Synfacts

Issue 11 · November 2014

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A143
SYNFORM ISSUE 2014/11
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Synthesis of Natural Products and Potential Drugs
z1117
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1117
Syntheses of (+)-Flabellidine and (–)-Lycodine
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1118
Synthesis of Fibrinolysis Inhibitor AZD6564

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1119
Synthesis of a CETP Inhibitor
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1120
Synthesis of (−)-Methyl Atisenoate and (−)-Isoatisine

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1121
Formal Synthesis of Rosuvastatin and Pitavastatin

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PDF (112 kb)
1122
Total Synthesis of Aspeverin

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PDF (113 kb)
1123
Synthesis of (–)-Lepistine

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PDF (107 kb)
1124
Synthesis of VX-787

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PDF (111 kb)
1125
Synthesis of Δ¹²-Prostaglandin J₃

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PDF (125 kb)
1126
Total Synthesis of Gymnothelignan N

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PDF (110 kb)
1127
Synthesis of (–)-Xanthatin

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PDF (111 kb)
1128
Synthesis of SGLT-2 Inhibitor Empagliflozin

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PDF (111 kb)
1129
Synthesis of Thrombin Inhibitor AZD8165

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Synthesis of Heterocycles
z1131
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PDF (331 kb)
1131
Spirocyclic and Ring-Expanded Fused Pyrazoles

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PDF (115 kb)
1132
Synthesis of Aminotriazoloazepinone-Containing Di- and Tripeptides

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PDF (108 kb)
1133
N-Aryl Heterocycles by Catalytic Photoredox Olefin Hydroamination

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PDF (112 kb)
1134
Synthesis of the SF₅ Analogue of Umemoto Salt

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PDF (108 kb)
1135
An Organocatalytic Cascade Route to Functionalized Azepines

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PDF (103 kb)
1136
Iron-Catalyzed Synthesis of Difluoromethylsulfonylated Oxindoles

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PDF (111 kb)
1137
Quinoxaline N-Oxides by Dehydrogenative N-Incorporation of Imines

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PDF (119 kb)
1138
Synthesis of Spiroaminals by Au/Sc Relay Catalysis

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PDF (105 kb)
1139
NHC-Promoted Annulation Approach to Pyranyl Aldehydes

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PDF (108 kb)
1140
C-8 Alkylation and Alkynylation of Quinoline N-Oxides by Rhodium Catalysis

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PDF (111 kb)
1141
Copper-Catalyzed Synthesis of Dibenzodiazepinones

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PDF (105 kb)
1142
Copper-Catalyzed Synthesis of Sulfonylated Oxindoles

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PDF (109 kb)
1143
Synthesis of Benzotriazoles from 2-(Arylamino)aryliminophosphoranes

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PDF (101 kb)
1144
Synthesis of Heterocycles by Palladium-Catalyzed Intramolecular C–H Amination

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PDF (114 kb)
1145
Three-Component Reaction Approach to Aminopyrazoles and Iminopyrimidines

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PDF (107 kb)
Synthesis of Materials and Unnatural Products
z1147
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PDF (323 kb)
1147
A Starphene is Born: Largest and Most Soluble to Date
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PDF (121 kb)
1148
Covalent Cage Construction via Alkyne Metathesis

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PDF (113 kb)
1149
Every Cloud Has a Silver(I) or Tetramethylammonium Lining

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PDF (104 kb)
1150
Iterative Benzannulation for Rapid Build-up of Congested Aromatic Systems

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PDF (100 kb)
1151
Playing Dominoes with Palladium: Synthesis of Biaryl Tertiary Amines

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PDF (108 kb)
1152
Rearrange Your Way to Tricyclic Heteroaromatics

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PDF (104 kb)
1153
Taming the Wild Terminal Aryl Alkyne for High-Yield Cross-Metathesis

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PDF (99 kb)
1154
Complex Polyphenylenes from Bromo-Oligophenylboronic Acids

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PDF (108 kb)
1155
Platinum(II)-Catalyzed Synthesis of Substituted Azulenes

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PDF (103 kb)
1156
The Road to Rotanes is Paved with Exocyclic Alkenes

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PDF (110 kb)
1157
Synthetic Strategy Toward Enantiopure Helicene Quinones

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PDF (112 kb)
1158
Nitrogen-Doped Zigzag-Edge Nanographenes

