synthesis of Indolactam V

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Synthesis of (+)-Minfiensine

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Synthesis of Heterocycles
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0783
Minisci-Type Reaction of Nonactivated Ethers with Heterocycles

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0784
Fluorinated Triazoles by Using a Heterobifunctional Fluoroalkylation Reagent

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0785
1,3-Dipolar Cycloaddition of Azomethine Imines with Enecarbamates

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0786
Synthesis of Chiral Piperazinones from Aziridine Aldehyde Dimers

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0787
[3+2] Cycloaddition Route to Imidazopyrrolo-Fused Isoxazoles

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0788
Synthesis of Enantiomerically Enriched Isoquinoline Derivatives

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0789
Synthesis of Pyrroles by Rhodium-Catalyzed Hydroacylation of Alkynylamines

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0790
Synthesis of 3-Bromoquinoline-2(1H)-thiones

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0791
Functionalized Arynes from Aryl Iodonium Salts

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0792
Four-Component Palladium-Catalyzed Synthesis of Pyrroles

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Palladium-Catalyzed Synthesis of (Spiro)polyheterocycles by Domino Post-Ugi Route

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0794
Halogenated Piperidines and Tetrahydropyrans by the Prins Reaction

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0795
Palladium-Catalyzed Synthesis of Phenanthridinones by Dual C–H Activation

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0796
Heteroannulation Route to Fluorinated Purine Derivatives

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Synthesis of Materials and Unnatural Products
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Synthesis of Symmetrical and Unsymmetrical 1,4-Dithiins

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Two Dots in One ‘DIAn’

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0799
Bottoms Up! Ball Mill Synthesis of Water-Soluble ZnO from Molecular Precursors

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0800
A Novel TBI Building Unit for Semiconducting Polymers

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0801
Synthesis of Twisted PAH via [4+4] Dimerization

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Switch-Hitter but Primarily a Dienophile

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Cyclic Polyacetylenes by Tungsten Catalysis

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One-Pot Synthesis of Tetraphene and Construction of Expanded Conjugated Aromatics

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0805
Calcium-Sensitive Photocage: An In Situ Ca²⁺ Sensor

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0806
Let Me Reiterate…Sequence Control in Living Radical Polymerizations

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0807
Making the Most of γ-Butyrolactones: Catalytic, Chemoselective, Clickable

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0808
Feeling Lucky? Making d20 Dice Stand On a Vertex

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0809
Asymmetric Michael Addition Reaction via Rhodium Catalyst Fragmentation
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0810
Rhodium-Catalyzed Asymmetric Cycloisomerization of (E)-1,6-Enynes

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0811
Quaternary Stereocenters by Asymmetric Allylic Alkylation

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0812
Pd-Catalyzed Diastereoselective Synthesis of Borylated Chromans

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0813
Enantioselective Rhodium-Catalyzed Silylation of C−H Bonds

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0814
Enantio- and Regioselective Copper-Catalyzed Hydroboration of Internal Alkenes

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0815
Enantioselective and Diastereoselective Scandium-Catalyzed [3+3] Annulation

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0816
Asymmetric Nickel-Catalyzed Diels–Alder Reaction

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0817
Iridium-Catalyzed Asymmetric C–H Functionalization with Ethyl Diazoacetate

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0818
Cobalt-Catalyzed Regioselective Alkenylation of 8-Methylquinoline with Alkynes

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0819
Synthesis of Chiral Spiro-nitroprolinates by Silver(I) Catalysis

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0820
Desymmetrization of Cyclohexadienones by Conjugate Hydrosilylation

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0821
Asymmetric Iridium-Catalyzed Hydrogenation of Pyridinium Salts

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0822
Desymmetrization of Cyclopentenes by Rh-Catalyzed Hydroformylation Reaction

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0823
Synthesis of Indolines from 1,2,3-Triazoles by a Rhodium-Catalyst

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0824
Titanium-Catalyzed Asymmetric Epoxidation of N-Alkenyl Sulfonamides

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0825
Site- and Stereoselective Functionalization of Nonactivated Alkanes

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0826
Asymmetric [3+2] Cycloaddition by Synergistic Catalysis

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0827
Asymmetric Photoinduced Copper-Catalyzed C–N Coupling of Alkyl Chlorides

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0828
Enantioselective Rhodium-Catalyzed C−H Insertion of Carbenes

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0829
Asymmetric Hydrogenation of 1,8-Naphthyridines by Ruthenium(II) Catalysis

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0830
Copper-Catalyzed [3+2] Cycloaddition of Enones with a Trifluoromethyl Group

