Synfacts
Issue 03 · March 2024
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A036
SYNFORM
ISSUE 2024/03
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Synthesis of Natural Products
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0223
Total Synthesis of (–)-Cephalocyclidin A
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0224
Synthesis of Calyciphylline A-Type and Macrodaphniphyllamine-Type Alkaloids
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0225
Total Synthesis of (+)-Rhodomollin A
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0226
Enantioselective Total Synthesis of (+)-Euphorikanin A
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0227
Synthesis of (–)-Garryine
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0228
Total Synthesis of (+)-Arboduridine
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0229
Total Synthesis of (–)-Magellanine
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Synthesis of Heterocycles
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0231
Strained
exo
-Methylene Heterocycles as Dipolarophiles: Synthesis of Unexplored Spiroisoxazolines
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0232
Multicomponent Synthesis of Tetrahydroisoquinolines
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0233
Synthesis of 2-Alkylmethyl Pyrroline Derivatives
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0234
Sc(OTf)
3
‑Catalyzed Cycloadditions for the Synthesis of Substituted Indolines
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0235
Gram-Scale, Modular Access to C
2
-Bis(Oxazoline) Ligands
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0236
Multicomponent Synthesis of Quinolines via Hydrogen-Transfer Reaction
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0237
A Highly Diastereoselective Synthesis of Sulfur-Containing Unnatural Amino Acids
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0238
Efficient, Epimerization-Free Solid-Phase Peptide Synthesis
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0239
Versatile Synthesis of Tertiary and Heterocyclic and Aromatic Amines
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0240
Practical and Efficient Access to Multifunctional BCPs
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0241
Synthesis of 2,5-Disubstituted Pyridines via Gold(I)-Catalyzed Cycloisomerization of 1-Bromoalkynes
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0242
Nitrogen Atom Insertion into Arenols in the Synthesis of Benzazepines
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0243
Palladium-Mediated Synthesis of 3-Methylindoles Under Mild Conditions
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Synthesis of Materials and Unnatural Products
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0245
2-Center-3-Electron π-Bond without a σ-Bond
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0246
Aryne-Activated Smiles Rearrangement of Anilines
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0247
Hydroaminoalkylation of Polybutadiene
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0248
Iterative Binomial Synthesis of Monodisperse Conjugated Polymers
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0249
Alternating Poly(Lactic-
co
-Glycolic Acid) from Racemates
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0250
Phenanthridines from Oxime Esters
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0251
1,3-Azaphospholes
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0252
Chloride-Directed Enantioselective C(sp
2
)–H Borylation
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0253
Macrocycle Skeletal Rearrangement of a Cationic Borane
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0254
Facile Synthesis of Indolocarbazole from Indoles
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0255
Heptagon Annulation via C−H Activation
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0256
A Neutral 2π-Aromatic Si
2
B
2
Ring
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Metals in Synthesis
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0257
Wittig-Type
E
-Selective Olefination of Imines with Vinyl Boronate Esters Under Copper Hydride Catalysis
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0258
Cyanation of Allenes via Copper-Catalyzed Site-Selective C(sp
2
)–H Hydrogen Atom Abstraction
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0259
Regioselective C(sp³)–H Activation of Cyclic Aliphatic Acids: Synthesis of Unsaturated Bicyclic Lactones
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0260
Acylation of Unactivated C(sp
3
)–H Bonds with Acyl Azolium Reagents under Photoinduced Cerium Catalysis
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0261
Rhodium Catalyzed Three-Component Coupling Annulation of 2-Aryloxazolines
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0262
Asymmetric Synthesis of Eight-Membered
N
-Hetero-cycles by Palladium-Catalyzed (4+4) Cycloaddition
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0263
