Synfacts

Issue 02 · February 2017

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SYNFORM ISSUE 2017/02
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Synthesis of Natural Products and Potential Drugs
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Divergent Syntheses of Aflavazole and 14-Hydroxyaflavinine

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Synthesis of MK-8666

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Total Synthesis of a Ladderane Phospholipid
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Total Synthesis of (–)-Nakadomarin A

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Synthesis of BMS-741672
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0120
Synthesis of (–)-Cycloclavine

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0121
Synthesis of Epothilone D

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0122
Synthesis of Verubecestat

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Synthesis of a TRPV3 Antagonist

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0124
Synthesis of (+)-Haplophytine

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Synthesis of (±)-Berkeleyone A

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0126
Asymmetric Synthesis of an 11β-HSD-1 Inhibitor

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Synthesis of Heterocycles
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0127
Palladium-Catalyzed Synthesis of Six- and Seven-Membered-Ring Heterocycles

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0128
Enantioselective Organocatalytic Synthesis of Benzo-Fused Acetals

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0129
Palladium-Catalyzed Carbonylation of Aliphatic Amines To Form β-Lactams

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0130
Stereodivergent Diels–Alder Route to Bicyclic Lactones

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0131
Lewis-Acid-Mediated Multistep Synthesis of (–)-Mersicarpine

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0132
Direct Nickel-Catalyzed Synthesis of Oxaborins from Benzofurans

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0133
Palladium-Catalyzed Synthesis of Cyclopropyl-Fused Azacycles

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0134
Synthesis of Pyrrolopyridinones by the Ugi Reaction

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0135
Synthesis of Acylated Benzimidazoles with Copper Catalysts

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0136
Synthesis of 3-Cyano-1H-indolo-2′-deoxy-ribonucleosides

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0137
Synthesis of Polyhydroxyindolizidines from Carbohydrates

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0138
Nickel-Catalyzed Trifluoromethylation of Electron-Rich Heteroarenes

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0139
Synthesis of 3,4-Dihydroquinazolinones from 2-Aminobenzaldehydes

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0140
Synthesis of 6-Phosphorylated Phenanthridines

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0141
Synthesis of Pyrroloquinolinones from Donor–Acceptor Cyclopropanes

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Synthesis of Materials and Unnatural Products
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0143
Electrochromism of Porous Network Thin Films

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0144
Nonplanar Polycyclic Aromatic Hydrocarbons

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0145
Toward Automated Oligo[n]rotaxanes
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0146
Photoredox Activation of SF₆ for Fluorination

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0147
A Facile Approach to DTT

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0148
A Negotiation between Different Nucleophiles in S_NAr Reactions

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0149
From 1,4-Dibromo-bis-alkynes to Heptacyclic Heteroacenes in One Step

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0150
Thiophene-Bridged Carbazole-Based Diporphyrin

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0151
Aryl(triethyl)silanes for Biaryl and Teraryl Synthesis by Copper(II) Catalysis

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0152
Unsymmetric Dibenzopentalenes

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0153
Bis-Lactam as Acceptor

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0154
Azaanthracenes via Inverse Electron-Demand Diels–Alder Reaction

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0155
Enantioselective α-Arylation of α-Fluoroketones

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0156
Enantioselective Copper-Catalyzed Cyanotrifluoromethylation

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0157
Enantioselective Rhodium-Catalyzed α-Allylation of Aldehydes
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0158
1,3-Dipolar Cycloaddition of Alkenyl Arenes with Azomethine Ylides

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0159
Enantioselective Coupling of Diazoalkanes with Terminal Alkynes
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0160
Catalytic Asymmetric α-Vinylation of β-Keto Amides/Esters

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0161
Enantioselective Desymmetrization of Cyclohexadienones

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0162
Iridium-Catalyzed Asymmetric Hydrogenation of Alkenoic Acids

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0163
Palladium-Catalyzed Asymmetric Benzylic C–H Arylation of Amines

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0164
Cobalt-Catalyzed Asymmetric Hydrosilylation of Alkynes

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0165
Molybdenum-Catalyzed Deoxygenation of Epoxides

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0166
Asymmetric Hydrogenation of Lactones through Dynamic Kinetic Resolution

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0167
Iridium-Catalyzed Asymmetric Allylic Alkylation of β-Keto Esters

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0168
Ligand Effect on Diastereoselectivity in Suzuki–Miyaura Coupling

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0169
Copper-Catalyzed Propargylation of Cyclic Aldimines

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0170
Enantioenriched Borylalkanes by Copper-Catalyzed Hydroallylation

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0171
Regio- and Enantioselective Palladium-Catalyzed Hydroesterification

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0172
Asymmetric Cross-Coupling with Organoaluminum Reagents

