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Synthesis 1987; 1987(3): 275-276
DOI: 10.1055/s-1987-27914
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A Convenient One-Flask Preparation of Di-t-butyl Iminodicarbonate: A Versatile Gabriel Reagent

Leif Grehn* , Ulf Ragnarsson
  • *Institute of Biochemistry, University of Uppsala, Biomedical Center, Box 576, S-751 23 Uppsala, Sweden
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Publikationsdatum:
12. September 2002 (online)

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An improved synthesis of di-t-butyl iminodicarbonate from formamide and di-t-butyl dicarbonate with dimethylaminopyridine as a catalyst followed by aminolytic removal of the formyl group is described as well as a few applications related to the synthesis of primary amines.