Synlett

Issue 08 · July 2002

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1181
Familoni, Oluwole Babafemi:
Metalated Sulfonamides and their Synthetic Applications

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1211
Toyota, Masahiro; Ihara, Masataka:
Development of Palladium-Catalyzed Cycloalkenylation and its Application to Natural Product Synthesis

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1223
Donohoe, Timothy J.:
Development of the Directed Dihydroxylation Reaction

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1233
Kawanaka, Yasufumi; Kobayashi, Kaoru; Kusuda, Shinya; Tatsumi, Tadashi; Murota, Masanori; Nishiyama, Toshihiko; Hisaichi, Katsuya; Fujii, Atsuko; Hirai, Keisuke; Naka, Masao; Komeno, Masaharu; Nakai, Hisao; Toda, Masaaki:
One Step Synthesis of Dihydropyridin-2-imines: Inhibitors of Inducible Nitric Oxide Synthase

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1237
Gooßen, Lukas J.; Winkel, Lars; Döhring, Arno; Ghosh, Keya; Paetzold, Jens:
Pd-Catalyzed Synthesis of Functionalized Arylketones from Boronic Acids and Carboxylic Acids Activated in situ with Dimethyl Dicarbonate

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1241
Sanki, Aditya Kumar; Pathak, Tanmaya:
A Glycosylation Driven Strategy for the Synthesis of Anomerically Pure Vinyl Sulfone-modified Pent-2-enofuranoses and Hex-2-enopyranoses

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1245
Shinohara, Yoshiaki; Kurata, Takaaki; Kitano, Hiroyoshi; Matsumoto, Kazutsugu; Takahashi, Ichiro; Hosoi, Shinzo; Ota, Tomihisa; Hatanaka, Minoru:
Annulation of 3-[(R)-p-Toluenesulfinyl]-2-oxopropylidenetriphenyl-phosphorane with 1,4-Enediones; Highly Enantioselective Synthesis of Cyclopentenones

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1249
Guillon, Jean; Léger, Jean-Michel; Massip, Stéphane; Thé, Corinne; Vidaillac, Céline; Monti, Jean-Pierre; Jarry, Christian:
First Diels-Alder Cycloaddition of N′-Oxazolyl-N,N-dimethylalkylamidines with Electron-Poor Dienophiles: Characterization of a Diastereoselective Pathway

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1253
Schmalz, Hans-Günther; Kiehl, Oliver; Gotov, Battsengel:
Electron Transfer Driven Transformations of Transition Metal π-Complexes: Samarium(II) Iodide Mediated Coupling of Fluoroarene-Cr(CO)₃ Complexes with Ketones

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1257
Renard, Delphine; Rezaei, Hadi; Zard, Samir Z.:
A New Convergent Approach to α-Branched Alkynes

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1261
Audran, Gérard; Uttaro, Jean-Pierre; Monti, Honoré:
Enantioselective Taxanes Approach Using Both Enantiomers of the Same Building-Block. Part 1: Taxol^® A-Ring Subunit

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1265
Chen, Jian; Lin, Guo-Qiang; Wang, Zhi-Min; Liu, Han-Quan:
A Short and General Approach to the Synthesis of Styryllactones:(+)-Goniodiol, its Acetates and β-Trifluoromethyl Derivative, (+)-7-epi-Goniodiol and (+)-9-Deoxygoniopypyrone

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1269
Akiyama, Takahiko; Itoh, Junji; Fuchibe, Kohei:
Mannich-type Reaction Catalyzed by HBF₄ in Water: Effect of the Loading of Surfactant

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1273
Smitt, Olof; Högberg, Hans-Erik:
First Total Synthesis of (-)-1(10),5-Germacradien-4-ol

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1277
Singh, Satwinder; Kumar, Subodh; Chimni, Swapandeep Singh:
First Chemoenzymatic Synthesis of Optically Active Uracil and Chromen-4-one Substituted Homoallylic Alcohols: An Entry into Chiral Pool

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1281
Huang, Zhi-Zhen; Wang, Lei:
Novel Synthesis of (E)-α-Fluorochalcones

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1283
Tsujimoto, Takashi; Murai, Akio:
Efficient Detachment of N-Benzyl Carbamate Group

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1285
Bujok, Robert; MĽkosza, Mieczysaw:
Synthesis of 1,1-Difluoroalkanes via Phase Transfer Catalysed Reaction of 1,1-bis-Triflates with KF in the Presence of Cocatalyst - Ph₃SnF

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1287
Kanno, Hisashi; Taylor, Richard J. K.:
Tandem Oxidation Processes: The Direct Conversion of Activated Alcohols into Oximes; Synthesis of Citaldoxime

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1291
McAllister, Graeme D.; Wilfred, Cecilia D.; Taylor, Richard J. K.:
Tandem Oxidation Processes: The Direct Conversion of Activated Alcohols into Nitriles

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1293
Foot, Jonathan S.; Kanno, Hisashi; Giblin, Gerard M. P.; Taylor, Richard J. K.:
Tandem Oxidation Processes: The Direct Conversion of Activated Alcohols into Esters and Amides

