Synlett

Issue 01 · January 1998

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1
Trost, Barry M.; Krische, Michael J.:
Transition Metal Catalyzed Cycloisomerizations

PDF (383 kb)
17
Scarpati, Rachele; Iesce, M. Rosaria; Cermola, Flavio; Guitto, Antonio:
1-Alkoxy-2,3,7-trioxabicyclo[2.2.1]hept-5-enes: Bicyclic Monoperoxy Ortho Esters as Useful Synthons for Multifunctional Compounds

PDF (404 kb)
letter
26
Blakemore, Paul R.; Cole, William J.; Kocieński, Philip J.; Morley, Andrew:
A Stereoselective Synthesis of trans-1,2-Disubstituted Alkenes Based on the Condensation of Aldehydes with Metallated 1-Phenyl-1H-tetrazol-5-yl Sulfones

PDF (63 kb)
29
Yu, Biao; Zhang, Jianbo; Lu, Shoufu; Hui, Yongzheng:
A Novel and Efficient Deprotection of the Allyl Group at the Anomeric Oxygen of Carbohydrates

PDF (38 kb)
31
Boukouvalas, John; Lachance, Nicolas:
A Mild, Efficient and General Method for the Synthesis of Trialkylsilyl (Z)-4-Oxo-2-alkenoates and γ-Hydroxybutenolides

PDF (41 kb)
33
Duffault, Jean-Marc:
Strategy for a Seven-Membered Ring Closure with Bicyclic Framework

PDF (41 kb)
35
Aoyama, Toyohiko; Sonoda, Naoko; Yamauchi, Mariko; Toriyama, Kyoko; Anzai, Masahiro; Ando, Akira; Shioiri, Takayuki:
Chemical Manganese Dioxide (CMD), an Efficient Activated Manganese Dioxide. Application to Oxidation of Benzylic and Allylic Alcohols

PDF (33 kb)
37
Yokoyama, Yasuo; Mochida, Kunio:
Stereoselective Syntheses of 2-Fluoro-2-methyl-3-hydroxypropionamides by Use of a Germyl Anion Species

PDF (47 kb)
39
Jang, Doo Ok; Cho, Dae Hyan; Barton, Derek H. R.:
Radical Deoxygenation of Alcohols via Their S-Methyl Dithiocarbonate Derivatives with Di-n-butylphosphine Oxide as Hydrogen Atom Donor

PDF (42 kb)
41
Beier, Christian; Schaumann, Ernst; Adiwidjaja, Gunadi:
The First Asymmetric Synthesis of (1R,1′S)-1-[1′-(Benzyloxycarbonyl-methylamino)-2′-phenylethyl]oxirane: a Promising Building Block for the Synthesis of Peptide Mimics

PDF (37 kb)
43
Enders, Dieter; Müller, Peter; Klein, Daniela:
Diastereo- and Enantioselective Synthesis of syn-2,3-Disubstituted 1,4-Diketones via Oxidative Coupling of Metalated Hydrazones

PDF (44 kb)
45
Achiwa, Issei; Yamazaki, Akira; Achiwa, Kazuo:
Synthesis of a Novel Type of Chiral Bisphosphine Ligand (NORPHOS-7-NEt₂) with an Amino Group for Neighboring Participation in Asymmetric Allylic Alkylation

PDF (36 kb)
47
Prabhu, Kandikere R.; Sivanand, P. S.; Chandrsekaran, Srinivasan:
A New Methodology for the Reductive Cyclization of ω-Azido Carbonyl Compounds Mediated by Tetrathiomolybdate: Application to an Efficient Synthesis of Pyrrolo[2,1-c][1,4]benzodiazepines

PDF (23 kb)
49
Constantieux, Thierry; Brunel, Jean-Michel; Labande, Agnès; Buono, Gérard:
Enantioselective Palladium Catalyzed Allylic Amination Using New Chiral Pyridine-Phosphine Ligands

PDF (47 kb)
51
Kajiro, Hiroshi; Mitamura, Shu-ichi; Mori, Atsunori; Hiyama, Tamejiro:
A Practical Synthesis of (1S,2R)-1-Amino-2-indanol, a Key Component of HIV Protease Inhibitor, Indinavir

PDF (41 kb)
53
Gläser, Björn; Kunz, Horst:
Enantioselective Allylic Substitution Using a Novel (Phosphino-α-d-glucopyrano-oxazoline)palladium Catalyst

PDF (49 kb)
55
Craig, Donald; McCague, Raymond; Potter, Gerard A.; Williams, Meredith R. V.:
1,4-Bis(arylsulfonyl)-1,2,3,4-tetrahydropyridines in Synthesis. Highly Regio- and Stereoselective S_N1′ and Alkylation Reactions

