Synfacts

Issue 05 · May 2012

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A41
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Synthesis of Olopatidine Hydrochloride

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Formal Synthesis of Aspergillide B

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Synthesis of Zanamivir

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Synthesis of Lobucavir

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Synthesis of (+)-Ambuic Acid

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Synthesis of (±)-Trigonoliimine B

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Synthesis of the Amathaspiramides

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Synthesis of (±)-Janoxepin

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Synthesis of MK-7246

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Synthesis of (+)-Cyperolone

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Synthesis of A-315675

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Synthesis of Heterocycles
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0481
Cu-Catalyzed Synthesis of Indolizines

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Pd-Catalyzed Heteroannulative Route to Isocoumarins

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0483
Synthesis of Oxindoles via Intramolecular Enantioselective α-Arylation

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0484
Efficient Stereoselective Synthesis of Tricyclic Chromenoisoxazolines

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Diastereoselective Rh-Catalyzed Cascade Affording Piperidine Derivatives

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Dearomatizative Intramolecular 1,3-Dipolar Cycloaddition of Nitrile N-Oxides

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0487
Gold-Catalyzed Asymmetric Heteroannulation Route to Isochromenes

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0488
Convergent Domino Oxidation for Oxazole Synthesis

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0489
Cu-Catalyzed Synthesis of Imidazopyridines from 2-Aminopyridines and Nitroolefins

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0490
Substituted Pyrroles via Rh-Catalyzed Rearrangement of α-Diazo Oxime Ethers

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0491
Five-, Six- and Seven-Membered N-Hetero-cycles via Pd(II)-Catalyzed Hydroamination

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0492
Three-Component Synthesis of Pyrido[2,1-d]-[1,2,5]triazepines

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0493
Pd-Catalyzed C(sp³)–H Activation Route to Oxindoles

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0494
Rhodium-Catalyzed Intramolecular [2+2+2] Cycloaddition to Planar-Chiral Cyclophanes

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0495
Pd-Catalyzed C–H Activation–Carboamination Route to Phenanthridines

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Synthesis of Materials and Unnatural Products
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0497
NH-π(C≡C) Hydrogen Bonding in BN-Doped Tolans

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Near-Infrared Dye

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0499
Direct C–H Arylation

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0500
Cooling Ketene Generation in Meldrum’s Acid Derivatives

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0501
Increasing π-Conjugation Length via Protonation

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0502
Building a Bigger Azaacene

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0503
Pyridone Derivatives of Large Azaacenes

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0504
Halogen Templation of Catenanes for Anion Binding

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0505
Tunable Catalysts for Polymerizations under Visible Lights

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0506
Synthesis of the Smallest Nanohoop

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0507
Stereoselective After Initiation

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0508
A Route to Oxoverdazyl Radicals without Phosgene or Hydrazine

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0509
7,8,15,16-Tetraazaterrylene. It’s as Simple as One, Two, Three FREE ACCESS

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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0511
Asymmetric Synthesis of Indolines by Pd-Catalyzed C(sp³)–H Activation FREE ACCESS

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0512
Cu-Catalyzed Alkylation of β-Keto Esters and Cyclization to Spirolactones

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0513
Nickel-Catalyzed Enantioselective Synthesis of Benzobicyclo[2.2.2]octenes FREE ACCESS

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0514
Pd(II)-Catalyzed anti-Diamination of Acrylates Using Sulfamates

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0515
Asymmetric Reactions with Diamidophosphite Ligands

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0516
Ruthenium-Catalyzed Asymmetric Addition of Boronic Acids to Glyoxylates

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0517
Alkali Base Promoted Cascade Synthesis of Tricyclic Structures

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0518
Asymmetric [3+2] Cycloaddition of α-Imino Amides with Activated Olefins

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0519
Ruthenium NHC Catalyzed Highly Enantio-selective Hydrogenation of Benzofurans

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0520
Palladium-Catalyzed Asymmetric α-Arylation of Ketones

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0521
Rh(I)-Catalyzed Asymmetric Hydrogenation of Tetrasubstituted Enones

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0522
Stereoselective Rhodium-Catalyzed Ene-Cycloisomerizations

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0523
Enantioselective Cyclizations of Silyloxyenynes

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0524
Photocatalyzed [2+2] Cycloadditions of Enones with Redox Auxiliaries

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0525
Enantioselective Hydrocyanation of N-Protected Aldimines

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0526
Novel Cooperative Catalyst for anti-Selective Henry Reactions

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0527
Iridium-Catalyzed Domino Alkene-Isomerization–Claisen Rearrangement

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0528
Rh-Catalyzed Three-Component Tandem Reaction to Pyrrolidines

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0529
Catalytic Asymmetric Allylic Dearomatization of Indoles

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0530
Iron-Catalyzed Enantioselective Mukaiyama Aldol Reaction

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0531
Synthesis of Branched Aldehydes via Asymmetric Hydroformylation

