Synlett

Issue 02 · February 1998

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105
Ciufolini, Marco A.; Hermann, Cynthia Y. W.; Dong, Qing; Shimizu, Toshio; Swaminathan, Shankar; Xi, Ning:
Nitrogen Heterocycles From Furans: The Aza-Achmatowicz Reaction

PDF (249 kb)
115
Lu, Xiyan; Zhu, Guoxin; Wang, Zhong:
Enyne Coupling as the Potent Methodology for the Synthesis of Bioactive Molecules

PDF (223 kb)
letter
122
Bachi, Mario D.; Korshin, Edward E.:
Thiol-Oxygen Cooxidation of Monoterpenes. Synthesis of Endoperoxides Structurally Related to Antimalarial Yingzhaosu A

PDF (53 kb)
125
Schmidt, Ulja; Stiller, Regine; Brade, Helmut; Thiem, Joachim:
Formation of an Unusual Secondary Sedoheptulose Phosphate by Hexokinase-Mediated Phosphorylation

PDF (25 kb)
127
Gyergyói, K.; Tóth, A.; Bajza, I.; Lipták, A.:
Unusual sugars of the GPL-type antigen of Mycobacterium avium serovar 19. Stereoselective synthesis of methyl 6-deoxy-3-C-methyl-2,4-di-O-methyl-α-L-mannopyranoside and its C-4 epimer

PDF (57 kb)
129
Maiti, Soumen; Achari, Basudeb; Banerjee, Asish K.:
A Short Enantioselective Synthetic Route to (+)-Cassiol

PDF (26 kb)
131
Togo, Hideo; Katohgi, Masashi; Yokoyama, Masataka:
Direct Preparation of Saccharin Skeletons from N-Methyl(o-methyl)arenesulfonamides with (Diacetoxyiodo)arenes

PDF (36 kb)
133
Bissantz, Caterina; Bisel, Philippe; Schlewer, Gilbert:
C- or O-Alkylation of 5-Ethoxycarbonyl-2-Hydroxymethyl Pyridine with Arylmethane Derivatives

PDF (22 kb)
135
Moody, Christopher J.; Swann, Elizabeth:
N-H Insertion Reactions of Rhodium Carbenoids: A Modified Bischler Indole Synthesis

PDF (25 kb)
137
Yoda, Hidemi; Kawauchi, Miho; Takabe, Kunihiko:
Novel Asymmetric Synthesis of an Indolizidine Alkaloid, (+)-Lentiginosine Employing Highly Stereoselective Hydrogenation of α-Hydroxypyrrolidine

PDF (42 kb)
139
Cortes-Lopez, Gerardo; Gutierrez Tunstad, Linda M.:
Preparation of Mono-, Di- and Trisubstituted Resorcinol Macrocycles

PDF (31 kb)
141
Thiebes, Christoph; Thiebes, Christoph; Prakash, G. K. Surya; Petasis, Nicos A.; Olah, George A.:
Mild Preparation of Haloarenes by Ipso-Substitution of Arylboronic Acids with N-Halosuccinimides

PDF (31 kb)
143
Stüdemann, Thomas; Ibrahim-Ouali, Malika; Cahiez, Gérard; Knochel, Paul:
Stereoselective Nickel and Manganese Catalyzed Cyclizations of 5-Haloketones

PDF (41 kb)
145
Tietze, Lutz F.; Ferraccioli, Raffaella:
Efficient Synthesis of Aza-Heterocycles by a Domino Process using an Inter- and an Intramolecular Heck Reaction

PDF (27 kb)
147
Siro, Jorge G.; Martín, Justina; García-Navío, JoséL.; Remuiñan, Modesto J.; Vaquero, Juan J.:
Easy Microwave Assisted Deprotection of N-Boc Derivatives

PDF (30 kb)
149
Hale, Karl J.; Cai, Jiaqiang; Williams, Glyn:
Total Synthesis of 4-Epi-A83586C. Epimerisation in a Macrolactamisation Mediated by BOP and DMAP

PDF (131 kb)
153
Damour, D.; Barreau, M.; Fardin, V.; Dhaleine, F.; Vuilhorgne, M.; Mignani, S.:
1,3-Dipolar Cycloaddition Reactions of 4-Silacyclohex(hept)-2-en-1-one Derivatives: Synthesis of Novel Azasilabicyclic Compounds

PDF (84 kb)
157
Díaz, M. Teresa; Cobas, Agustín; Guitián, Enrique; Castedo, Luis:
Polar Control of the Regioselectivity of Hetaryne Cycloadditions. Synthesis of Ellipticine

