Synlett

Issue 12 · December 1997

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1327
Cossu, Sergio; Fabris, Fabrizio; De Lucchi, Ottorino:
Synthetic Equivalents of Cyclohexatriene in [4+2]-Cycloaddition Reactions: Methods for Preparing Cycloadducts to Benzene

PDF (681 kb)
1335
Dürr, U.; Kisch, H.:
In the Dark and in the Light: Homogeneous and Heterogeneous Catalytic Activation of 1,2-Diazenes

PDF (591 kb)
letter
1342
Chattopadhyay, Shital K.; Pattenden, Gerald:
A Convergent Synthesis of the tris-Oxazole Ring System in Ulapualide A and Related Marine Metabolites

PDF (165 kb)
1345
Chattopadhyay, Shital K.; Pattenden, Gerald:
Towards a Total Synthesis of Ulapualide A. A Concise Synthesis of the tris-Oxazole Macrolide Core and Entire Carbon Skeleton

PDF (183 kb)
1349
Nenajdenko, Valentine G.; Krasovsky, Arkady L.; Lebedev, Mikhail V.; Balenkova, Elizabeth S.:
A Novel Efficient Synthesis of Heteroaryl Substituted α,β-Unsaturated Trifluoromethyl Ketones

PDF (152 kb)
1351
Lai, Chien-Hsun; Shen, Yin-Ling; Liao, Chun-Chen:
Synthesis of Stable Bromo-substituted Masked o-Benzoquinones and their Application to the Synthesis of Bicyclo[2.2.2]octenones

PDF (158 kb)
1353
Gao, Yuan; Yoshida, Yukio; Sato, Fumie:
In Situ Generation of Titanium-imine Complexes from Imines and Ti(OiPr)₄/2 iPrMgX, and Their Reactions with Alkynes, Nitriles and Imines

PDF (174 kb)
1355
Bulman Page, Philip C.; Bethell, Donald; Stocks, Paul A.; Heer, Jag P.; Graham, Andrew E.; Vahedi, Hooshang; Healy, Mark; Collington, Eric W.; Andrews, David M.:
Sulfur Oxidation Mediated by Imine Derivatives

PDF (276 kb)
1359
McAlonan, H.; Stevenson, P. J.; Thompson, N.; Treacy, A. B.:
Synthesis of trans-5-Substituted-indolizidin-3-one

PDF (151 kb)
1361
Attanasi, Orazio A.; Filippone, Paolino; Fiorucci, Chiara; Mantellini, Fabio:
Novel and Convenient Synthesis of 1,4-Dihydropyridazines and Pyridazines from Aminocarbonylazoalkenes

PDF (196 kb)
1363
Cacchi, Sandro; Fabrizi, Giancarlo; Marinelli, Fabio; Moro, Leonardo; Pace, Paola:
3-Aryl-2-Unsubstituted Indoles through the Palladium-Catalysed Reaction of o-Ethynyltrifluoroacetanilide with Aryl Iodides

PDF (343 kb)
1367
Cacchi, Sandro; Fabrizi, Giancarlo; Moro, Leonardo; Pace, Paola:
Stereo- and Regioselective Palladium-Catalysed Hydroarylation and Hydrovinylation of Functionalised Alkynes: a Route to Substituted Z-2-Cinnamyl Esters, 3-Chromen-2-ols, and Coumarins

PDF (325 kb)
1371
Probert, Gareth D.; Harding, Ross; Whitby, Richard J.; Coote, Steven J.:
Early Transition Metal Induced Intramolecular Cocyclisation/Elaboration Reactions Using a Cleavable Silicon Linker

PDF (341 kb)
1375
Yoshida, Akihiro; Mikami, Koichi:
Dramatic Changeover of Regioselectivity in the Reduction of Propargylic Phosphates by Palladium(0)/SmI₂/Proton Source System

PDF (168 kb)
1377
Kaufman, Teodoro S.:
Convenient One-pot Synthesis of Primary α-Alkoxystannanes

PDF (159 kb)
1379
Yang, Yang; Wang, Dong:
The Addition of Trimethylsilyl Cyanid to Carbonyl Compounds Using Yb(OTf)₃ as Lewis Acid Catalyst

PDF (165 kb)
1381
Ishii, Akihiro; Higashiyama, Kimio; Mikami, Koichi:
Asymmetric Addition Reactions of Grignard Reagents to Chiral Fluoral Hemiacetal: Asymmetric Synthesis of 1-Substituted-2,2,2-Trifluoroethylamines

