Synfacts

Ausgabe 03 · März 2020

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Ausgabe
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A31
SYNFORM ISSUE 2020/03

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Synthesis of Natural Products and Potential Drugs
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0245
Total Synthesis of Swinhoeisterol A, Dankasterones A and B, and Periconiastone A FREIER ZUGRIFF

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0246
Total Syntheses of (+)-Lyconadins D and E

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0247
Synthesis of a Macrocyclic Mcl-1 Inhibitor FREIER ZUGRIFF

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0248
Synthesis of d₉-Ivacaftor Using o-Quinone Methide Chemistry

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0249
Synthesis of Sonidegib Using Palladium Catalysis in Water

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0250
Synthesis of (–)-Oridonin

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0251
Synthesis of Taniborbactam

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0252
Synthesis of β-Lactamase Inhibitor Relebactam

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0253
Synthesis of (–)-Curvulamine

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0254
Synthesis of a Baloxavir Marboxil Fragment

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0255
Total Synthesis of (–)-PF-1018

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0256
Synthesis of O-GlcNAcase Inhibitor MK-8719

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0257
Synthesis of ERK1/2 Inhibitor AZD0364

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0258
Synthesis of AMG 510

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0259
Synthesis of Axelopran

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0260
Synthesis of (+)-Tronocarpine

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0261
Synthesis of (±)-Tetrodotoxin FREIER ZUGRIFF

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Synthesis of Heterocycles
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0263
One-Step Synthesis of 4-Fluoropyrimidines

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0264
Synthesis of Benzofuroindolines through Biocatalytic Oxidative Phenol–Indole [3+2] Reactions

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0265
Palladium-Catalyzed Ring Expansion for the Synthesis of 12-Membered Heterocycles

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0266
Synthesis of Butenolides from Functionalized Cyclopropenones

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0267
Electrochemical Synthesis of trans-2,3-Disubstituted Aziridines

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0268
Regioselective Synthesis of CF₂H-Containing Pyrazoles

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0269
Enantioenriched Dihydroquinolines by NHC Catalysis

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0270
Diastereoselective Cyclization of Oxime-Tethered Cyclopropanes to Pyrrolooxazines

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0271
Light-Mediated Dehydrogenative Povarov Reaction of Indoles and Benzofurans

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0272
Stereoselective and Regioselective Functionalization of Piperidines through C–H Activation

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0273
The N-Oxide Moiety as a Traceless Directing Group for Pyridine 2-C(O)–C Bond Activation

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0274
Asymmetric Palladium-Catalyzed Synthesis of Fluoropiperidines

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0275
Modified Pomeranz–Fritsch Reaction for the Synthesis of 1,2-Dihydroisoquinolines

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Synthesis of Materials and Unnatural Products
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0277
Dendralenes and Radialenes and Butadienes, Oh My!

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0278
Two ‘L’s are a Win for Fluorescent Helical Foldamers

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0279
Close to N-Doped Zigzag Carbon Nanobelts

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0280
A Palladium-Catalyzed Tandem Reaction to Construct bis-BN-Naphthalene-Fused Oxepins

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0281
Synthesis of Fold-Line-Shaped BN-Embedded Polycyclic Aromatic Hydrocarbons

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0282
Helical Nanographenes: Now with Azulene

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0283
Stereospecific PAH Synthesis with a Twist

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0284
Covalently Linked Dimers with Intramolecular Stacking

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0285
Gold-Digging Polythioamides via Sulfur, Acid and Amine Polymerization

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0286
Little PolyANIs

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0287
Supramolecular Pi

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0288
Oxygen/Sulfur Exchange in Epoxides to Make Poly(thioethers)

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Metals in Synthesis
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0289
Palladium-Catalyzed Dicarbonylation of 1,3-Dienes for the Synthesis of Adipic Acid Esters FREIER ZUGRIFF

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0290
Dual-Catalyzed 1,2-Difunctionalization of Vinyl Boronates

