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Synthesis 1986; 1986(4): 305-308
DOI: 10.1055/s-1986-31592
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A New, Efficient Synthesis of Thioloesters

Tomasz Nowicki* , Anna Markowska, Piotr Kiełbasinski, Marian Mikołajczyk
  • *Institute of Organic Chemistry, Technical University (Politechnika) Zwirki 36, 90-924 Łodz, Poland
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Publication Date:
27 September 2002 (online)

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The reaction between phosphorothioic and thiocarboxylic acids and O-alkyl-N,N-dicyclohexylisoureas has been found to give the corresponding phosphorothiolates and thiolocarboxylates in high yields (65-95%), providing a new method for the thiophosphorylation and thiocarboxylation of alcohols.

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