PDF (68 kb)
58
Craig, Donald; McCague, Raymond; Potter, Gerard A.; Williams, Meredith R. V.:
1,4-Bis(arylsulfonyl)-1,2,3,4-tetrahydropyridines in Synthesis. Intramolecular Alkylation Reactions and Stereoselective Synthesis of Anti-2,6-Disubstituted Piperidines

PDF (61 kb)
61
Eastham, Stephen A.; Herbert, John; Painter, James E.; Patel, Prakash; Quayle, Peter:
Modified Dötz Benzannulation Reactions Part 2: β-Chlorovinyl Carbene Complexes in Organic Synthesis

PDF (63 kb)
64
Faust, Rüdiger; Göbelt, Bernd; Weber, Christian:
Triisopropylsilyl Protected Hexa-1,5-diyne-3,4-dione: A Convenient Precursor to 2,3-Dialkynyl 1,4-Diazabutadienes

PDF (42 kb)
67
Nishii, Yoshinori; Wakasugi, Kazunori; Tanabe, Yoo:
Dimethylation and Hydrodechlorination of gem-Dichlorocyclopropanes with Grignard Reagents Promoted by Fe(III) or Co(II) Catalyst

PDF (60 kb)
70
Gil, S.; Lázaro, M. A.; Parra, M.; Breitmaier, E.; Mestres, R.:
γ-Alkylation of Unsaturated Carboxylic Acids. Stereoselective Synthesis of 2Z- and 2E,6E-3-Methyldeca-2,6-dienoic Acids from 3-Methylbut-2-enoic Acid Through Consecutive Ireland Claisen and Cope Rearrangements

PDF (34 kb)
73
Cavalier, Jean-François; Fotiadu, Frédéric; Verger, Robert; Buono, Gérard:
New Highly Diastereoselective Synthesis of Phosphoramidates. A Route to Chiral Methyl p-Nitrophenyl Alkylphosphonates

PDF (54 kb)
76
Nishizawa, Mugio; Takao, Hiroko; Iwamoto, Yoshihiro; Yamada, Hidetoshi; Imagawa, Hiroshi:
Synthesis of a Bicyclic Cation Related to Sterol Biosynthesis and Its Chemical Destiny, Part I

PDF (49 kb)
79
Nishizawa, Mugio; Takao, Hiroko; Iwamoto, Yoshihiro; Yamada, Hidetoshi; Imagawa, Hiroshi:
Synthesis of a Bicyclic Cation Related to Sterol Biosynthesis and Its Chemical Destiny, Part II

PDF (32 kb)
81
Jégou, Anne; Pacheco, Carole; Veyrières, Alain:
Stereoselective Synthesis of α-C-Glycopyranosyl Isoprenoid Compounds

PDF (58 kb)
84
Fukase, Koichi; Nakai, Yoshihiko; Kanoh, Takeshi; Kusumoto, Shoichi:
Mild but Efficient Methods for Stereoselective Glycosylation with Thioglycosides: Activation by [N-Phenylselenophthalimide-Mg(ClO₄)₂] and [PhIO-Mg(ClO₄)₂]

PDF (46 kb)
87
Mandal, Ashis B.; Delgado, Francisco; Tamariz, Joaquín:
New Synthesis of Carbazoles from Novel exo-2-Oxazolidinone Dienes

PDF (52 kb)
90
Giovannini, Riccardo; Petrini, Marino:
Synthesis and Radical Cyclization of 2-Allylamino-3-chloropropylphenyl Sulfones to 2,4-Disubstituted Pyrrolidines

PDF (44 kb)
93
Huang, Yao-Zeng; Mo, Xue-Sheng:
The Generation of Highly Functionalized Organometallics via Organotellurides and The Stereospecific Preparation of N-Isobutyl 6-Hydroxyl-(2E,4Z)-hexadienamide Derivatives

PDF (47 kb)
96
Schwan, Adrian L.; Refvik, Mitchell D.:
The Preparation of (E)-1-Alkenylthiosilanes by the Reduction and Silicon Capture of 1-Alkenesulfenate Anions

PDF (31 kb)
99
Boßhammer, Stephan; Gais, Hans-Joachim:
Stereoselective Synthesis of Allylic Sulfoximines from S-(Chloromethyl)-N-methyl-S-phenylsulfoximine and Alkenyl Cuprates

PDF (37 kb)
102
Aitken, R. Alan; Thomas, Andrew W.:
Behaviour of Dioxolanones as Chiral Acyl Anion Equivalents

PDF (42 kb)

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Synlett

Transition Metal Catalyzed Cycloisomerizations

1-Alkoxy-2,3,7-trioxabicyclo[2.2.1]hept-5-enes: Bicyclic Monoperoxy Ortho Esters as Useful Synthons for Multifunctional Compounds

