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Synthesis 1985; 1985(10): 975-977
DOI: 10.1055/s-1985-31411
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Synthesis of Symmetrical and Unsymmetrical O,O-Dialkyl Imidodicarbonothioates

Manuel A. Martinez* , Juan C. Vega
  • *Departamento de Química, Facultad de Ciencia, Universidad de Santiago de Chile, Casilla 5659, Santiago, Chile
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Publication Date:
27 September 2002 (online)

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Symmetrical and unsymmetrical (with respect to the alkyl groups) O,O-dialkyl esters of imidodicarbonothioic acid are prepared by reaction of O-alkyl carbonochloridothioates with sodium thiocyanate and treatment of the resultant alkoxythiocarbonyl isothiocyanates with alcohols.