Nicotine Chemistry. The Addition of Alkyl Radicals to (S)-(-)-Nicotine: Synthesis of Optically Active 6-Alkylnicotines

Jeffrey I. Seeman; Leigh E. Clawson; Henry V. Secor

doi:10.1055/s-1985-31399

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Synthesis 1985; 1985(10): 953-955
DOI: 10.1055/s-1985-31399

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Nicotine Chemistry. The Addition of Alkyl Radicals to (S)-(-)-Nicotine: Synthesis of Optically Active 6-Alkylnicotines

Jeffrey I. Seeman^* , Leigh E. Clawson, Henry V. Secor

^*Philip Morris U.S.A. Research Center, P.O. Box 26583, Richmond, Virginia 23261, U.S.A.

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Publikationsdatum:
27. September 2002 (online)

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Radical alkylation of (S)-nicotine (1) with alkanoic acids (6) in the presence of ammonium peroxydisulfate and silver nitrate to give optically active 6-alkylnicotines 4 is described.