Synfacts

Issue 12 · December 2014

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A156
SYNFORM ISSUE 2014/12 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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1233
Synthesis of Norleucosceptroids A, B, and K FREE ACCESS

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1234
Collective Synthesis of Humulanolides Using a Metathesis Cascade

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1235
Synthesis of Nominal Cycloinumakiol and Structural Revision

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1236
Synthesis of Trifluorinated Thiazolines That Target Prohibitins

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1237
Synthesis of a c-Kit Kinase Inhibitor Using Organocatalysis

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1238
Total Synthesis of (±)-Tubastrindole B

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1239
Synthesis of BMS-663068 FREE ACCESS

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1240
Synthesis of Nominal Trichodermatide A

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1241
Synthesis of Lycopodium Alkaloids Containing Seven-Membered Rings

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1242
Synthesis of an Androgen Receptor Modulator

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1243
Divergent Total Synthesis of Aspidosperma Alkaloids

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Synthesis of Heterocycles
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1246
Synthesis of Imidazo-Fuzed Heterocycles via Gold-Catalyzed Cycloaddition

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1247
Inverse-Electron-Demand Diels–Alder Reaction of Asymmetric 1,2,3-Triazines

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1248
Pyridazines via an Organophosphorus-Catalyzed Diaza-Wittig Reaction

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1249
Palladium-Catalyzed Synthesis of Quinolines From Cyclopropanols

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1250
Catalyst-free Synthesis of 1-Aryltetrazoles

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1251
Synthesis of Phenanthridines from Diaryliodonium Salts and Nitriles

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1252
Synthesis of Oxazinoindoles and Pyrrolooxazines by Sc(III) Catalysis

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1253
Amidation–Oxidative Cyclization Route to 2-Aryl-2H-benzotriazoles

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1254
Fused Isoquinolones by Aryne/Alkyne Insertion into C–H/N–H Bonds

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1255
ArI-Catalyzed Synthesis of Benzolactones

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1256
Copper-Catalyzed Synthesis of 1-Bromoindolizines from Pyridines

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1257
Enantioselective Synthesis of Pyrrolidinones and Dihydropyridinones

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1258
A Photocatalytic Hydroamination Route to Dihydropyrazoles

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1259
Synthesis of 1,4-Thiazepin-5(4H)-ones without Transition Metals

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Synthesis of Materials and Unnatural Products
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1261
Pass the P₂ FREE ACCESS

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1262
New Macrocycles on the Scene: O₆-Corona[3]arene[3]tetrazines

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1263
Alkynes of Routes to Furans, Pyrroles, and Thiophenes

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1264
Fluorescent Indazoloquinazolinones by Intramolecular C−H Amination

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1265
Sequential Steps Save the Day

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1266
A Panchromatically Electrochromic Small Molecule

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1267
Expecting Silicon Valley, Finding Silicon Planar

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1268
Efficient Heteroarylation of Aromatic Amines via Dual C–H Activation

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1269
Next Time You Need a Fluorene, Try a Triazene

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1270
Climbing the Bisindeno-[n]thienoacene Ladder, One Rung/Ring at a Time

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1271
Air-Stable and Conductive 13-Fused-Ring Thienoacenes

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1272
Kick Your MOFs Up a Notch

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1273
Fe(III)-Catalyzed Enantioselective Conia-ene Reaction FREE ACCESS

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1274
Rhodium-Catalyzed Hydroformylation of Z-Enamides and Z-Enol Esters

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1275
Iridium-Catalyzed Allylic Substitution of Silyl Dienolates FREE ACCESS

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1276
Nickel-Catalyzed Asymmetric Hydrogenation of Olefins

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1277
Asymmetric 1,4-Addition of Alkyl Groups to N-Sulfonyl Imines

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1278
Iron(II)-Catalyzed Intermolecular Amino-Oxygenation of Olefins

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1279
Copper-Catalyzed Enantioselective Allylic Alkylation Using Terminal Alkynes

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1280
Enantioselective Gold-Catalyzed Cyclopropanation of 1,6-Enynes

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1281
Enantioselective Trifluoromethylation of Unactivated Alkenes

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1282
Chiral Chromanes via Gold-Mediated Cyclization Employing Free Allylic Alcohols

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1283
Copper-Mediated E-Selective Trifluoromethylation of α,β-Unsaturated Hydrazones

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1284
Iron-Catalyzed Asymmetric Intramolecular Cyclopropanation

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1285
Asymmetric Alkene Carboamination by Palladium Catalysis

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1286
Asymmetric Synthesis of α,α-Diﬂuoro-β-lactams

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1287
Copper-Mediated Enantioselective Hydrobromination of Styrenes

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1288
Synthesis of Chiral Pyrazolines via Chiral π-Cation Catalysis

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1289
Enantioselective Amination of Racemic Allylic Alcohols

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1290
Reverse Regioselective [4+3] Cycloaddition

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1291
Iridium-Catalyzed Enantioselective Hydrogenation of Pyridinium Salts

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1292
Palladium-Mediated Asymmetric 1,4-Addition of Diarylphosphines to N-Enoyl Phthalimides