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0291
Synthesis of C-Alkyl Glycoamino Acids via Palladium-Catalyzed C(sp³)–H Glycosylation FREIER ZUGRIFF

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0292
Nickel-Catalyzed Hydroalkylation of Olefins

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0293
Iron-Electrocatalyzed C–H Arylations

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0294
Synthesis of Acylsilanes via Carbonylative Silylation of Alkyl Halides Using Copper Catalysis

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0295
Reduction of Amides and Esters with Borane Dimethyl Sulfide Complex

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0296
Hydroamination of Olefins

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0297
Hydroamination of Cyclobutenes and Cyclopropenes

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0298
Highly Selective Rhodium-Catalyzed Tandem Spirocyclization/Reduction of 3‑Allenylindoles

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0299
Enantioselective Rhodium-Catalyzed C–H Borylation of N-Alkylamines and Amides

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0300
Dual Photoredox/Nickel-Catalyzed Preparation of Aryl Aminooxetanes

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0301
Nickel/Photoredox Dual Catalysis Mediated Dicarbofunctionalization of Olefines

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0302
Iron-Catalyzed Allylic and Propargylic C–H Functionalization for the Formation of C–C Bonds

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0303
Enantioselective C(sp³)–H Amidation under Rhodium Catalysis

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0304
Conjunctive Cross-Coupling of Vinyl Boronic Esters

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0305
[4+2] Cycloaddition of Dienes with Vinylcarbenes

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0306
A New para-Selective Difluoroalkylation

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0307
Regioselective Aziridine Opening

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0308
Nickel-Catalyzed Synthesis of Homoallylic Alcohols under Photoredox Conditions

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0309
Thiiranes and Thiethane Oxyalkynylation through a Copper-Catalyzed Ring Opening

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0310
Enantioselective Pd-Catalyzed Desymmetrization of Cyclohexanones: γ‑All-Carbon Quaternary Centers

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0311
Palladium-Catalyzed Dearomative [2+2+1] Spiroannulation through Alkyne-Directed C–H Activation

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0312
Enantioselective Rhodium-Catalyzed Dearomatization of Pyridinium Salts

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0313
Photoredox- and Cobalt-Catalyzed Intermolecular Reductive Ene-Yne Coupling

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0314
The Stille Carbonylative Cross-Coupling Reaction FREIER ZUGRIFF

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0315
Directed Metalation Using TMP₂AgCNLi₂

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0316
Difluoromethylation of Benzylic C–H Bonds via Copper Catalysis

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Polymer-Supported Synthesis
z0317
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0317
Shape-Selective Hydrogenation of Nitroarenes by Using Zeolite-Encaged Single-Atom Rhodium Catalysts FREIER ZUGRIFF

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0318
Synthesis of Chromenopyrimidines on Cobalt Oxide–Nickel Oxide–Sulfonated Graphene Quantum Dots

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0319
Oxygenation of Olefins with N-Doped Carbon-Incarcerated Cobalt Nanoparticles

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0320
Dehydrogenation and Hydrogen-Borrowing Reactions with a P-Doped Polymer-Supported Iridium Catalyst

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0321
Photodehydrogenation of N-Heterocycles on Nickel(II)-Grafted Titanium Dioxide

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0322
Palladium Nanoparticle Catalyzed Suzuki–Miyaura Cross-Coupling under Ultrasonic Irradiation

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0323
Micellar Cross-Coupling of Aryl Halides with N-Tosylhydrazones Catalyzed by Palladium Nanoparticles

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0324
Synthesis of Chromeno[b]pyridines under Ultrasonic Irradiation using TiO₂ NPs on Carbon Nanotubes

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0325
Photoinduced Aerobic C–C Coupling of Xanthenes on Sulfated Carbon Dots

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0326
Continuous-Flow Asymmetric Transfer Hydrogenation of Acetophenones with Propan-2-ol

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0327
Silica-Supported Manganese(II) Catalyst for Carbonyl Hydrosilylation, Hydroboration, and Transesterification

