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Synthesis 1995; 1995(2): 158
DOI: 10.1055/s-1995-3867
DOI: 10.1055/s-1995-3867
short paper
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Simple Alternative Method for the Preparation of Bis(dimethylamino)methylene(trimethylsilyl)phosphane
Further Information
Publication History
Publication Date:
31 December 2000 (online)
Bis(dimethylamino)methylene(trimethylsilyl)phosphane is prepared in good yield by the reaction of the thiuronium salt [(Me2N)2CSMe]I with LiP(SiMe3)2 in 1,2-dimethoxyethane.
phosphaalkene - thiuronium iodide - lithium disilylphosphide - condensation