PDF (161 kb)
1383
Liu, Zhi-Yu; Yu, Chen-Zhi; Yang, Jia-De:
Chiral Synthesis of the C_3-13 Segment of Epothilone A

PDF (136 kb)
1385
Maki, Shojiro; Niwa, Haruki; Hirano, Takashi:
Facile Cleavage Reactions of Styrylic Olefins using Electrochemical Methods

PDF (117 kb)
1387
Yoshizawa, Junko; Obitsu, Kazuyoshi; Maki, Shojiro; Niwa, Haruki; Hirano, Takashi; Ohashi, Mamoru:
Novel Dehydration Reaction of Neoanisatin and Transformation of Neoanisatin into Anisatin

PDF (108 kb)
1391
Andrés, Celia; Duque-Soladana, Juan P.; Iglesias, Jesús M.; Pedrosa, Rafael:
Unexpected Stereoselective 6-exo versus 7-endo Aryl Radical Cyclisation Controlled by Positional Isomers in a Chiral Octahydro-1,3-benzoxazine Moiety

PDF (199 kb)
1393
Baba, Yoshiyasu; Noutary, Carole; Ichikawa, Satsuki; Kusumoto, Tetsuo; Watanabe, Hisayuki; Adachi, Michiaki; Hotta, Hiroyasu; Nakajima, Yasuyuki; Arai, Kazutaka; Hiyama, Tamejiro:
Stereo- and Regioselective Bromination of 1,5-Cyclooctadiene Derivatives and Their Substitution Reactions with Organocopper Reagents

PDF (163 kb)
1395
Gesson, Jean-Pierre; Mondon, Martine; Pokrovska, Natacha:
Synthesis of Fused Aromatic [1,3]Dioxoles from 2-Hydroxymethylphenols

PDF (162 kb)
1400
Cacchi, Sandro; Carangio, Antonella; Fabrizi, Giancarlo; Moro, Leonardo; Pace, Paola:
A Convenient Synthesis of Nitrogen-Containing Heterocycles Bearing Amino Substituents from Heteroaryl Triflates

PDF (188 kb)
1403
Morera, Enrico; Ortar, Giorgio:
An Efficient Synthesis of 4-Aryl and 4-Vinylphenylalanines by Stille Cross-Coupling Reaction

PDF (266 kb)
1406
Johnson, Carl R.; Johns, Brian A.:
Suzuki Cross-Coupling of Carbohydrates: Synthesis of β-Arylmethyl-C-glycosides and Aryl-Scaffolded Trisaccharide Mimics

PDF (206 kb)
1409
Sajiki, Hironao; Hattori, Kazuyuki; Sako, Magoichi; Hirota, Kosaku:
A New Synthesis of Pyrazolo[3,4-d]pyrimidine-4,6(5H,7H)-diones by Oxidative N-N Bond Formation of 6-Amino-5-(N-aryliminomethyl)uracils Using Iodobenzene Diacetate

PDF (159 kb)
1411
Cassidy, John H.; Marsden, Stephen P.; Stemp, Geoffrey:
Stereoselective Synthesis of 2,3,5-Trisubstituted Tetrahydrofurans by an Allyl Silane Metathesis - Nucleophilic Addition Sequence

PDF (270 kb)
1414
Martín, R.; Romea, P.; Tey, C.; Urpí, F.; Vilarrasa, J.:
Simple and Efficient Preparation of Ketones from Morpholine Amides

PDF (215 kb)
1417
Ishihara, Jun; Miyakawa, Jun; Tsujimoto, Takashi; Murai, Akio:
Synthetic Study on Gymnodimine: Highly Stereoselective Construction of Substituted Tetrahydrofuran and Cyclohexene Moieties

PDF (241 kb)
1420
Bertrand, M. P.; Gastaldi, S.; Nouguier, R.:
Radical Cyclization of Dialkyldiallylammonium Salts. A Stereoselective Route to Pyrrolidines

PDF (231 kb)
1423
Craig, Donald; Jones, Philip S.; Rowlands, Gareth J.:
Synthesis of 2,5-Disubstituted 3-(Phenylsulfonyl)pyrrolidines via 5-Endo-Trig Cyclisation Reactions

PDF (274 kb)
1429
Knöbel, Andreas K. H.; Escher, Iris H.; Pfaltz, Andreas:
Enantioselective Copper-Catalyzed 1,4-Addition of Organozinc Reagents to Enones Using Chiral Oxazoline-Phosphite Ligands

PDF (240 kb)
1432
Moriarty, Robert M.; Tao, Anping; Wendler, Angelica; Prakash, Om; Liu, Kaiming; Gilardi, Richard:
Stereoisomers of a Simulant of the Nerve Agent Soman. Synthesis and Protein Conjugation

