Synfacts

Issue 10 · October 2024

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SYNFORM ISSUE 2024/10
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Synthesis of Natural Products
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Total Synthesis of (–)-Rauvomine B
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Synthesis of (+)-Kalmanol

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Synthesis of (–)-Griseoviridin

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Total Synthesis of (–)-Platensilin

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Total Synthesis of (–)-Crinipellin A and B

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Total Synthesis of (±)-Baphicacanthcusine A

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A Formal Synthesis of (±)-Morphine
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Synthesis of Heterocycles
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Substituent-Directed Cycloisomerization Reduction Cascade for Synthesizing Oxacycles
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1020
Using Bench-Stable 2-Mercaptothiazolinium Salts for the Photoredox Alkylation of N-Heteroarenes

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1021
Nickel-Mediated Skeletal Editing: Internal ‘O’-to-‘N’ Exchange of Oxazoles and Oxadiazoles

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1022
Ring Expansion of Pyrroles with Concomitant Nitrogen Deletion

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1023
Synthesis of Functionalized Pyrrolidines and Piperidines

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1024
Simple Two-Step Protocol for the Synthesis of Amino-Oxetanes

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1025
Regioselective Approach to (Z)-5-Methylene-morpholin-2-ones from Amino Acids and Enones

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1026
Multigram Synthesis of Diastereomerically Pure 3-Substituted 6-Azacyclo[3.3.1]heptane Derivatives

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1027
Synthesis and Property Analysis of Monocyclic B–OH Diazaborines

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1028
Atom Transmutation Converting Pyridines into Substituted Benzene Derivatives

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1029
Formal Reductive Amination of N-Heterocycles through N-Alkenylation/Reduction Sequence

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1030
Ru-Mediated Synthesis of Chiral Secondary Alcohols

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Synthesis of Materials and Unnatural Products
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1031
A Stable Stannyne
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1032
Surface-Initiated HAT-RAFT

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1033
Photoreductive Functionalization of Aryl Alkynes

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1034
Azaparacyclophanes by One-Step Catalyst-Transfer Macrocyclization

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1035
Intramolecular ipso-Arylation via Halogen Atom Transfer

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1036
Giant Supramolecular Hexagons

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1037
Fusing Twisted Nanobelts with Helicenes

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1038
Porphyrin-Diazaporphyrin Molecular Tapes

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1039
Visible-Light-Induced Direct C–H Alkylation of Polycyclic Aromatic Hydrocarbons with Alkylsulfones

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1040
Fused Koelsch Radical

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1041
Thermally Stable, Chemically Recyclable Polymers

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1042
Boraphenalenes

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Metals in Synthesis
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1043
Copper-Catalyzed Oxidative Hydrofunctionalization of Alkenes
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1044
Synthesis of 2-Aminothiozaoles via Photocatalyzed Annulation of Enaminones with Thioureas

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1045
Regiodivergent Nickel-Catalyzed Hydrosilylation of α-(Fluoroalkyl)styrenes
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1046
Enantioselective Benzylation of Sulfonylimines with para-Methylphenols via a Paired Electrolysis Strategy

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1047
Nickel-Catalyzed Regio- and Diastereoselective Hydroalkylation of Alkynyl Boronamides

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1048
Enantioselective Carboamination via Palladium Catalysis

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1049
A Nickel-Catalyzed Nozaki–Hiyama–Kishi Reaction under Visible Light Photocatalysis

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1050
C–C Bond Cleavage of Allylic Alcohols Enabled by a Modified Mukaiyama Hydration

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1051
Synthesis of Aryl Sulfonamides by a Sandmeyer-Type Chlorosulfonylation of Anilines

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1052
Photocatalyzed Amination of Phenols and Halophenols

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1053
Asymmetric Synthesis of Spirocyclic Lactones

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1054
Ligand-Controlled Regiodivergent Asymmetric Cascade Hydroboration and Hydroallylation of Terminal Alkynes

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1055
Copper-Photocatalyzed Amination of Unactivated Alkyl Halides by Inner-Sphere Single Electron Transfer

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1056
Synthesis of Enantioenriched β-Aryl Amino Acids via Palladium/Lewis Acid Relay Catalysis

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1057
Iridium-Catalyzed Desymmetrization Enables Access to Distal Biaxial Atropisomers

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1058
Single-Carbon Skeletal Editing of Alkenes via Rhodium Catalysis

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1059
Nickel-Catalyzed Asymmetric Cross-Hydrodimerization of Enamides and Unactivated Alkenes

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1060
Synthesis of Allenylsilanes via Dirhodium(II) Catalysis: An Amine ON-OFF Effect

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1061
Kinetic Resolution and DYKAT via Palladium-Catalyzed Asymmetric Allylic Substitution of C(sp³)–C(sp³) Bonds

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1062
Silver-Catalyzed Rearrangement of Cyclopropenones to α-Alkylidene Lactones

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1063
Dual Bismuth and Nickel-Catalyzed Deoxygenative Arylation of Alcohols Facilitated by the β-Silicon Effect

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1064
Synthesis of 1-Fluoro-1-arylcyclopropanes via Stille Cross-Coupling

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1065
Asymmetric Synthesis of Sulfur-Stereogenic Sulfilimines by Palladium-Catalyzed Arylation of Sulfenamides

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1066
Rhodium-Catalyzed Hydroformylation of Cyclopropenes

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1067
Dual Iron and Nickel-Catalyzed Photoelectrochemical C–C Functionalization of Alcohols

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1068
Synthesis of N-Aryl-oxamic Acids via Copper Catalysis

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Polymer-Supported Synthesis
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1069
Aerobic Dehydrogenation of Hydrazones to Diazo Compounds with a Fe–N–C Catalyst

