Synlett

Issue 01 · January 2006

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Hodgson, David M.; Bray, Christopher D.; Humphreys, Philip G.:
Expanding the Utility of Lithiated Epoxides and Aziridines in Synthesis

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0023
Spino, Claude:
The Ever-Challenging Quassinoids

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0033
Kramer, Rainer; Brückner, Reinhard:
Desymmetrizing Asymmetric Epoxidations of Bis(cis-configured) Divinylcarbinols: Unusual syn-Selectivity Combined with ee-Enhancement through Kinetic Resolution

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0039
Wojczykowski, Klaus; Jutzi, Peter:
Amphiphilic Trithiols RC(CH₂SH)₃

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0041
Berkessel, Albrecht; Mukherjee, Santanu; Lex, Johann:
Reversal of Enantioselectivity by Catalyst Protonation: Asymmetric Hydrocyanation of Imines with Oxazaborolidines

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0045
Vera-Ayoso, Yolanda; Borrachero, Pastora; Cabrera-Escribano, Francisca; Gómez-Guillén, Manuel; Vogel, Pierre:
A Novel Approach to the Synthesis of N-Substituted 1-C-Aminomethyl Glycofuranosides

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0049
Yin, Guodong; Wang, Zhiguo; Chen, Yunfeng; Wu, Anxin; Pan, Yuanjiang:
Synthesis of Novel Molecular Clips Based on Diethoxycarbonyl Glycoluril

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0053
Cailly, Thomas; Fabis, Frédéric; Bouillon, Alexandre; Lemaître, Stéphane; Sopkova, Jana; de Santos, Olivieira; Rault, Sylvain:
Synthesis of ortho-Cyanopyridylboronic Acids and Esters toward Cyano-Functionalized Bipyridines

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0057
Ménard, Delphine; Vidal, Anne; Barthomeuf, Chantal; Lebreton, Jacques; Gosselin, Pascal:
Mercuric Triflate·(TMU)₂ Catalyzed Cyclization of a Propargylic Ketone into a Monosubstituted Furan

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0061
Kim, Young-Ju; Tae, Jinsung:
Resolution of 2-Silyloxy-1-oxiranyl-4-pentenes by HKR: Total Synthesis of (5S,7R)-Kurzilactone

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0065
Lee, Jae Hak; Lee, Byoung Se; Shin, Hyunik; Nam, Do Hyun; Chi, Dae Yoon:
Acetonitrile-Mediated Synthesis of 2,4-Dichloroquinoline from 2-Ethynylaniline and 2,4-Dichloroquinazoline from Anthranilonitrile

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0069
Kashiwagi, Yoshitomo; Ikezoe, Hiroshi; Ono, Tetsuya:
Oxidation of Alcohols with Nitroxyl Radical Resins under Two-Phase Conditions

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0073
Abbiati, Giorgio; Beccalli, Egle; Broggini, Gianluigi; Martinelli, Michela; Paladino, Giuseppe:
Pd-Catalyzed Cyclization of 1-Allyl-2-indolecarboxamides by Intramolecular Amidation of Unactivated Ethylenic Bond

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0077
Richardson, Robert D.; Hernandez-Juan, Felix A.; Dixon, Darren J.:
Pyrrolate-Catalyzed Conjugate Addition of Pyrrole to Electron-Deficient Alkenes

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0081
Dixon, Darren J.; Richardson, Robert D.:
Enantioselective Brønsted Acid Catalyzed Conjugate Addition of Aryl Methyl Ketone Derived Enamines to Nitroalkenes

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0086
Jung, Doo Young; Kang, Sol; Chang, Sukbok; Kim, Yong Hae:
Efficient Enantioselective Synthesis of α-Hydroxy-β-amino Acids Using the Claisen and Curtius Rearrangements

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0091
Sridharan, Vellaisamy; Perumal, Subbu; Avendaño, Carmen; Menéndez, J. Carlos:
Microwave-Assisted, Solvent-Free Bischler Indole Synthesis

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0096
Zhao, Jun-Ling; Liu, Li; Zhang, Hai-Bo; Wu, Yan-Chao; Wang, Dong; Chen, Yong-Jun:
Three-Component Friedel-Crafts Reaction of Indoles, Glyoxylate, and Amine under Solvent-Free and Catalyst-Free Conditions - Synthesis of (3-Indolyl)glycine Derivatives

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0101
Coumbarides, Gregory S.; Dingjan, Marco; Eames, Jason; Flinn, Anthony; Motevalli, Majid; Northen, Julian; Yohannes, Yonas:
Efficient Parallel Resolution of Racemic Evans’ Oxazolidinones Using quasi-Enantiomeric Profens