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1296
Ishihara, Kazuaki; Hasegawa, Aiko; Yamamoto, Hisashi:
Single-Pass Reaction Column System with Super Brønsted Acid-loaded Resin

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1299
Ishihara, Kazuaki; Hasegawa, Aiko; Yamamoto, Hisashi:
A Fluorous Super Brønsted Acid Catalyst: Application to Fluorous Catalysis without Fluorous Solvents

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1302
Bach, Thorsten; Lemarchand, Aude:
Synthesis of Ansa-Bridged Macrocyclic Lactams Related to the Antitumor Antibiotic Geldanamycin by Ring Closing Metathesis

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1305
Bach, Thorsten; Spiegel, Anja:
Stereoselective Total Synthesis of the Tricyclic Sesquiterpene (±)-Kelsoene by an Intramolecular Cu(I)-Catalyzed [2+2]-Photocycloaddition Reaction

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1308
Paintner, Franz F.; Allmendinger, Lars; Bauschke, Gerd; Polborn, Kurt:
Synthetic Studies Toward Tetrodecamycin: An Efficient Approach to the Core Structure of the Antibiotic

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1313
Sergeyev, Sergey; Hesse, Manfred:
A New Convenient Method for the Preparation of Enamides from N-Allylamides

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1318
Brimble, Margaret A.; Davey, Roger M.; McLeod, Malcolm D.:
Synthesis of Azido Analogues of Medermycin

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1323
Itoh, Tetsuji; Watanabe, Manabu; Fukuyama, Tohru:
Synthetic Approach to Tetrodotoxin

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1326
Miyawaki, Kazuhiro; Takagi, Toshiyuki; Shibakami, Motonari:
Efficient Synthesis of Parallel Cyclobolaphiles Having Two Diacetylenes: Mimetics of Archaeal Membrane Lipids

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1329
Ito, Masato; Shirakawa, Eiji; Takaya, Hidemasa:
Generation of Silylethynolates via C-Si Bond Cleavage of Disilylketenes Induced by t-BuOK

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1332
Hughes, David D.; Bagley, Mark C.:
One or Two-Step Bohlmann-Rahtz Heteroannulation of 6-Aminouracil Derivatives for the Synthesis of Pyrido[2,3-d]pyrimidines

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1335
Stefani, Hélio A.; Menezes, Paulo H.; Costa, Iguatemi M.; Silva, Diogo O.; Petragnani, Nicola:
Use of Chiral Sulfoxide in the Asymmetric Synthesis of (+)-Virol C

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1338
Kan, Toshiyuki; Kobayashi, Hideki; Fukuyama, Tohru:
Highly Versatile Synthesis of Polyamines by Ns-strategy on a Novel Trityl Chloride Resin

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1341
Shinada, Tetsuro; Fuji, Toshiyuki; Ohtani, Yasuhiro; Yoshida, Yasutaka; Ohfune, Yasufumi:
Syntheses of Gabosine A, B, D, and E from Allyl Sulfide Derived from(-)-Quinic Acid

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1344
Tamura, Osamu; Toyao, Atsushi; Ishibashi, Hiroyuki:
TBAT-Mediated Nitrone Formation of ω-Mesyloxy-O-tert-butyldiphenylsilyl-oximes: Facile Synthesis of Cyclic Nitrones from Hemiacetals

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1347
Saidi, Mohammad R.; Azizi, Najmedin:
A New Protocol for a One-pot Synthesis of α-Amino Phosphonates by Reaction of Imines Prepared In Situ with Trialkylphosphites

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1350
Pauvert, Mickaël; Dupont, Virginie; Guingant, André:
A Facile Access to the 1,5-Dihydro- and 1,3,4,5-Tetrahydro-benzo[b]azepin-2-one Ring Systems via a New Ring Enlargement

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1353
Shen, Yongcun; Feng, Xiaoming; Zhang, Guolin; Jiang, Yaozhong:
Asymmetric Cyanosilylation of Ketones Catalyzed by Chiral N-Oxide-titanium (IV) Complex

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1356
Blanchard, Stéphanie; Rodriguez, Ivan; Caubère, Paul; Guillaumet, Gérald:
Metallation and Functionalisation of Dihydrodipyridopyrazines

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1359
Lemaire, Marielle; Veny, Nicolas; Gefflaut, Thierry; Gallienne, Estelle; Chênevert, Robert; Bolte, Jean:
First Stereocontrolled Reduction of Isoxazoline by Hydrogenolysis: A New Route to Iminosugars via Cyclic Sulfates

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1362
Voigt, Tobias; Winsel, Harald; de Meijere, Armin:
Easy Access to (n+3)-Dimethylamino-1-ethenylbicyclo[n.1.0]alkanes and their Facile Conversion to Ring-annelated Cyclopentadienes

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1365
García-Martínez, Joaquín C.:
DABdendr as a Building Block
FREE ACCESS

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1368
Fischer, Fabian:
3-Mercaptopropionic Acid (3-MPA)
FREE ACCESS

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PDF (155 kb)