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PDF (115 kb)
Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z1159
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PDF (675 kb)
1159
Mannich–Cyclization Cascade Reaction Catalyzed by Squaramide/AgOAc

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1160
Asymmetric Hydrogenation of Sterically Hindered Enones

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1161
Asymmetric Synthesis of Tetrahydrofurans Bearing Multiple Stereocenters
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PDF (139 kb)
1162
Ruthenium-Catalyzed Synthesis of Enantioenriched γ-Substituted Lactones

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PDF (122 kb)
1163
Iridium-Mediated Asymmetric Synthesis of Branched Allylic Sulfilimines

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PDF (113 kb)
1164
Diastereoselective Cyanation and Trifluoromethylation of Ketimines

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PDF (113 kb)
1165
Palladium-Catalyzed Asymmetric Allyl–Aryl Cross-Coupling Using Allylboronates

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PDF (108 kb)
1166
Synthesis of (+)-Discodermolide via Borylation

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PDF (106 kb)
1167
Asymmetric Hydrogenation of α,β-Unsaturated Nitriles

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PDF (124 kb)
1168
Stereoselective Synthesis of cis-4-Aryl-cyclopent-2-en-1-ols

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PDF (111 kb)
1169
Enantioselective C–H Addition of Pyridines to Alkenes

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PDF (112 kb)
1170
Palladium-Catalyzed Stereoselective Cascade Reaction for a Planar Core Structure

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PDF (106 kb)
1171
Rhodium/Phosphoric Acid Co-Catalyzed Asymmetric Csp²–H Functionalization

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PDF (112 kb)
1172
Ruthenium-Catalyzed Cylization of Aromatic Nitriles with Alkenes

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PDF (111 kb)
1173
Pd/Cu-Catalyzed Alkynylative Ring Opening of Oxabenzonorbornadienes

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PDF (114 kb)
1174
Diastereoselective Amination of Alcohols Catalyzed by Ruthenium

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PDF (107 kb)
1175
Enantioselective Allyl–Allylsilane Cross-Coupling Catalyzed by Iridium
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PDF (131 kb)
1176
Intramolecular Ruthenium-Mediated trans-Selective Silylvinylation of Alkynes

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PDF (122 kb)
1177
Rhodium-Catalyzed Cyclopropanation of N-Enoxyphthalimides

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PDF (115 kb)
1178
Synergistic Catalysis for Asymmetric Cascade Transformations

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PDF (118 kb)
1179
Functionalized Azulenes via Rhodium-Mediated N-Sulfonylaminoalkenylation

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PDF (116 kb)
1180
Rhodium-Catalyzed Asymmetric Synthesis of Tetrahydroquinolines

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PDF (105 kb)
1181
Chiral Bicyclo[3,2,1]octanes via Domino Reaction

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PDF (113 kb)
1182
Asymmetric aza-Henry Reaction Catalyzed by Copper

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PDF (107 kb)
1183
Copper-Catalyzed Asymmetric Boron Conjugate Addition in Water

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PDF (104 kb)
1184
Palladium-Catalyzed Stereospecific C-3 Arylation of Proline Derivatives

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PDF (112 kb)
1185
Rhodium-Catalyzed Enantioselective Carbonyl–Ene Reaction

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PDF (109 kb)
1186
Asymmetric Nickel-Catalyzed Synthesis of Spiro[isoxazolin-3,3′-oxindoles]

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PDF (126 kb)
1187
Heterobimetallic Rare-Earth–Lithium Complexes for Asymmetric Epoxidations

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Metal-Mediated Synthesis
z1189
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PDF (336 kb)
1189
Synthesis of 2,3-Disubstituted Indoles from Isatins

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PDF (100 kb)
1190
γ-Selective Arylation of Zincated Boc-Allylamines

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PDF (115 kb)
1191
Ketones from Carbon Dioxide and Organolithium or Grignard Reagents
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PDF (124 kb)
1192
Carbolithiation of Chloro-Substituted Alkynes

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PDF (101 kb)
1193
Zinc-Catalyzed Synthesis of Aryl Boronates

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PDF (100 kb)
1194
Synthesis of Polysubstituted Phenanthridines

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PDF (100 kb)
1195
Trifluoromethylthiolation of Alcohols

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PDF (99 kb)
1196
Alkoxide-Promoted Deborylative Alkylation of Bis(boronates)