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0532
Ruthenium-Catalyzed Asymmetric Transfer Hydrogenation

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0533
Palladium-Catalyzed Enantioselective Saucy–Marbet Claisen Rearrangement

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0534
Rhodium-Catalyzed Alkyne Carbothiolations

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0535
Palladium-Catalyzed Oxidative Oxyarylation

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0536
Copper-Catalyzed Desymmetrization of 1,3-Diols

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0537
Rhodium(II)-Catalyzed Asymmetric Sulfur(VI) Reduction

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0538
Enantioselective Reduction of Carbonyl Ylides via Relay Catalysis

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0539
Nickel-Catalyzed Reductive Coupling of Norbornene with Aldehydes

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0540
Synthesis of Spirocyclic Rings via Pd-Catalyzed Allylic C–H Activation

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Metal-Mediated Synthesis
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0541
Synthesis of Ketones and Ketimines via Organometallics and Secondary Amides FREE ACCESS

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0542
Synthesis of Thiopyrans Using a Sulfur-Enabled Anionic Cascade

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0543
Cu-Catalyzed Intermolecular Ritter-Type C–H Amination

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0544
[1,5]-Anion Relay–[2,3]-Wittig Rearrange- ment to Yield Vinyl Bis(silane) Products

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0545
Bismuth-Mediated Diastereoselective Construction of syn-1,3-Dioxanes

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0546
Controlled Diastereoselectivity in Aldehyde Crossed-Aldol Reactions

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0547
Enantioselective Zn-Catalyzed Alkynylation of α-Amido Sulfones

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0548
Ni-Catalyzed Enantioselective Cross-Coupling of Propargylic Carbonates

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0549
Pd-Catalyzed Synthesis of δ-Bromo γ,δ-Unsaturated Carbonyl Compounds

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0550
Enantioselective Chiral Brønsted Acid Catalyzed Propargylation of Aldehydes

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0551
SmI₂-Mediated Diastereoselective Cross-Coupling to Yield β-Silyl Lactams

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0552
Iron-Catalyzed Cross-Coupling of Chloroalkanes with Aryl Grignards

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0553
Regio- and Stereoselective Ru(II)-Catalyzed ortho-Alkenylation of Aldehydes

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0554
Copper-Mediated Cyanation of Aryl C–B and Arene C–H Bonds

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0555
Cu-Catalyzed Asymmetric Allylic Alkylation with Organolithium Reagents

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Organo- and Biocatalysis
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0557
Primary Amine Catalyzed Hajos–Parrish–Eder–Sauer–Wiechert Reactions

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0558
Catalytic Asymmetric Synthesis of Dihydropyridones

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0559
Lewis Base Catalyzed Vinylogous Adol Reaction

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0560
Organocatalytic Multicomponent Approach towards Pyrroloisoquinolines

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0561
Catalytic Asymmetric One-Pot Synthesis of γ-Nitroesters

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0562
Asymmetric Synthesis of Spirooxindole-Tetrahydrothiophenes

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0563
Asymmetric [4+1] Annulation of Sulfur Yildes and Nitroolefins

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0564
N-Heterocyclic Carbene Catalyzed Internal Redox Reaction of Alkynals

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0565
Catalytic Asymmetric Diels–Alder Reaction with 2,4-Dienones

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0566
High-Pressure Accelerated Friedel–Crafts Alkylation of Indoles with Enones

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0567
Asymmetric Cyclization of Aldehydes with γ-Hydroxy Enones

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0568
Brønsted Acid Catalyzed Oxysulfenylation and Oxyselenenylation

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Polymer-Supported Synthesis
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0569
Polymeric Imidazole Pd Catalyst for Cross-Couplings FREE ACCESS

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0570
Hydrogen Transfer Reductive N-Alkylation with Alcohols by Pd/C/Zn

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0571
Diaryl Ketone as a Traceless Linker for SPS of Arylthiophenes

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0572
Cyanosilylation of Carbonyls and Imines with PS-TBD

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0573
Oxidation of Alcohols with Heterogeneous Hypervalent Iodines

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0574
The Suzuki–Miyaura Coupling Using a Rasta Resin Supported Pd Catalyst

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0575
Transformation of Primary Amines to Amides with MnO₂-Based OMS-2

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0576
Nitro-Michael Addition Using Polymer-Supported Bifunctional Catalysts

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0577
Oxidation of Silanes to Silanols with H₂O Using a Nano-Pd Catalyst

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0578
Preparation of gem-Dihydroperoxides with Fe₂O₃-Immobilized SiO₂-TfOH

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0579
C–S Coupling with a Nano-Fe-DOPA-Cu Catalyst

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0580
Asymmetric Dimerization of Ketenes with Heterogeneous Organocatalysts

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0581
Aerobic Oxidation of Alcohols with a Pd Complex Immobilized on SBA-15

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