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0173
Iridium-Catalyzed Stereoselective Hydrogenation of α-Alkyl β-Keto Esters

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0174
Catalytic Asymmetric Cycloisomerization and Parallel Kinetic Resolution

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0175
CF₃-Substituted Pyrrolidines through Cycloaddition of Azomethine Ylides

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0176
Palladium-Catalyzed Decarboxylative Asymmetric [4+2] Cycloaddition

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0177
Rhodium-Catalyzed Asymmetric Hydroacylation of Trisubstituted Alkenes

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0178
Samarium-Catalyzed Asymmetric Synthesis of Aminocyclopropanes

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0179
Rhodium-Catalyzed Enantioselective Cascade Cyclopropanation

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0180
Palladium-Catalyzed Asymmetric Alkynylation of Axially Chiral Biaryls

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0181
Enantioselective Synthesis of α-Mercapto-β-Amino Esters

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0182
Enantioselective Narasaka–Heck Cyclization

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Metal-Mediated Synthesis
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0183
Direct Primary Amination and Hydroxylation of (Hetero)arylmetals

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0184
Synthesis of Tertiary Aminocyclopropanes

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0185
Cross-Coupling of O-Based Electrophiles

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0186
Synthesis of 3-Aminoaryne Precursors

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0187
Synthesis of β-Alkoxy- and β-Aryloxyacrylates

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0188
Directed Arylation and Alkenylation of C(sp³)–H Bonds

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0189
Synthesis of Aryl Amines by Metal-Free C–N Coupling

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0190
N-Arylation of 2-Imidazolines

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0191
Radical-Type Cross-Coupling Reactions

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0192
Suzuki–Miyaura Cross-Coupling of Triazolopyrimidines

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0193
Multicomponent Synthesis of β-Hydroxy- and β-Aminocarbonyl Compounds

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0194
Borylative Cyclization for the Formation of Benzofurans and Benzothiophenes

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0195
Nickel-Catalyzed CO₂ Rearrangement

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0196
Selective Addition of Alkyl Grignard Reagents to Pyridine-N-oxides

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0197
Silaboration of Oxetanes and Unactivated Epoxides

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Organo- and Biocatalysis
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0199
Asymmetric Enzymatic Carbon–Silicon Bond Formation
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0200
Phosphoric Acid Catalyzed Asymmetric Synthesis of SPINOL Derivatives

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0201
Catalytic Enantioselective Vinylogous Pinacol Rearrangement

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0202
Construction of Adjacent Quaternary Stereocenters

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0203
Annulation of Donor–Acceptor Cyclobutanes with N-Heterocyclic Carbenes

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0204
Photocatalytic Hydrodefluorination Promoted by π-Hole–π Interactions

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0205
Hydrogen-Bonding Catalysis with Sulfonium Salts

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0206
Catalytic Asymmetric Synthesis of C₂-Symmetric Secondary Amines

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0207
Transaminase-Catalyzed Enantioselective Synthesis of Piperidines

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0208
ortho-Selective Chlorination of Anilines

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Polymer-Supported Synthesis
z0209
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PDF (516 kb)
0209
Alcohol Oxidation with Ionic Liquid Supported IBX Generated in situ

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0210
Reduction of 4-Nitrophenol with Porphyrin Polymer Supported Gold

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0211
Azide–Alkyne Cycloaddition with a Melanin-Supported Copper(I) Catalyst
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0212
MOF-Catalyzed N-Arylation of Heterocycles with Aryl Iodides

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0213
Knoevenagel Condensation Catalyzed by Nickel Ferrite Nanoparticles

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PDF (118 kb)
0214
Asymmetric Ethylation of Aryl Aldehydes with a PEG-Supported Chiral Ligand

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PDF (134 kb)
0215
A Cr(salen)-Based Metal–Organic Framework as a Chiral Lewis Acid Catalyst

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0216
Direct Oxidative C(sp³)–H/N–H Coupling on a Copper/Metal–Organic Framework

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0217
Preparation of β-Enaminones with Copper(II) Oxide Nanoparticles

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0218
C–C Bond Formation by Using a Supported Palladium–Schiff Base Complex

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0219
Synthesis of Propargylamines on Thiolate-Protected Gold Nanoclusters

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0220
Oxidation and Reduction of Olefins on Copper/Metal–Organic Framework Catalysts

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0221
Chemoselective Hydrogenation of Nitroarenes on Cobalt/Silicon Carbonitride

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0222
Cerum Oxide Catalyzed Oxidative Coupling of Alcohols with Amines to Form Imines

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0223
Oxidative Amidation with Heteropolyanion-Based Ionic Liquids

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0224
Synthesis of Pyrazolo[3,4-b]pyridines on Cobalt Ferrite/Sulfonated Graphene Oxide

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