PDF (33 kb)
159
Maier, Martin E.; Perez, Caroline:
Intramolecular Diels-Alder Reaction with an α-Methylene Lactone as Dienophile

PDF (30 kb)
161
Fürstner, Alois; Seidel, Günter:
Suzuki Reactions with B-Allyl-9-Borabicyclo[3.3.1]nonane (B-Allyl-9-BBN)

PDF (41 kb)
163
Charette, AndréB.; Chua, Peter:
A New Mild Method for the Cleavage of the Amide Bond: Conversion of Secondary and Tertiary Amides to Esters

PDF (54 kb)
166
Schürer, Stephan C.; Blechert, Siegfried:
Ruthenium-Catalyzed Yne-Ene Cross Metathesis Binding to Solid Support and Cleavage by Pd⁰-Catalysis

PDF (49 kb)
169
Stragies, Roland; Blechert, Siegfried:
Domino Metathesis - A Combined Ring Opening-, Ring Closing- and Cross Metathesis

PDF (36 kb)
171
Heckel, Alexander; Mross, Elmar; Jung, Karl-Heinz; Rademann, Jörg; Schmidt, Richard R.:
Oligosaccharide Synthesis on Controlled-Pore Glass as Solid Phase Material

PDF (49 kb)
174
Yanagisawa, Akira; Kikuchi, Tetsuo; Yamamoto, Hisashi:
Effects of Lithium Salts on the Enantioselectivity of Protonation of Enolates with Chiral Imide

PDF (66 kb)
177
Rubira, María-José; Pérez-Pérez, María-Jesús; Balzarini, Jan; Camarasa, María-José:
Synthesis of Phosphonate Analogues of 2-Deoxyribose-1-Phosphate

PDF (47 kb)
180
Stevens, Christian; Verbeke, Aart; De Kimpe, Norbert:
A Convenient Synthesis of Dialkyl [[2-(Bromomethyl)aziridin-1-yl]methyl]phosphonates, New Heterocyclic β-Azaphosphonates

PDF (33 kb)
183
Kubota, Yoshihiro; Nakada, Shigekuni; Sugi, Yoshihiro:
Palladium-Catalyzed Alkoxycarbonylation of Aryl p-Toluenesulfonate

PDF (83 kb)
186
Tozer, Matthew J.; Woolford, Alison J. A.; Linney, Ian D.:
A Convenient Synthesis of N-Alkyl-(E)-1-alkenesulfonamides

PDF (46 kb)
189
Blake, Alexander J.; Ebden, Mark R.; Fox, David N. A.; Li, Wan-Sheung; Simpkins, Nigel S.:
Diastereoselective and Enantioselective Substitution Reactions of an Isoindoline-Borane Complex

PDF (52 kb)
192
Rutjes, Floris P. J. T.; Kooistra, T. Martijn; Hiemstra, Henk; Schoemaker, Hans E.:
A Novel Transition Metal-Catalyzed Route to Functionalized Dihydropyrans and Tetrahydrooxepines

PDF (50 kb)
195
Hashem, Md Abul; Jung, Alexander; Ries, Monika; Kirschning, Andreas:
Iodine(III)-Initiated Bromoacetoxylation of Olefins

PDF (50 kb)
198
Zhou, Shao-Man; Yan, Yi-Long; Deng, Min-Zhi:
A Novel Stereocontrolled Synthesis of Cyclopropyl-Substituted α,β-Unsaturated Esters: Palladium Catalyzed Cross-coupling of Cyclopropylboronic Acids with Bromoacrylates

PDF (43 kb)
201
Gibson, Christoph; Buck, Thomas; Walker, Martina; Brückner, Reinhard:
Approaching the C₃₃-C₃₈ Fragments of Amphotericin B and Nystatin by a Retro-[1,4]-Brook Rearrangement and the Stereoselective Manipulation of the Resulting Allylsilane

PDF (102 kb)
206
David, Marc; Dhimane, Hamid; Vanucci-Bacqué, Corinne; Lhommet, Gérard:
Stereocontrolled Addition of π-type Nucleophiles to a Bicyclic N-Acyliminium Ion. New Access to trans-2,6-Disubstituted Piperidine Substructures

PDF (44 kb)
209
Bartoli, Giuseppe; Bosco, Marcella; Marcantoni, Enrico; Sambri, Letizia; Torregiani, Elisabetta:
A Mild, Efficient, and Selective Method for the Desilylation of More Common Trialkylsilyl Ethers by Cerium(III) Chloride Heptahydrate and Sodium Iodide in Acetonitrile