A Stereoselective Synthesis of trans-1,2-Disubstituted Alkenes Based on the Condensation of Aldehydes with Metallated 1-Phenyl-1H-tetrazol-5-yl Sulfones

A Novel and Efficient Deprotection of the Allyl Group at the Anomeric Oxygen of Carbohydrates

A Mild, Efficient and General Method for the Synthesis of Trialkylsilyl (Z)-4-Oxo-2-alkenoates and γ-Hydroxybutenolides

Strategy for a Seven-Membered Ring Closure with Bicyclic Framework

Chemical Manganese Dioxide (CMD), an Efficient Activated Manganese Dioxide. Application to Oxidation of Benzylic and Allylic Alcohols

Stereoselective Syntheses of 2-Fluoro-2-methyl-3-hydroxypropionamides by Use of a Germyl Anion Species

Radical Deoxygenation of Alcohols via Their S-Methyl Dithiocarbonate Derivatives with Di-n-butylphosphine Oxide as Hydrogen Atom Donor

The First Asymmetric Synthesis of (1R,1′S)-1-[1′-(Benzyloxycarbonyl-methylamino)-2′-phenylethyl]oxirane: a Promising Building Block for the Synthesis of Peptide Mimics

Diastereo- and Enantioselective Synthesis of syn-2,3-Disubstituted 1,4-Diketones via Oxidative Coupling of Metalated Hydrazones

Synthesis of a Novel Type of Chiral Bisphosphine Ligand (NORPHOS-7-NEt₂) with an Amino Group for Neighboring Participation in Asymmetric Allylic Alkylation

A New Methodology for the Reductive Cyclization of ω-Azido Carbonyl Compounds Mediated by Tetrathiomolybdate: Application to an Efficient Synthesis of Pyrrolo[2,1-c][1,4]benzodiazepines

Enantioselective Palladium Catalyzed Allylic Amination Using New Chiral Pyridine-Phosphine Ligands

A Practical Synthesis of (1S,2R)-1-Amino-2-indanol, a Key Component of HIV Protease Inhibitor, Indinavir

Enantioselective Allylic Substitution Using a Novel (Phosphino-α-d-glucopyrano-oxazoline)palladium Catalyst

1,4-Bis(arylsulfonyl)-1,2,3,4-tetrahydropyridines in Synthesis. Highly Regio- and Stereoselective S_N1′ and Alkylation Reactions

1,4-Bis(arylsulfonyl)-1,2,3,4-tetrahydropyridines in Synthesis. Intramolecular Alkylation Reactions and Stereoselective Synthesis of Anti-2,6-Disubstituted Piperidines

Modified Dötz Benzannulation Reactions Part 2: β-Chlorovinyl Carbene Complexes in Organic Synthesis

Triisopropylsilyl Protected Hexa-1,5-diyne-3,4-dione: A Convenient Precursor to 2,3-Dialkynyl 1,4-Diazabutadienes

Dimethylation and Hydrodechlorination of gem-Dichlorocyclopropanes with Grignard Reagents Promoted by Fe(III) or Co(II) Catalyst

γ-Alkylation of Unsaturated Carboxylic Acids. Stereoselective Synthesis of 2Z- and 2E,6E-3-Methyldeca-2,6-dienoic Acids from 3-Methylbut-2-enoic Acid Through Consecutive Ireland Claisen and Cope Rearrangements

New Highly Diastereoselective Synthesis of Phosphoramidates. A Route to Chiral Methyl p-Nitrophenyl Alkylphosphonates

Synthesis of a Bicyclic Cation Related to Sterol Biosynthesis and Its Chemical Destiny, Part I

Synthesis of a Bicyclic Cation Related to Sterol Biosynthesis and Its Chemical Destiny, Part II

Stereoselective Synthesis of α-C-Glycopyranosyl Isoprenoid Compounds

Mild but Efficient Methods for Stereoselective Glycosylation with Thioglycosides: Activation by [N-Phenylselenophthalimide-Mg(ClO₄)₂] and [PhIO-Mg(ClO₄)₂]

New Synthesis of Carbazoles from Novel exo-2-Oxazolidinone Dienes

Synthesis and Radical Cyclization of 2-Allylamino-3-chloropropylphenyl Sulfones to 2,4-Disubstituted Pyrrolidines

The Generation of Highly Functionalized Organometallics via Organotellurides and The Stereospecific Preparation of N-Isobutyl 6-Hydroxyl-(2E,4Z)-hexadienamide Derivatives

The Preparation of (E)-1-Alkenylthiosilanes by the Reduction and Silicon Capture of 1-Alkenesulfenate Anions

Stereoselective Synthesis of Allylic Sulfoximines from S-(Chloromethyl)-N-methyl-S-phenylsulfoximine and Alkenyl Cuprates

Behaviour of Dioxolanones as Chiral Acyl Anion Equivalents