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1070
Aerobic Photooxidative Amidation of Aldehydes and Amines with a Triazine-Based COF

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1071
Triazine COF for the Photocatalytic Aerobic Oxidation of Toluenes
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1072
Reduction of Nitroarenes to Anilines Using H₂S as a Hydrogen Donor by a Ceria-Supported Iron Composite

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1073
Enantioselective Electrophilic Amination of Active Methine Compounds Using Chiral COFs

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1074
Palladium Nanoparticles Supported by Co-Ferrite Bearing Arginine-Triazine Units for Aryl Cyanation

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1075
N,P co-Doped Carbon Materials Derived from Yeast for Selective Reduction of Halogenated Nitrobenzenes

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1076
Synthesis of Spiro-Thiazolone-Tetrahydrothiophenes Using a Polystyrene-Supported Amine Catalyst

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1077
Selective Semi-Hydrogenation of Alkynes Catalyzed by a Bimetallic Ag and Cu Single-Atom on g-C₃N₄

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1078
Photocatalytic Oxidation of Sulfides by Perovskite Cs₃Bi₂Br₉/TiO₂ Composites

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1079
Selective Reduction of Nitroolefins to Nitroalkanes Using Frustrated Lewis Pairs Modified NU-1000 MOF

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1080
Hydroboration of Alkynes and Alkenes Using a Core-Shell Copper Nanocluster

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Organo- and Biocatalysis
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1081
A Novel Trifunctional Catalyst Enables Radical–Radical Coupling via Intramolecular Frustrated Lewis Pairs
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1082
Remote C–H Functionalization via Radical NHC Organocatalysis

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1083
Peptide-Catalyzed Kinetic Resolution of β-Branched Aldehydes

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1084
A Novel Electrophilic Cyanation through Phosphonium Activation of Isocyanates

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1085
Inverse Hydride Shuttle Catalysis Enables the Stereoselective Synthesis of Azabicycles

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1086
Carbonic Anhydrase: Zinc-Based Enzyme as a Catalyst for Enantioselective Reduction of Dialkyl Ketones

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1087
Asymmetric Base-Catalyzed Tetrahydrofuran Synthesis from Cyclopropanes and Carbonyl Compounds

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1088
Chiral Phosphoric Acid-Catalyzed Synthesis of 3-Hydroxyindolenines and 3-Oxindoles

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1089
Enantioselective Relay Coupling of Perfluoroalkyl and Vinylogous Ketyl Radicals

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1090
Organocatalytic Asymmetric Synthesis of Si-Stereogenic Silacycles

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Innovative Drug Discovery and Development
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1091
Late-Stage O-to-N Molecular Editing of Bilobalide Alters Pharmacology
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1092
A Convenient, Stable Alternative to SOF₄ for Access to S(VI) Compounds

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1093
Exhaustive Deuterium Editing Study of 1,4-Benzodiazepine-2,5-dione Derivatives
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1094
Rapid Access to Structurally Diverse α-Amido Aldehydes via Dual Fe/Organo-Catalysis

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1095
Three-Component Alkyl Petasis Boron–Mannich Reaction for Accessing C(sp³)-Rich Amines

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1096
Streamlined Synthesis of Antibacterial Polycyclic Xanthenes

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1097
Photochemical Synthesis of Thioesters from Aryl Halides and Carboxylic Acids

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1098
Access to THβC-type Indole Alkaloids via Enantioselective 1,3-Dipolar Cycloaddition

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1099
Highly Selective, Scalable, and Green Access to Esomeprazole via Enantioselective Sulfoxidation

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1100
Enantioselective Diels–Alder Approach to Cannabinoids

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1101
Total Synthesis of Hypersampsone M, an Archetypal Homoadamantane PPAP

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1102
Novel Bismuth-Photocatalyzed Cyclopropanation

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Peptide Chemistry
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1103
Synthesis of Quaternary α-Amino Acids

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1104
Carbon-Isotope-Labeled Amino Acid Synthesis

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1105
Rhodium-Catalyzed Macrocyclization of Peptides
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1106
3,3-Difluoroallyl Sulfonium Salts Mediated the gem-Difluroallylation of Cysteine Residues in Peptides

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1107
Protection of Sterically Hindered Amide of Cyclo-(AA-Gly) Regioselectively Using Triisobutylaluminum

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1108
Aldolase-Catalyzed Enantioselective Amino Acid Synthesis from Glycine

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1109
Synthesis of 3-Benzyl-β-alanine Using Electrochemical Nickel-Catalyzed C(sp²)–C(sp³) Cross-Coupling

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1110
Enantioselective Synthesis of Unnatural Amino Acids by N–H Bond Insertion of Anilines

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1111
Epimerization-Free Native Chemical Ligation Using β-Lactone for the Synthesis of Polypeptides

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1112
α-Amino Acids by Reductive Carboxylation of Imines Using Formate and CO₂

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1113
Pd-Catalyzed β-C(sp³)–H Olefination/Cyclization of Methionine-Containing Peptides

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1114
Direct Alkylamination of Tyrosine Derivatives Using Fe Catalysis and O-Benzoyl-N,N-dialkylhydroxylamines

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1115
Peptide Synthesis Using Unprotected Amino Acids with N-(Z-α-Aminoacyl)benzotriazoles
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Flow Chemistry
z1117
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1117
Enantioselective Alkylation of Ketones In Flow

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1118
Two-Step, Multi-Kilo Synthesis of 4-Methyl-1,2,5-Oxadiazole-3-Carboxylic Acid

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Erratum
1119
Erratum: Synthesis of (–)-Aspersteroid A

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PDF (116 kb)

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