Synthesis 1990; 1990(4): 271-273
DOI: 10.1055/s-1990-26849
paper
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One-Pot Synthesis of 4,5-Unsubstituted 1,3-Dithioles and 2-Alkylidene-1,3-dithioles from 1,3-Dithiolane S-Oxides

Ernst Schaumann* , Susanne Winter-Extra, Knut Kummert, Stefan Scheiblich
  • *Institut für Organische Chemie, Universität Hamburg, Martin-Luther-King-Platz, 6, D-2000 Hamburg 13, Federal Republic of Germany
Further Information

Publication History

Publication Date:
17 September 2002 (online)

An efficient synthesis of the title compounds via formal dehydration of the corresponding 1,3-dithiolane S-oxides with iodotrimethylsilane and diisopropylethylamine (Hünig's base) is reported.

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