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PDF (103 kb)
1197
Indium-Mediated Intramolecular Allenylation of N-tert-Butanesulfinyl Imines

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PDF (104 kb)
1198
Copper-Mediated ortho-Nitration of Aromatic Amides

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PDF (111 kb)
1199
Cross-Coupling of N-Tosylaziridines with Organozinc Reagents

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PDF (106 kb)
1200
Nickel-Catalyzed Difluoroalkylation of Organoboronic Acids

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PDF (104 kb)
1201
Cross-Coupling Reactions of Diazo Compounds and Vinylboronic Acids

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PDF (100 kb)
1202
Copper(II)-Mediated Ortho C–H Alkynylation

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PDF (100 kb)
1203
Asymmetric Arylation of Cyclic N-Sulfonyl Ketimines

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PDF (110 kb)
Organo- and Biocatalysis
z1205
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PDF (320 kb)
1205
Organocatalytic Asymmetric Mannich Synthesis of α-Amino Esters

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PDF (122 kb)
1206
ω-Transaminase-Catalyzed Reductive Amination of Ketones

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PDF (123 kb)
1207
N-Heterocyclic Carbene Catalyzed Formal [3+2] Annulation of Enals

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PDF (113 kb)
1208
Kinetic Resolution of Axially Chiral Diols and Amino Alcohols

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PDF (116 kb)
1209
Kinetic Resolution of BINOL Derivative Catalyzed by Chiral DMAPs

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PDF (112 kb)
1210
Enantioselective Formation of All-Carbon Quaternary Stereocenters

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PDF (110 kb)
1211
Biocatalytic Oxidative Desymmetrization of Piperidine Carboxylates

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PDF (124 kb)
1212
Disulfonimide-Catalyzed Enantioselective Torgov Cyclization

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PDF (107 kb)
1213
Catalytic Asymmetric Synthesis of 4-Nitropyrazolidines

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PDF (108 kb)
1214
Asymmetric Synthesis of Pyrrolines Using Bicyclic Phosphine Catalysts

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PDF (114 kb)
1215
Enantioselective Route to Piperidines via Covalent Phosphoric Acid Catalysis

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PDF (117 kb)
1216
Desymmetrization of 1,3-Diols via Oxidative Cleavage of Benzylidene Acetals

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PDF (112 kb)
Polymer-Supported Synthesis
z1217
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PDF (399 kb)
1217
1,3-Addition of Silyl Enol Ethers to Nitrones Using Al-MCM-41

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PDF (106 kb)
1218
Allylation of Imines and Aldehydes Using Pd-POMs

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PDF (108 kb)
1219
An Organo Porous Polymer Catalyst for Asymmetric Alkylation with Et₂Zn
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PDF (137 kb)
1220
Selenophenes and Selanyl Selenophenes Using CuO Nanoparticles

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PDF (106 kb)
1221
C–C Cross-Couplings Using Triazole Dendrimer Stabilized Pd Nanoparticles

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PDF (112 kb)
1222
Co–Pd Magnetic Nanoparticle Catalyst for the Aerobic Oxidation of Alcohols

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PDF (103 kb)
1223
Oxidation of Alcohols Using CoFe₂O₄@APTES@Ni(OH)₂

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PDF (103 kb)
1224
Direct Glycosylation with Sc(OTf)₂-NSMP Catalyst in Water

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PDF (148 kb)
1225
Polymer-Incarcerated Gold Nanocluster Catalysts for Oxidation

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PDF (107 kb)
1226
Chemoselective Hydrogenation of Chloronitrobenzenes Using Pt/C

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PDF (99 kb)
1227
Deoxygenation of Sulfoxides Using Ruthenium Nanoparticles Supported on TiO₂

HTML

PDF (105 kb)
1228
O-Arylation of Phenols with Aryl Halides Using Cu/Nf–Graphene Nanoribbons

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PDF (103 kb)
1229
The Michael Addition of Aldehydes to Nitroalkenes with Carrageenan/MNPs

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PDF (114 kb)
1230
Solid-Phase Synthesis of 1,2,3-Triazoles Using 4,4′-Bismethoxybenzhydryl Azide

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PDF (127 kb)
1231
C(sp)–C(sp) and C(sp)–C(sp²) Cross-Coupling with CuFe₂O₄ Nanoparticles

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PDF (109 kb)

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