PDF (59 kb)

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Synlett

Nitrogen Heterocycles From Furans: The Aza-Achmatowicz Reaction

Enyne Coupling as the Potent Methodology for the Synthesis of Bioactive Molecules

Thiol-Oxygen Cooxidation of Monoterpenes. Synthesis of Endoperoxides Structurally Related to Antimalarial Yingzhaosu A

Formation of an Unusual Secondary Sedoheptulose Phosphate by Hexokinase-Mediated Phosphorylation

Unusual sugars of the GPL-type antigen of Mycobacterium avium serovar 19. Stereoselective synthesis of methyl 6-deoxy-3-C-methyl-2,4-di-O-methyl-α-L-mannopyranoside and its C-4 epimer

A Short Enantioselective Synthetic Route to (+)-Cassiol

Direct Preparation of Saccharin Skeletons from N-Methyl(o-methyl)arenesulfonamides with (Diacetoxyiodo)arenes

C- or O-Alkylation of 5-Ethoxycarbonyl-2-Hydroxymethyl Pyridine with Arylmethane Derivatives

N-H Insertion Reactions of Rhodium Carbenoids: A Modified Bischler Indole Synthesis

Novel Asymmetric Synthesis of an Indolizidine Alkaloid, (+)-Lentiginosine Employing Highly Stereoselective Hydrogenation of α-Hydroxypyrrolidine

Preparation of Mono-, Di- and Trisubstituted Resorcinol Macrocycles

Mild Preparation of Haloarenes by Ipso-Substitution of Arylboronic Acids with N-Halosuccinimides

Stereoselective Nickel and Manganese Catalyzed Cyclizations of 5-Haloketones

Efficient Synthesis of Aza-Heterocycles by a Domino Process using an Inter- and an Intramolecular Heck Reaction

Easy Microwave Assisted Deprotection of N-Boc Derivatives

Total Synthesis of 4-Epi-A83586C. Epimerisation in a Macrolactamisation Mediated by BOP and DMAP

1,3-Dipolar Cycloaddition Reactions of 4-Silacyclohex(hept)-2-en-1-one Derivatives: Synthesis of Novel Azasilabicyclic Compounds

Polar Control of the Regioselectivity of Hetaryne Cycloadditions. Synthesis of Ellipticine

Intramolecular Diels-Alder Reaction with an α-Methylene Lactone as Dienophile

Suzuki Reactions with B-Allyl-9-Borabicyclo[3.3.1]nonane (B-Allyl-9-BBN)

A New Mild Method for the Cleavage of the Amide Bond: Conversion of Secondary and Tertiary Amides to Esters

Ruthenium-Catalyzed Yne-Ene Cross Metathesis Binding to Solid Support and Cleavage by Pd⁰-Catalysis

Domino Metathesis - A Combined Ring Opening-, Ring Closing- and Cross Metathesis

Oligosaccharide Synthesis on Controlled-Pore Glass as Solid Phase Material

Effects of Lithium Salts on the Enantioselectivity of Protonation of Enolates with Chiral Imide

Synthesis of Phosphonate Analogues of 2-Deoxyribose-1-Phosphate

A Convenient Synthesis of Dialkyl [[2-(Bromomethyl)aziridin-1-yl]methyl]phosphonates, New Heterocyclic β-Azaphosphonates

Palladium-Catalyzed Alkoxycarbonylation of Aryl p-Toluenesulfonate

A Convenient Synthesis of N-Alkyl-(E)-1-alkenesulfonamides

Diastereoselective and Enantioselective Substitution Reactions of an Isoindoline-Borane Complex

A Novel Transition Metal-Catalyzed Route to Functionalized Dihydropyrans and Tetrahydrooxepines

Iodine(III)-Initiated Bromoacetoxylation of Olefins

A Novel Stereocontrolled Synthesis of Cyclopropyl-Substituted α,β-Unsaturated Esters: Palladium Catalyzed Cross-coupling of Cyclopropylboronic Acids with Bromoacrylates

Approaching the C₃₃-C₃₈ Fragments of Amphotericin B and Nystatin by a Retro-[1,4]-Brook Rearrangement and the Stereoselective Manipulation of the Resulting Allylsilane

Stereocontrolled Addition of π-type Nucleophiles to a Bicyclic N-Acyliminium Ion. New Access to trans-2,6-Disubstituted Piperidine Substructures

A Mild, Efficient, and Selective Method for the Desilylation of More Common Trialkylsilyl Ethers by Cerium(III) Chloride Heptahydrate and Sodium Iodide in Acetonitrile