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Synlett 1995; 1995(6): 641-642
DOI: 10.1055/s-1995-5009
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Facile Aluminum Induced Synthesis of (Trifluoromethyl)trimethylsilane

Joseph Grobe* , Joachim Hegge
  • *Anorganisch-Chemisches Institut, Westfälische Wilhelms-Universität, Wilhelm-Klemm-Straße 8, D-48149 Münster, Germany, Fax: 0251/833169
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Publication Date:
31 December 2000 (online)

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An efficient trifluoromethylation of chlorotrimethylsilane with aluminum powder in N-methylpyrrolidinone is described. The reaction affords the title compound on a preparative scale in 62% isolated yield.

(Trifluoromethyl)trimethylsilane - bromotrifluoromethane - chlorotrimethylsilane - aluminum