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0831
Highly Asymmetric Synthesis of α-Aryl Ketones

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0832
Palladium-Catalyzed Asymmetric Synthesis of Functionalized 2,3-Dihydrofurans

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0833
Axially Chiral Boron Catalyst for Asymmetric Piers Hydrosilylation

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0834
Palladium-Catalyzed Asymmetric Hydrogenation of Fluorinated Hydrazones

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0835
Copper-Catalyzed Mannich Type Reaction of Alkylamides

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0836
Copper(II)-Catalyzed (E)-Selective Hydrosilylation of Allenes

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0837
Rhodium-Catalyzed Stepwise Asymmetric Arylation of Cyclic Sulfamidates

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Metal-Mediated Synthesis
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0839
Enantioselective Addition of Organoboron Reagents to Fluoroketones
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0840
Oxidative Trifluoromethylation of Alkynes with Fluoroform-Derived CuCF₃

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0841
Magnesium-Catalyzed Hydroboration of Carbodiimides

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0842
Palladium-Catalyzed Carboperfluoroalkylation

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0843
Iron-Catalyzed Cross-Coupling of Tosylates

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0844
2,3-Dihydroisoxazole Synthesis from Alkynes and Nitrones

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0845
Palladium-Catalyzed Cross-Coupling of Allylboronic Acids with α-Diazoketones

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0846
Cobalt-Catalyzed Arylative Cyclization of Acetylenic Esters and Ketones

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0847
Coupling of Organocuprates with Propargyl Electrophiles

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0848
Nickel-Catalyzed Cyclization of Alkyne-Nitriles

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0849
Photoredox/Nickel Dual Catalytic Cross-Coupling

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0850
Nickel-Catalyzed Cross-Coupling of Anisoles with Alkylmagnesium Reagents

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0851
Carboxylation of Alkenes and Heteroaromatics

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0852
Multicomponent Cascade Synthesis

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0853
Chemoselective Primary Amination of Boronic Acids

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Organo- and Biocatalysis
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0855
N-Hydroxyphthalimide-Catalyzed Electrochemical Allylic Oxidation
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0856
A New Substituent for BINOL-Phosphate Catalysis

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0857
Proline-Catalyzed Enantioselective Synthesis of 2,3-Disubstituted Piperidines

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0858
Triflic Acid Catalyzed Enyne Cyclization

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0859
Iminium Catalysis in a Supramolecular Host

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0860
An Organocatalytic Approach to Enantiopure 2H- and 3H-Pyrroles

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0861
Organocatalytic Construction of Spiroindane Derivatives

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0862
Visible-Light-Promoted Synthesis of Benzo[b]phosphole Oxides

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0863
One-Pot Biocatalytic Cascade to Substituted Piperidines and Pyrrolidines

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Polymer-Supported Synthesis
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0865
Arylation of Pyrroles and Imidazoles with Bromobenzenes Using Pd@PPy

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0866
Peptide-Catalyzed Epoxidation with Inverted Juliá–Colonna Stereoselectivity

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0867
Organocatalyzed Asymmetric Michael Addition of Ketones and Nitrostyrenes
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0868
Chemoselective Reduction of Aldehydes with Pd-Nanoparticles

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0869
Homocoupling of Alkynes on Polystyrene-Supported Copper Catalyst

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0870
Gold/Titania-Catalyzed Semireduction of Alkynes by Formic Acid

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0871
Solid-Phase Syntheses of Polysubstituted 2-Sulfanylbenzimidazoles

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0872
A Functionalized Covalent Organic Framework for Formylation of Amines

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0873
Three-Component Synthesis of Propargylamines with Supported Au Nanoparticles

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0874
Reduction of Nitroarenes on Microsphere-Supported Silver Nanoparticles

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0875
An Activated Metal–Organic Framework Catalyst with a Lewis Acid

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0876
Gold-Catalyzed Oxidation of Anilines to Nitrosobenzenes by Hydrogen Peroxide

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0877
Hydrogenation of Enals and Enones on Supported Palladium Nanoparticles

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0878
Copper-Catalyzed Coupling of Arylboronic Acids with Sulfonyl Azides

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0879
Pd-Catalyzed Carbonylative Coupling of Triarylbismuthines with Aryl Iodides

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0880
Copper-Catalyzed Oxidative Coupling of Amines with Disulfides or Thiols

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0881
Ferrite Nanoparticle/Montmorillonite-Catalyzed Baeyer–Villiger Oxidation

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0882
Hydrosilylation of Terminal Alkynes with a Copper/Carbene-Functionalized Polymer

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