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0328
One-Pot Synthesis of Propargylamines on a Zinc Chloride Loaded Titania Catalyst

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0329
Cycloaddition of Carbon Dioxide to Epoxides on a Hollow Zn–Co Based Zeolitic Imidazole Framework

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Organo- and Biocatalysis
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0331
Foldamer-Catalyzed Macrocyclizations FREIER ZUGRIFF

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0332
Lewis-Basic Peptide-Catalyzed Coupling of Naphthols and Quinones to Non-C₂-Symmetric Biaryls

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0333
Efficient Enzymatic Cascade for the Biosynthesis of Islatravir

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0334
Decarboxylative C(sp³)–X (X = O, NBoc, S) Bond Formation through Photoredox Catalysis

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0335
Methyl Triptycen-1-yl Sulfide Catalyzed Electrophilic Aromatic Halogenation with N-Halosuccinimides

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0336
NHC Catalysis Enables a Practical and General Organocatalytic Approach to C1-Deuterated Aldehydes

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0337
Asymmetric Counteranion-Directed Catalysis Meets Supramolecular Chemistry

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0338
Chiral Acyl Azolium Permits Dynamic Kinetic Resolution of Hydroxyphthalides

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0339
Biocatalytic Cascade Reduction of Cyclic Enimines

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0340
Nitrenium Salts as Hydrogen-Transfer Catalysts

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Chemistry in Medicine and Biology
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0341
A Repurposed Chemotherapy Drug as C1 Synthon FREIER ZUGRIFF

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0342
Permeable and Fluorogenic Nanoscopy Probes

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0343
A Highly Selective Inhibitor of TBK1/IKKε

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0344
Cell-Type-Specific Voltage Imaging Using Covalently Tethered Fluorophores

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0345
A Versatile Cellular Target Engagement Probe for MPC2

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0346
Natural PDE4 Inhibitor Toddacoumalone

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0347
Bioinspired Nucleobase Caging

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0348
Investigating TRPA1 Modulation with Noncovalent Piperidine Carboxamide Based Binders

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0349
Staudinger Reduction-Activated Lysine for the Control of Protein Subcellular Localization and SUMOylation

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0350
Total Synthesis of a Gene FREIER ZUGRIFF

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Peptide Chemistry
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0351
Cyclic Peptides Synthesis with the Assistance of a Removable Activating Group FREIER ZUGRIFF

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0352
Synthesis of syn-α,β-Diamino Esters through an Asymmetric Mannich Reaction

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0353
Chiral Ammonium Salt Phase-Transfer-Catalyzed Synthesis of Quaternary β^2,2-Amino Acids

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0354
Hydroperoxide-Mediated Decarboxylative Acylation of Amines with α-Keto Acids

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0355
Metal-Free Photochemical Synthesis of α-Amino Acid Derivatives

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0356
Synthesis of α-Amino Acid Derivatives from Amines

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0357
Synthesis of C-Terminal Glycopeptides

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0358
Heterogeneous Catalysis for Amide Bond Formation

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0359
Photocatalytic Amide-Bond Formation

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0360
Enantioselective Synthesis of α-Aryl-β-amino Acids from N-Boc Imines and Homophthalic Anhydrides

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0361
Rhodium-Catalyzed Synthesis of α-Amino Acid Derivatives

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0362
Synthesis of α-Amino Acids by One-Pot Oxidation and Transamination of 1,2-Diols

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0363
Chlorofusin Cyclic Peptide Synthesis FREIER ZUGRIFF

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Flow Chemistry
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0365
Heterogeneous Catalysis in Continuous Flow

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0366
Organocatalyzed Rauhut–Currier and [3+2] Annulation Domino Reaction under Flow Conditions

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0367
Functionalized Aryl Azides through Aryllithium Generation in Flow

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0368
Continuous Palladium-Catalyzed Carbonylative Cyclization Using Iron Pentacarbonyl as a CO Source

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Addendum
0370
Enzyme-Catalyzed Site-Selective C–H Amidation

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