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0106
Rössle, Michael; Christoffers, Jens:
Access to Eight-Membered Ring Lactams from Five-Membered Ring 1,4-Diketones and Primary Amines

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0109
Nishiyama, Yutaka; Fujimoto, Mayu; Sonoda, Noboru:
A New Method for the Synthesis of 2-Aryl-1H-benzimidazoles: Selenium-Catalyzed Reductive N-Heterocyclization of Benzylidene(2-nitroaryl)amines with Carbon Monoxide

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0112
Iwanami, Katsuyuki; Oriyama, Takeshi:
A New and Efficient Method for the Trifluoromethylation of Carbonyl Compounds with Trifluoromethyltrimethylsilane in DMSO

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0115
Kitamura, Yuki; Hashimoto, Ayano; Yoshikawa, Seiji; Odaira, Jun-ichi; Furuta, Takumi; Kan, Toshiyuki; Tanaka, Kiyoshi:
Synthesis of Novel Phenylnaphthyl Phosphines and their Applications to Pd-Catalyzed Intramolecular Amidation

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0118
Murata, Miki; Yoshida, Syo; Nirei, Shin-ichiro; Watanabe, Shinji; Masuda, Yuzuru:
An Efficient Catalyst System for Palladium(0)-Catalyzed Cross-Coupling of Aryltrialkoxysilanes with Aryl Halides

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PDF (72 kb)
0121
Körner, Marleen; Hiersemann, Martin:
The Catalytic Asymmetric Claisen Rearrangement (CAC) in Natural Product Synthesis: Synthetic Studies toward Curvicollides A-C

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0124
Komiyama, Takuzo; Takaguchi, Yutaka; Tsuboi, Sadao:
Synthesis of Anthraquinone Derivatives: Tandem Diels-Alder-Decarboxylation-Oxidation Reaction of 3-Hydroxy-2-pyrone with 1,4-Naphthoquinone

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cluster
0129
Katayama, Mayumi; Nagase, Ryohei; Mitarai, Kumi; Misaki, Tomonori; Tanabe, Yoo:
Isolation of Intermediary anti-Aldol Adducts of the Horner-Wadsworth-Emmons Reaction Utilizing Direct Titanium-Aldol Addition and Successive Brønsted Acid Promoted Stereoselective Elimination Leading to (Z)-α,β-Unsaturated Esters

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0133
Terada, Masahiro; Sorimachi, Keiichi; Uraguchi, Daisuke:
Phosphorodiamidic Acid as a Novel Structural Motif of Brønsted Acid Catalysts for Direct Mannich Reaction of N-Acyl Imines with 1,3-Dicarbonyl Compounds

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0137
Xu, Xuenong; Yabuta, Takaya; Yuan, Pei; Takemoto, Yoshiji:
Organocatalytic Enantioselective Hydrazination of 1,3-Dicarbonyl Compounds: Asymmetric Synthesis of α,α-Disubstituted α-Amino Acids

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0141
Akiyama, Takahiko; Tamura, Yukio; Itoh, Junji; Morita, Hisashi; Fuchibe, Kohei:
Enantioselective Aza-Diels-Alder Reaction Catalyzed by a Chiral Brønsted Acid: Effect of the Additive on the Enantioselectivity

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0144
Sohtome, Yoshihiro; Takemura, Nobuko; Iguchi, Toshitsugu; Hashimoto, Yuichi; Nagasawa, Kazuo:
Diastereoselective Henry Reaction Catalyzed by Guanidine-Thiourea Bifunctional Organocatalyst

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0147
Hess, Abram S.; Yoder, Ryan A.; Johnston, Jeffrey N.:
Chiral Proton Catalysis: pK_a Determination for a BAM-HX Brønsted Acid

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0150
Nakashima, Daisuke; Yamamoto, Hisashi:
Titanium Tetrachloride and Chiral Aliphatic Alcohol as a New Lewis Acid Assisted Chiral Brønsted Acid for the Enantioselective Protonation of Silyl Enol Ether

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0153
Bernardi, Dan:
Sodium Nitrite (NaNO₂)
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0155
Siddiqui, Shafi A.:
N-Alkylimidazolium Tetrafluoroborate
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Synlett

Editorial

Expanding the Utility of Lithiated Epoxides and Aziridines in Synthesis

The Ever-Challenging Quassinoids

Desymmetrizing Asymmetric Epoxidations of Bis(cis-configured) Divinylcarbinols: Unusual syn-Selectivity Combined with ee-Enhancement through Kinetic Resolution

