Synfacts

Issue 03 · March 2016

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Synform
A36
SYNFORM ISSUE 2016/03
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Synthesis of Natural Products and Potential Drugs
z219
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0219
Synthesis of (–)-Chloramphenicol

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0220
Synthesis of (S)-Baclofen

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0221
Synthesis of Gelsenicine
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0222
Total Synthesis of (+)-Cytosporolide A

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0223
Synthesis of a CGRP Receptor Antagonist
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0224
Synthesis of (–)-Hymenosetin

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0225
Synthesis of a MCH₁ Receptor Antagonist

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0226
Synthesis of (R)-Lacosamide

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0227
Synthesis of PF-04191834

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0228
Synthesis of Enigmazole A

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0229
Synthesis of (+)-Fastigiatine

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0230
Synthesis of Cyclomarin A

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0231
Synthesis of Vismodegib

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0232
Synthesis of (+)-Chlorolissoclimide

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Synthesis of Heterocycles
z233
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0233
Synthesis of Dihydrofurans from β-Ketocarbonyl Compounds and Olefins

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0234
Synthesis of Oxazinanones from β-Lactams by Amide Bond Activation

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0235
Tetrahydroquinolines by Michael Addition/Nitro-Mannich Reaction

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0236
Palladium-Catalyzed Heteroannulation Route to (E)-Oxindolylideneacetates

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0237
Aldehyde Allylation/Cyclization with Isocyanato Allylboronic Esters

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0238
Enantiopure α-Substituted Piperazines by Asymmetric Lithiation−Trapping

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0239
Gold-Catalyzed Synthesis of 7-Acylindoles from Anthranils

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0240
Synthesis of Fluorinated Thiophenes by Ring Contraction of Thiopyrans

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0241
Synthesis of 1-Benzyl- or 1-Benzoyliso-quinolines by Dehydrogenative Coupling

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0242
Palladium-Catalyzed Synthesis of Difluoroalkylated Phenanthridines

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0243
Pd-Catalyzed Arylation/[1,2]-Wittig Rearrangement of Pyridylmethyl Ethers

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0244
Synthesis of Imidazo[1,2-a]pyridines by 1,3-Dipolar Cycloaddition

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0245
Synthesis of Pyrrolopyridines from 3-Aminopyrrole

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0246
Synthesis of Benzoxazoles by Copper/Palladium Catalysis

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0247
Three-Component Synthesis of Oxazolidin-2-ones

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Synthesis of Materials and Unnatural Products
z249
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0249
A Biphenyl Donor–Acceptor–Donor Ladder System

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0250
Mind the ‘Band’ Gap

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0251
A Solution for Dissolution of Polysaccharides

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0252
Filling the Two-Coordinate, Acyclic Diaminosilylene Gap

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0253
Adopting a Reductive Coupling Route to Grams of DOPT

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0254
Potential Holey-Nanographene Precursor: A Pyrene-Based Macrocycle

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0255
Good Things Come in Threes: Kabachnik–Fields Polycondensation

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0256
Building Energetic Wheels for Hydrazine

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0257
Got an Eye on Binding Anions? Better Put a (Rhenium-Capped) Ring on It

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0258
Synthesis of Dibenzo[a,m]rubicenes and their Application in OTFTs

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0259
Photochemical Cyclodehydrochlorination with Regioselectivity

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0260
2 Se or Not 2 Se, That is the Question

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z261
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0261
Synthesis of Axially Chiral Vinyl Arenes by Palladium(0) Catalysis
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0262
A New Ligand Design for Asymmetric Dehydrogenative Heck Arylation

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0263
Asymmetric Hydrothiolation by Dynamic Kinetic Resolution

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0264
Palladium-Catalyzed Regioselective 1,1-Difluoroallylation and Heck Cyclization

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0265
Copper-Catalyzed Asymmetric Synthesis of Polysubstituted Cyclopropanes

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0266
N–C Axial Chirality in Phenanthridine-6-ones by Palladium(0) Catalysis

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0267
Iridium-Catalyzed Asymmetric Allylation of Silyl Enol Ethers

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0268
Zinc-Catalyzed Diastereo- and Enantioselective Mannich-Type Reaction

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0269
Enantioselective Aza-Michael Addition Catalyzed by a Chiral Boronic Acid

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0270
A Copper-Catalyzed Enantioselective Hydroamination Sequence

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0271
Copper-Catalyzed Nitroso-Diels–Alder Reaction

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0272
A Bimetallic Titanium Catalyst for Asymmetric Epoxidation and Sulfoxidation

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0273
Palladium-Catalyzed Asymmetric Decarboxylative Cycloaddition

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0274
Asymmetric Domino Heck/Intermolecular C–H Bond Functionalization

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0275
Metal Amide Catalyzed Asymmetric endo-Selective Cycloadditions

