Synfacts

Issue 05 · May 2013

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Synform
A52
SYNFORM ISSUE 2013/05
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Synthesis of Natural Products and Potential Drugs
z461
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0461
Total Synthesis of (±)-Goniomitine
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0462
Synthesis of (–)-Huperzine A

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0463
Commercial Manufacture of Halaven^®
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0464
Synthesis of a Dual NK-1/Serotonin Receptor Antagonist

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0465
Total Syntheses of Xanthofulvin and Vinaxanthone

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0466
Synthesis of Pumilaside Aglycon

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0467
Synthesis of (−)-Trichodermatide A

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0468
Synthesis of an MDM2 Antagonist

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0469
Synthesis of (–)-Galanthamine

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0470
Synthesis of Clinprost

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0471
Total Synthesis of Cladoniamide G

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0472
Total Synthesis of Teurilene

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0473
Synthesis of LY2784544

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0474
Total Synthesis of (–)-Acutumine and (–)-Dechloroacutumine

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Synthesis of Heterocycles
z475
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0475
Palladium-Catalyzed Synthesis of 3-Alkynylindoles

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0476
Synthesis of Tetrahydroquinazolinediones and Dihydropyrido[2,3-d]pyrimidines

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0477
Copper-Catalyzed Synthesis of Furans via (2-Furyl)Carbene Complexes

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0478
Interconversion of Benzodiazepinediones into Oxazoloquinolinones

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0479
Gold(I)-Catalyzed Synthesis of Pyrrolo[1,2-a]indoles

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0480
FeBr₃-Catalyzed C–H Activation Route to Indazoles and Pyrazoles

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0481
Phenanthridine Derivatives from Intramolecular Diels–Alder Reaction

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0482
Rhodium-Catalyzed Synthesis of Phthalides from Benzoic Acids

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0483
De Novo Synthesis of 2-Pyridones

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0484
Two-Step Synthesis of 2H-Indazoles via C–H Activation of Azobenzenes

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0485
One-Pot Synthesis of Benzo[4,5]imidazo[2,1-a]isoquinolines

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0486
Zinc Triflate Catalyzed Double Michael Addition Route to Enantioenriched Chromans

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0487
Synthesis of Pyrroles and 2H-Pyrrolo[3,4-c]quinolines

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0488
Synthesis of 2-Aryl-2H-indazoles Using Silver Catalysis

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0489
A Cloke–Wilson Rearrangement Approach to Fused Bromofurans

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Synthesis of Materials and Unnatural Products
z491
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0491
Functional Phthalaldehyde–Benzaldehyde Copolymers

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0492
A Route to Highly Substituted Phenanthrenes and Naphthalenes

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0493
Bottom-up Synthesis of Nickel Bis(dithiolene) Complex Nanosheet

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0494
Cross-Coupling at C–S Bonds

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0495
Cross-Coupling at C–S Bonds

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0496
Migration Insertion Polymerization: A Route to Metal-Containing Polymers

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0497
[2+2+2] Reaction Leads the Way to a C₇₀ Buckybowl

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0498
Synthesis of a Bolaamphiphilic Sexithiophene

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0499
Synthesis of [5]- and [7]Phenacenes

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0500
Negative Photochromism of 1,1′-Binaphthyl-Bridged Imidazole Dimer

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0501
Naphthalene Derivatives by an Iron-Catalyzed Benzannulation

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0502
A Macroinimer Approach Affords Hyperbranched Block and Brush Copolymers

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z503
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0503
Synthesis of Aminoindanes via a Novel C−H Activation–[3+2]-Annulation Strategy
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0504
Copper-Catalyzed Asymmetric Alkynylation of Ketoimines

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0505
Copper-Catalyzed Asymmetric Synthesis of Piperidines by a [6+3] Cycloaddition
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0506
Synthesis of α-Chiral Succinimides by Iridium-Catalyzed Hydrogenation

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0507
Stereospecific Synthesis of β-Amido-α-diazoesters

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0508
Palladium-Catalyzed Asymmetric Cycloaddition of Trimethylenemethanes

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0509
Asymmetric Allylic Alkylation for the Synthesis of 3,3-Disubstituted Oxindoles

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0510
Rhodium-Catalyzed Enantioselective Hydrogenation of Oxime Acetates

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0511
Enantioselective Synthesis of cis- and trans-Thiazolidines

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0512
Iridium-Catalyzed Enantio- and Diastereoselective Allylation of Azlactones

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0513
Iridium-Catalyzed Enantioselective Heterohydroarylation of Bicycloalkenes

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0514
Palladium-Catalyzed Allylic Alkylations of 3-Substituted Indoles

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0515
Enantioselective Synthesis of 1,5-Dienes via Copper-Catalyzed Allyl–Allyl Coupling

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0516
Chiral Bidentate Phosphite Ligands in Rhodium-Catalyzed Hydrogenation

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0517
Asymmetric Catalytic Addition of Allylic Cyanides to Aldehydes

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0518
Copper-Catalyzed Asymmetric Synthesis of Mixed 3,3′-Bisindoles

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0519
Mechanistic Insights – A Chiral Organocatalyst Meets an Achiral Iridium Catalyst

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0520
Palladium-Catalyzed Diamination of Alkyl Dienes

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0521
Nitrogen-Containing Heterocycle Synthesis Initiated by Rh(III)-Catalyzed C−H Activation