Amphiphilic Trithiols RC(CH₂SH)₃

Reversal of Enantioselectivity by Catalyst Protonation: Asymmetric Hydrocyanation of Imines with Oxazaborolidines

A Novel Approach to the Synthesis of N-Substituted 1-C-Aminomethyl Glycofuranosides

Synthesis of Novel Molecular Clips Based on Diethoxycarbonyl Glycoluril

Synthesis of ortho-Cyanopyridylboronic Acids and Esters toward Cyano-Functionalized Bipyridines

Mercuric Triflate·(TMU)₂ Catalyzed Cyclization of a Propargylic Ketone into a Monosubstituted Furan

Resolution of 2-Silyloxy-1-oxiranyl-4-pentenes by HKR: Total Synthesis of (5S,7R)-Kurzilactone

Acetonitrile-Mediated Synthesis of 2,4-Dichloroquinoline from 2-Ethynylaniline and 2,4-Dichloroquinazoline from Anthranilonitrile

Oxidation of Alcohols with Nitroxyl Radical Resins under Two-Phase Conditions

Pd-Catalyzed Cyclization of 1-Allyl-2-indolecarboxamides by Intramolecular Amidation of Unactivated Ethylenic Bond

Pyrrolate-Catalyzed Conjugate Addition of Pyrrole to Electron-Deficient Alkenes

Enantioselective Brønsted Acid Catalyzed Conjugate Addition of Aryl Methyl Ketone Derived Enamines to Nitroalkenes

Efficient Enantioselective Synthesis of α-Hydroxy-β-amino Acids Using the Claisen and Curtius Rearrangements

Microwave-Assisted, Solvent-Free Bischler Indole Synthesis

Three-Component Friedel-Crafts Reaction of Indoles, Glyoxylate, and Amine under Solvent-Free and Catalyst-Free Conditions - Synthesis of (3-Indolyl)glycine Derivatives

Efficient Parallel Resolution of Racemic Evans’ Oxazolidinones Using quasi-Enantiomeric Profens

Access to Eight-Membered Ring Lactams from Five-Membered Ring 1,4-Diketones and Primary Amines

A New Method for the Synthesis of 2-Aryl-1H-benzimidazoles: Selenium-Catalyzed Reductive N-Heterocyclization of Benzylidene(2-nitroaryl)amines with Carbon Monoxide

A New and Efficient Method for the Trifluoromethylation of Carbonyl Compounds with Trifluoromethyltrimethylsilane in DMSO

Synthesis of Novel Phenylnaphthyl Phosphines and their Applications to Pd-Catalyzed Intramolecular Amidation

An Efficient Catalyst System for Palladium(0)-Catalyzed Cross-Coupling of Aryltrialkoxysilanes with Aryl Halides

The Catalytic Asymmetric Claisen Rearrangement (CAC) in Natural Product Synthesis: Synthetic Studies toward Curvicollides A-C

Synthesis of Anthraquinone Derivatives: Tandem Diels-Alder-Decarboxylation-Oxidation Reaction of 3-Hydroxy-2-pyrone with 1,4-Naphthoquinone

Isolation of Intermediary anti-Aldol Adducts of the Horner-Wadsworth-Emmons Reaction Utilizing Direct Titanium-Aldol Addition and Successive Brønsted Acid Promoted Stereoselective Elimination Leading to (Z)-α,β-Unsaturated Esters

Phosphorodiamidic Acid as a Novel Structural Motif of Brønsted Acid Catalysts for Direct Mannich Reaction of N-Acyl Imines with 1,3-Dicarbonyl Compounds

Organocatalytic Enantioselective Hydrazination of 1,3-Dicarbonyl Compounds: Asymmetric Synthesis of α,α-Disubstituted α-Amino Acids

Enantioselective Aza-Diels-Alder Reaction Catalyzed by a Chiral Brønsted Acid: Effect of the Additive on the Enantioselectivity

Diastereoselective Henry Reaction Catalyzed by Guanidine-Thiourea Bifunctional Organocatalyst

Chiral Proton Catalysis: pK_a Determination for a BAM-HX Brønsted Acid

Titanium Tetrachloride and Chiral Aliphatic Alcohol as a New Lewis Acid Assisted Chiral Brønsted Acid for the Enantioselective Protonation of Silyl Enol Ether

Sodium Nitrite (NaNO₂)

N-Alkylimidazolium Tetrafluoroborate