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Synthesis 1994; 1994(2): 145-146
DOI: 10.1055/s-1994-25422
short paper
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A Convenient Method for the Transformation of Alcohols into Alkyl Trifluoromethyl Sulfides

A. A. Kolomeitsev* , K. Yu. Chabanenko, G. -V. Röschenthaler, Yu. L. Yagupolskii
  • *Institute of Organic Chemistry, Ukrainian Academy of Sciences, 253660 Kiev-94, Ukraine
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Publication Date:
17 September 2002 (online)

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Alkyl trifluoromethyl sulfides are prepared by phosphitylation of alcohols or α-hydroxy esters using bis(diethylamido)chlorophosphite followed by the reaction with bis(trifluoromethyl) disulfide under extremely mild conditions in near by quantitative yields.