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0522
Copper-Catalyzed Enantioselective Intramolecular O–H Bond Insertion

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0523
Iridium-Catalyzed Enantioselective Decarboxylative Allylic Etherification

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0524
Ruthenium-Catalyzed [3+2] Cycloaddition via Allenylidene Intermediates

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0525
Ruthenium-Catalyzed Cyclopropanation of Vinylcarbamates

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0526
Copper-Catalyzed Enantioselective Fluorination of Keto Esters

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0527
Au(I)–Chiral Phosphoric Acid Catalyzed Multi-Component Spiroketal Synthesis

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0528
Copper-Catalyzed Asymmetric Conjugate Addition to Enones

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0529
Copper-Catalyzed Reactions of α-Alkylidene β-Keto Imides

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0530
Iridium-Catalyzed Asymmetric Hydrogenation of Isoquinolinium Salts

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0531
2-Enoylpyridine N-Oxides in Asymmetric Mukaiyama–Michael Additions

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0532
Rhodium-Catalyzed Enantioselective C–H Insertion of Sulfonyldiazoacetates

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Metal-Mediated Synthesis
z533
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0533
Heterocycle Synthesis by a One-Pot Oxidative C(sp³)–N Coupling Reaction

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0534
Deprotonation and Alkylation of 2-Boryl Allylic Sulfones

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0535
Catalytic Semireduction of Alkynes to Alkenes
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0536
Rhodium-Catalyzed Synthesis of Chiral Oxazolidinones

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0537
Copper-Mediated Oxidative Coupling of 1,3,4-Oxadiazoles with Polyfluoroarenes

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0538
Titanium–Magnesium-Mediated Enantioselective Alkylation of Aldehydes

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0539
Formation of Carbazoles by the Reaction of Arynes with Nitrosoarenes

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0540
Triethylborane–Oxygen-Mediated Hydrostannylation of Propargylic Alcohols

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0541
Silver-Catalyzed Hydrotrifluoromethylation of Unactivated Alkenes

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0542
Nickel-Catalyzed (sp³)–(sp³) Cross-Coupling to Yield Fatty Acids

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0543
Aryl Ether Synthesis via Directed C–H-Activating Alkoxylation with Decarboxylation

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0544
Silver-Mediated Trifluoromethylation–Iodination of Arynes

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0545
Reactions of Difluorocarbene with Benzyl- and Alkylzinc Reagents

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0546
Copper-Promoted Decarboxylative Direct C3-Acylation of N-Substituted Indoles

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0547
Copper-Catalyzed Trifluoromethylation of Aryl- and Vinylboronic Acids

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Organo- and Biocatalysis
z549
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0549
Organocatalytic C–H Bond Arylation of Aldehydes to Bis-heteroaryl Ketones

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0550
Highly Enantioselective Kita Oxidative Spirolactonization

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0551
Kinetic Resolution via Brønsted Acid Catalyzed Lactonization

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0552
Phase-Transfer-Catalyzed Asymmetric Synthesis of Tetrasubstituted Allenes

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0553
Phase-Transfer-Catalyzed Asymmetric Cyanation of Alkylidenemalonates

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0554
Pyridines via Synergistic Copper–Iminium Catalysis

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0555
Enantioselective Allylation of Imides with Allylboronic Acid Pinacol Esters

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0556
Lewis Base Catalyzed Double Aldol Reaction

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0557
Organocatalytic S_N2 Transetherification

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0558
Asymmetric Organocatalytic Synthesis of Tetrasubstituted Chiral Biaryl Compounds

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0559
A By-Product as a Lewis Base Catalyst for Conjugated Reductions

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Polymer-Supported Synthesis
z561
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0561
Reduction of N-Heterocycles with a Raney-Nickel-Type Catalyst

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0562
One-Pot Epoxidation of Alkenes over CuO/Al₂O₃Using Cumene and Oxygen

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0563
Hydrogenation of Alkenes Using Copper Nanoparticles Supported on Diamond
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0564
Synthesis of Benzimidazoles Using Silica-Supported CuO Nanoparticles

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0565
Cross-Coupling of Acyl Chlorides with Triarylbismuths Using MCM-41-2N-Pd(OAc)₂

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0566
Synthesis of 2-Oxo-2,5-Dihydropyrroles with TiO₂ Nanopowder

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0567
Oxirane Ring Opening with NaCN Using SiO₂-PEG-ImBr

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0568
A MNP-Supported Thiourea Catalyst for Asymmetric Diels–Alder Reactions

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0569
Asymmetric Alkylation of N-Phosphinylimines Using Supported l-Prolinol

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0570
Pd@Al₂O₃-Cellulose for Suzuki–Miyaura Cross-Couplings

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0571
Stereospecific Allylic Substitution by in situ Generated Palladium Nanoparticles

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0572
Passerini Reaction with Fe₃O₄ Nanoparticles Supported TEMPO

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0573
Nano CuO-Catalyzed Ullmann-Type Coupling at Ambient Temperature

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0574
Solid-Phase Synthesis of (S)-(+)-Clopidogrel

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Erratum
0575
Ru-Catalyzed trans Hydrogenation of Alkynes

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0575
Rhodium-Catalyzed Asymmetric [2+2+2] Cycloaddition

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0575
Carbocation-Induced Electrophilic Cyclization of Ynamides

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