Divergent Multicomponent Fluoroalkylative Carbonylation of 1,3-Enynes Under Palladium Catalysis
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0264
An Electroreductive Strategy for the Hydroxy Fluorosulfonylation of Alkenes
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0265
Regioselective C(sp
2
)–H Borylation of (Hetero)Arenes under Cobalt Catalysis
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0266
Iron-Catalyzed Coupling of Allylic Dithianes with Alkynylsilanes Involving a Dithiane Rearrangement
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0267
Tetracyclic Cycloheptanols Synthesis via Rhodium-Catalyzed Cascade Reaction
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0268
Cobalt-Catalyzed Synthesis of Amines via Nitriles Electrohydrogenation
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0269
Hiyama Cross-Coupling of
gem
-Difluoroalkenes: Stereoselective Synthesis of Tetrasubstituted Olefins
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0270
Copper-Catalyzed Suzuki–Miyaura Cross-Couplings of Unactivated Alkyl Halides
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0271
Photoenzymatic Catalyzed Coupling of Amino Acids with Vinylpyridines
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0272
Carbonylation/Amination of Alkylidenecyclopropanes Towards Eight-Membered Benzolactams
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0273
Electrophotochemical Decarboxylative Vinylation of Carboxylic Acids under Dual Cerium and Nickel Catalysis
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0274
Enantioselective α-Alkylation of Enolizable Ketones with Alkyl Iodides under Bimetallic Nickel Catalysis
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0275
Nickel-Catalyzed Silylalkylation of Unactivated Terminal Alkenes
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0276
Enantioselective Synthesis α-Gem-Difluorinated Alcohols via Rh(III)-Catalyzed Transfer Hydrogenation
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0277
Asymmetric Hydroacylation of Internal Olefins and Aldehydes
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0278
Alkyllithium- and Magnesium Salt-Assisted 1,1- and 1,3-Aminoboration of Alkenes under Nickel Catalysis
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0279
Iridium Photoredox-Catalyzed Nitrative Difunctionalization of Alkenes
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0280
Sequential Cu-Borylation Strategy for a Stereodivergent Synthesis of Functionalized Cyclohexanones
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0281
Synthesis of Linear Aliphatic Amides via Rh-Catalyzed Hydroamidation of Internal Olefins
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0282
Iron-Photocatalyzed C(sp
2
)–H Trifluoromethylation of (Hetero)Arenes with Trifluoroacetates
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0283
The First Use of Aryltrimethylammonium Salts in Nickel-Catalyzed Suzuki Cross-Couplings
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Polymer-Supported Synthesis
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Intramicellar Pd-Catalyzed β-Arylation of Thiophenes
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0286
Oxidative Coupling of Amines Using a 4-Nitrophenylacethylene-Functionilzed Cu
2
O Crystal
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0287
A Spirobifluorene-Based COF for Photo-Induced Nickel-Catalysed Amination of Aryl Halides
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0288
Photocatalytic Synthesis of 1,3-Diarylated Imidazo[1,5-
a
]pyridines with Carbon Nitride
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0289
Photocatalytic Dehalogenative Deuteration and Hydrogenation of Halides by a Chromium-Based MOF
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0290
Nitriles and Amides Synthesis from 1,2-Diols by N-Doped Porous Carbons
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0291
Borylation of Alkyl and Aryl Halides Using CeO
2
Nanorods
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0292
Preparation of Alkylamines from Alcohols and Carbonyl Compounds through Reductive Amination
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0293
Minisci-Type Reactions Promoted by a Zirconium-Phenazine MOF
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0294
Dehydrogenative Coupling of Organosilanes with Alcohols by a Single-Atom Gold(I) Catalyst
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0295
Dehydrogenative Cross-Coupling of P(O)H and Thiols by a Polyoxomolybdate Photocatalyst
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Organo- and Biocatalysis
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0297
Metal-free
meta
-Selective C–H Amination of Arenes
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0298
Acid-Catalyzed Nitromethane Activation for the Synthesis of Amides and Nitriles
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0299
Enzymatic C–H Amidation toward Stereoselective Construction of β-, γ- and δ-Lactams