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1293
Palladium-Mediated Asymmetric Decarboxylative Allylic Alkylations of α-Imino Anions

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1294
De Novo Synthesis of P-Stereogenic Compounds via Iridium Catalysis

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1295
Enantioselective Hydroalkoxylation of Allene Catalyzed by Palladium

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1296
Asymmetric Allylic Alkylation of Hydroxyacrylates Catalyzed by Palladium

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1297
Intramolecular Alkene Hydrosilylation Catalyzed by Rhodium

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1298
Asymmetric Alkynylation–Lactamization Cascade Catalyzed by Copper

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1299
Enantioselective Palladium and Phosphoric Acid Catalyzed Allylations of Aldehydes

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1300
Asymmetric Synthesis of Planar Chiral Ferrocenes

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1301
Asymmetric Allylic Alkylation of Azlactones with Allylic Alcohols

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Metal-Mediated Synthesis
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1303
Catalytic gem-Difluoropropargylation Using Aryl and Alkenyl Boron Reagents FREE ACCESS

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1304
Palladium-Catalyzed Cross-Coupling of Secondary Alkylzinc Reagents

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1305
Copper-Mediated Bis-anilide Cyclization by Double C–H/Ar–H Coupling

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1306
Enantioselective Protoboration of Disubstituted Allenes

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1307
Gold-Catalyzed Cycloisomerization to C2- and C3-Borylated Furans

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1308
Toward the O-Arylation of β-Hydroxy-α-Amino Acid Substrates

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1309
Cross-Coupling of Organolithium Reagents with Aryl and Vinyl Triflates

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1310
Copper-Mediated Acetoxylation

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1311
Nickel-Catalyzed Double Carboxylation

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1312
Scandium-Catalyzed [3+2] Cycloaddition of Allylsilanes to β-Silylenones

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1313
Copper-Catalyzed Silylation of Aldehydes

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1314
Three-Component Differential Vicinal Diarylation of Terminal 1,3-Dienes

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1315
Cross-Coupling of Unactivated Aryl Sulfides with Arylzinc Reagents

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1316
Reaction of Arylboronic Acids with α-Aminoesters and α-Aminoacetonitriles

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1317
Noncryogenic Boronate Rearrangement

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Organo- and Biocatalysis
z1319
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1319
Cascade [4+2] Annulation by NHC Catalysis

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1320
Phosphepine-Catalyzed Enantioselective Synthesis of Cyclopentenes

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1321
Novel Oligomeric Helical Chiral Catalysts for Asymmetric Dearomatization FREE ACCESS

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1322
Enantioselective Phase-Transfer Alkylation of Sulfenate Anions to Sulfoxides

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1323
Organocatalytic Biomimetic Synthesis of Izidine Alkaloids

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1324
Synthesis of Dicarbonyls by Combining Organocatalysis and Photoredox Catalysis

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1325
Organocatalytic Radical Addition to Alkenes

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1326
Brønsted Acid Catalyzed Enantioselective Formation of Tetrahydroxanthenes

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1327
Thiourea-Catalyzed Enantioselective Addition of Indoles to Pyrones

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1328
Asymmetric Countercation-Directed Nucleophilic Aromatic Substitutions

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1329
Enantioselective α-Amination by a BINAM-Derived Phase-Transfer Catalyst

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1330
Anion-Binding Catalysis Mediated by Pyridinium Cations

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Polymer-Supported Synthesis
z1331
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1331
Dendritic Copper Catalysts for Homogeneous Click Chemistry in Water FREE ACCESS

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1332
Ritter Reaction of Alcohols with Nitriles Using NaHSO₄/SiO₂

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1333
Benzylic Oxidation with a Manganese Triazolate Framework

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1334
Reductive Amination of Nitriles to Tertiary Amines Using Platinum Nanowire

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1335
Reduction of Nitroarenes with NaBH₄ Using Graphene-Supported PdCu Nanoparticles

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1336
[2+2+2] Cycloaddition Using a Silica-Supported Rh–NHC Catalyst

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1337
Aerobic Oxidation and Reduction Using Pd⁰-in-UiO-67

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1338
C₃N₄-Catalyzed Oxidative Allylation of Tetrahydroisoquinoline Derivatives

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1339
The Sonogashira Coupling Using Pd_np-nSTDP

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1340
The Sonogashira Coupling with a PS-Supported Palladium Catalyst

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1341
Direct C–H Amination of Benzothiazoles Using CuFe₂O₄ Nanoparticles

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1342
Light-Mediated Deiodination and Cyclization Using PtNPs@TiO₂

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1343
Henry and Suzuki–Miyaura Reactions with SBA-15/CCMet and Pd Complex

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1344
Transfer Hydrogenation of Alkenes Using Ni/Ru/Pt/Au Nanoparticles

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1345
Titanosilicate Zeolite Catalyzed Selective Oxidation of Sulfides with H₂O₂

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Erratum
1347
Direct Amination of β-Keto Esters Employing Nitrosocarbonyl Compounds

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1347
Tandem Divergent Catalysis using Nitriles

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1348
Enantioselective Carbonyl Carboacylation Initiated by C–C Bond Activation

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