PDF (221 kb)
1435
Khan, M. Wahab; Kundu, Nitya G.:
A Highly Regio and Stereoselective Synthesis of (Z)-3-Aryl(alkyl)idene Isoindolin-1-ones via Palladium Catalyzed Annulation of Terminal Alkynes

PDF (244 kb)
1438
Vroman, Jeffrey A.; Khan, Iklas; Avery, Mitchell A.:
Conjugate Addition of Trimethylsilylmethyl Cuprates to Artemisinic Acid: Homologation and Subsequent Conversion to 9β-Modified Artemisinin Analogs

PDF (207 kb)
1441
Craig, D. C.; Edwards, G. L.; Muldoon, C. A.:
Synthesis of 2-Substituted Nitrogen Heterocycles Using para-Toluenesulfonyl Iodide in a Key Step

PDF (227 kb)
1444
Tomé, Augusto C.; Enes, Roger F.; Cavaleiro, José A. S.; Martarello, Laurent; Kirsch, Gilbert:
Carbazole-1,2-quinodimethane: Generation and Reactivity

PDF (197 kb)
1447
Kieburg, Christoffer; Dubber, Michael; Lindhorst, Thisbe K.:
A New Type of Carbohydrate Clustering: Synthesis of a Pentavalent Glycocluster Based on a Carbohydrate Core

HTML

PDF (209 kb)
1450
Itoh, Akichika; Masaki, Yukio:
Synthesis and Application of New Phenyl-Functionalized Zeolites as Protection Against Radical Bromination at the Benzylic Position

PDF (215 kb)
1453
Ariffin, Azhar; Blake, Alexander J.; Li, Wan-Sheung; Simpkins, Nigel S.:
Enantioselective Synthesis of Novel Enantiopure Phosphines via Reaction of a Tricarbonyl(η⁶-arene)chromium Complex with a Chiral Lithium Amide Base

PDF (244 kb)
1456
Kohmura, Yoshinori; Kawasaki, Ken-ichi; Katsuki, Tsutomu:
Benzylic and Allylic Amination

PDF (216 kb)
1459
Arai, Yoshitsugu; Masuda, Tsutomu; Masaki, Yukio:
Highly Stereoselective Aldol Reaction of Chiral 3-(p-Tolylsulfinyl)furfural with Silyl Ketene Acetal Catalyzed by Lanthanide Triflate

PDF (208 kb)
1462
Enders, Dieter; Peters, René; Lochtman, René; Runsink, Jan:
Enantioselective Synthesis of Planar Chiral ortho-Functionalised Ferrocenylketones

PDF (220 kb)
1465
Cha, Jin Soon; Kwon, Oh Oun; Kim, Jong Mi; Cho, Sung Dong:
Reexamination of Diisobutylaluminum Hydride as a Stereoselective Reducing Agent for Reduction of Cyclic Ketones to Thermodynamically More Stable Alcohols

PDF (163 kb)
1467
Mohar, Barbara; Kobe, Joe; Koomen, Gerrit-Jan:
Approach to Carbocyclic 4-Deoxypyrazofurin through Asymmetrisation of a meso-Norbornene Derivative

PDF (193 kb)
1469
Abelman, Matthew M.; Kado, Noriyuki; Overman, Larry E.; Sarkar, Achintya K.:
Synthesis of a Phenolic Analog of Aphidicolin. Diminished Stereoselection in Intramolecular 6-Exo Heck Reactions of Substrates Having a Hydrocarbon Tether

PDF (218 kb)
1472
Konno, Mitoshi; Nakae, Takahiko; Sakuyama, Shigeru; Imaki, Katsuhiro; Nakai, Hisao; Hamanaka, Nobuyuki:
An Efficient Method for the Synthesis of a Novel Leukotriene B₄ Receptor Antagonist, ONO-4057, via Michael Reaction of Dihydroresorcinol

PDF (162 kb)
1475
Couture, Axel; Deniau, Eric; Grandclaudon, Pierre; Lebrun, Stéphane:
A New Approach to the Synthesis of Aristolactams. Total Synthesis of Cepharanone A and B

PDF (298 kb)
1478
Jones, Iwan G.; Jones, Wyn; North, Michael:
Synthesis of Enantiomerically Pure, All Syn, Tetra and Pentasubstituted Cyclopentanes by the Desymmetrisation of Endo-Norborn-5-ene-2,3-Dicarboxylic Anhydrides

PDF (214 kb)

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