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0276
Enantioselective 1,3-Dipolar Cycloaddition of Azomethine Ylides

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0277
Synthesis of Chiral Tetrahydroquinolines by a Palladium–P,S Ligand Complex

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0278
Hydrosilylation of Imines by a Chiral Zinc Catalyst

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0279
Chiral α-Amino Acids by Palladium-Catalyzed Allylic Alkylation

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0280
Scandium(III)-Catalyzed Asymmetric Synthesis of 1,2-Allenyl Ketones

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0281
Copper-Catalyzed Asymmetric Cross-Aldol Reactions
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0282
Copper-Catalyzed Synthesis of Chiral α-Hydroxy Amides and β-Amino Alcohols

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0283
Iridium-Catalyzed Asymmetric Redox-Triggered Carbonyl Addition

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0284
Asymmetric Hydrogenation of α-Oxyfunctionalized α,β-Unsaturated Acids

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0285
Asymmetric Synthesis of α-Fluoromethylated Tertiary Alcohols

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0286
Enantioselective Arylation of Isatin-Derived Ketimines

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0287
Nonenzymatic Desymmetrization of Prochiral Allenic Diols

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0288
Rhodium-Catalyzed C–C Bond Activation

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Metal-Mediated Synthesis
z289
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0289
Catalytic Conjunctive Cross-Coupling
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0290
Multicarbometalation of Alkynes

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0291
Copper-Catalyzed Borylative Aromatization

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0292
Synthesis of N-Boc-Propargylic and -Allylic Amines

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0293
Copper-Catalyzed Asymmetric Allylic Arylation

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0294
Transition-Metal-Free Cross-Couplings of Organoboron Reagents

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0295
Ruthenium-Catalyzed C–O Activation/C–C Coupling Reactions

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0296
Asymmetric Direct 1,2-Addition

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0297
Sulfonylation of Aryl C(sp²)–H Bonds

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0298
Iridium-Catalyzed Borylation of Aromatic Aldehydes

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0299
Palladacycle-Catalyzed Aqueous Lipshutz–Negishi Cross-Coupling

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0300
Selective Activation of Isatin Carbonyls

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0301
Stereoselective Synthesis of Z-α,β-Unsaturated Sulfones

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0302
Chemoselective Addition of Halomethyllithiums to Isatins

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0303
Construction of α-Aryl β-Substituted Cyclic Ketone Scaffolds

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Organo- and Biocatalysis
z305
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0305
Strong Hydrogen-Bonding Organocatalysts Activated by Electrostatics

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0306
Organocatalytic Enantioselective Desymmetrization of Oxetanes

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0307
Whole-Cell Biocatalysts for Stereoselective C–H Amination Reactions

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0308
C₁-Symmetric Chiral Brønsted Acid Catalyzed Diels−Alder Reaction

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0309
Regiodivergent Enantioselective Addition of Oxazolones

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Polymer-Supported Synthesis
z311
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0311
Suzuki Coupling with an N-Heterocyclic Carbene–Palladium Catalyst
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0312
Synthesis of Spirocyclic Pyrazoles on Sulfonated Silica Supported Fe₃O₄

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0313
One-Pot Synthesis of Chiral Esters by Oxidation–Olefination–1,4-Addition

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0314
Amination of Aryl Halides with Palladium on Magnetic Nanoparticles

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0315
Titanium Superoxide Catalyzed Oxidative Esterification of Aldehydes

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0316
Palladium/Al(OH)₃-Catalyzed Stille and Kumada Coupling

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0317
Asymmetric Suzuki–Miyaura Coupling with Biotin-Tagged Palladium

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0318
Reduction of Hetarenes with a Rhodium Nanoparticle–Ionic Liquid Catalyst

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0319
Hydrogenation of Nitroarenes with Polymer-Supported Ruthenium Nanoparticles

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0320
Preparation of 3-Amino-1,4-Diynes by Using Copper Oxide Nanoparticles

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0321
Mesoporous Silica-Supported Zirconium Catalyst for Carbonyl Hydroboration

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0322
Hydrogenation of Carbonyl Groups with Ruthenium Nanoparticles on Graphene

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0323
A Chiral Imidazolidinone Polymer for the Asymmetric Diels–Alder Reaction

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0324
Oxidative Imine Formation with Vitamin B₁₂-Derived Mesoporous Carbon

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0325
Synthesis of Enol Carbamates and Amides with Copper Nanoparticles on Charcoal

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0326
Synthesis of Perhydrotriazolotriazole Derivatives with Fe₃O₄@SiO₂-TiO₂

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Erratum
327
Synthesis and Study of 7,12,17-Trioxa[11]helicene

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327
(±)-Spiramilactone B, (±)-Spiraminol, (±)-Dihydroajaconine, and (±)-Spiramines C and D

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