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0300
Enantioselective C−C Bond Insertion into Aldehydes via Oxazaborolidinium Catalyzed 1,2-Acyl Shift
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0301
Biocatalytic Approach for the Synthesis of Lactones via Carbene C–H Insertion
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0302
Photoenzymatic Hydrosulfonylation of Olefins Initiated by Single Electron Oxidation
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0303
VANOL-Derived Imidodiphosphorimidate-Catalyzed Bromospiroketalization
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0304
Stereoselective α-Benzylation of Cyclic Ketones via Chemoenzymatic Cascade
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0305
Asymmetric Cyclizations Catalyzed by Chiral Boryl Radicals
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0306
Brønsted Acid Catalyzed Aromatization-Enabled Umpolung of Imines
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Innovative Drug Discovery and Development
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0307
A Rhodium-Catalyzed “Hook-and-Slide” Homologation of Amides
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0308
HIV-1 Non-Nucleoside Reverse Transcriptase Inhibitors That Prematurely Activate Protease Causing Cell Death
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0309
Chemoenzymatic Syntheses of Fluorine-18-Disaccharides to Image Bacterial Infection
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0310
Facile Access to Bioactive Piperidine-γ-Butyrolactones
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0311
Synthesis, Structural Validation, and SAR of Antifungal Fusaramin
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0312
Tryptamine Derivatives of Norpsilocin Induce Psychedelic-Like Responses in Mice
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0313
Novel Synthesis of Levadopa Improves Efficiency and Eliminates Use of Pyrophoric Raney Nickel
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0314
Selective Installation of C
1
-C
3
Fluorocarbons to Aldehydes
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0315
Multikilogram Birch Reduction and Evaluation of Alternative Synthetic Routes to a Ketalized Cyclohexene Derivative
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0316
Accessing 2-Aminophenol Derivates Using Triplet-State Nitro(hetero)arenes and Copper Photocatalysis
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0317
Development of a Continuous Flow Process for Photoredox Decarboxylative Fluorination
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0318
A Chiral Amide Directing Group for Ruthenium-Catalyzed Asymmetric C–H Activation
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0319
Matteson Homologation-Based Total Synthesis of Meliponamycin A
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0320
Discovery of the Selective KRAS G13D Inhibitors Derived from the Scaffold of KRAS G12C Inhibitor
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0321
Photo-Uncaging of a Microtubule Depolymerizer Reduces Tumor Volume in a Mouse Model
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0322
Photomediated Deaminative Generation of Tertiary Anions
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Peptide Chemistry
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0323
Peptide Cyclization of Unprotected Peptides with Cysteine at C-Terminal
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0324
Boronic Acid-Catalyzed Peptide Bond Formation from Serine- and Threonine-Derived Inert Esters
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0325
Metal-Free Synthesis of α‑Tertiary Amino Acid Derivatives via Photoinduced Cross-Coupling
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0326
Unnatural Peptide Synthesis through Rh(III)-Catalyzed Diastereoselective Ligation with Three Components
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0327
Isothiourea-Catalyzed Conjugate Addition to Form Proline Derivatives
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0328
Palladium-Catalyzed Photoinduced Alkylation for Glycine Derivatives
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0329
Direct Amidation of Unprotected Amino Acids Mediated by Hexylsilane
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0330
Co-Catalyzed Asymmetric Aza-Barbier Reaction: A Useful Method for α-Tertiary Amino Ester Synthesis
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0331
Direct Synthesis of γ-Amino Acid Derivatives via Cobalt-Catalyzed Aminoalkylative Carbonylation of Alkenes
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0332
Palladium-Catalyzed Cross-Coupling for the Synthesis of Pyridyl Amino Acids
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Flow Chemistry
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0333
Continuous-Flow Heterogeneous Rhodium-Catalyzed Asymmetric Hydroacylations
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