Synfacts

Ausgabe 04 · April 2021

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A49
SYNFORM ISSUE 2021/04
FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
z0363
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PDF (473 kb)
0363
Total Synthesis of (+)-Peniciketal A
FREIER ZUGRIFF

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0364
Total Synthesis of (+)-Mycinolide IV

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PDF (87 kb)
0365
Synthesis of PF-07059013
FREIER ZUGRIFF

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PDF (132 kb)
0366
Synthesis of ent-Plagiochianin B

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PDF (107 kb)
0367
Synthesis of (–)-Dehydrocostus Lactone

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PDF (86 kb)
0368
Synthesis of Eldecalcitol

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PDF (91 kb)
0369
Synthesis of PF-06843195

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0370
Synthesis of DS79932728

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0371
Synthesis of Ceralasertib

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0372
Synthesis of (–)-Euonyminol

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0373
Total Synthesis of (±)-Longifolene
FREIER ZUGRIFF

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0374
Total Synthesis of (+)-Punicafolin and (+)-Macaranganin

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Synthesis of Heterocycles
z0375
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0375
Rhodium(III)-Catalyzed C–H Activation/Annulation To Form Isoquinolone Scaffolds

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0376
Chiral Phosphoric Acid Catalyzed Enantioselective Synthesis of 8-Azabicyclo[4.3.1]decanes

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0377
Preparation of Imidazolidine-2-ones from N-Benzoyloxyureas by C–H Amination

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0378
Nickel/Copper-Catalyzed Amidation of 2-Iodoglycals to Access Glycosamine Analogues

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0379
Palladium-Catalyzed Synthesis of Azepines from Pyrrolidines

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0380
Three-Component Approach to Indoles

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0381
Synthesis of N-Fused Hetarenes from Alkenes

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0382
N-Containing Bicyclic Heterocycles by Annulation of 2H-Azirines with 2-Chloropyridine Derivatives

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0383
Et₃N-Direct Cycloaddition of Allenoates with Acceptor Diazo-Compounds

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0384
Diastereoselective Synthesis of 2,3-Dihydrofurans from Silver Allenes

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0385
Synthesis of Enantiomerically Enriched Chiral 1-Pyrrolines

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Synthesis of Materials and Unnatural Products
z0387
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0387
From Saddles to Helices

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0388
Easy as 1,2,3,4-Tetrasubstituted Benzenes

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0389
An Expedient Approach to a Zigzag Carbon Nanobelt

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0390
Stereospecific Synthesis of Pyrene-Fused [5]Helicenes

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0391
Flip-Flopping Nanohoops

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0392
BRB, Looking for Aromaticity

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0393
Easy as 8π

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0394
Efficient Synthesis of azahelicenes through Imine-Based Mallory Cyclization

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0395
Alternative Retrosynthetic Approach towards Synthesis of Nile Red Analogues

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0396
Facile Functionalization of 6-Aryl-2,20-bipyridines

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0397
No Resolution Necessary

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0398
Novel Synthesis of Piperidinium-Functionalized Polyethylene for Alkaline Anion Exchange Membranes

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Metals in Synthesis
z0399
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0399
Iron-Catalyzed Asymmetric Carboazidation of Styrenes
FREIER ZUGRIFF

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0400
Diastereoselective Synthesis of (Spiro)Indanones by Nickel-Catalyzed Reductive Cyclization

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0401
Acyl Chlorides as Dual Source of Carbon Nucleophile and Carbon Monoxide
FREIER ZUGRIFF

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0402
Enantioselective Nickel Hydride Catalyzed Cross Coupling of Alkyl Electrophiles

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0403
Pd(0)-Catalyzed, Stereoselective Intermolecular Cycloaddition: Towards Substituted Cyclopentanes

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0404
α-Arylation of Ketones with Nitroarenes

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0405
Asymmetric Hydroarylation of N-Acyl Enamines

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0406
4-Thiooxazole Synthesis and Sulfanyl–Lithium Exchange

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0407
Palladium-Catalyzed Z-Selective Dienylations

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0408
Silver-Catalyzed Heteroarylation of Aliphatic Alcohols in Water

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PDF (76 kb)
0409
Site-Selective Silver-Catalyzed C−H Bond Deuteration of Five-Membered Heterocycles

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0410
Chiral Aldehydes from Cycloproyplacetylenes via Palladium/Organo Dual-Catalysis

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0411
Pd-Catalyzed Enantioselective Carbohalogenation Employing a H-Bonding Driven Reductive Elimination

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0412
Palladium-Catalyzed C–H Addition to Nitriles: α-Iminol Rearrangement

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0413
Scandium-Catalyzed Asymmetric Homologation of Ketones using α-diazo Esters

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0414
Photoredox Catalysis: Decarboxylative Cross-Coupling of Nitrones with α‑Amino Acids

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0415
Enantio- and Diastereoselective Conjugate Addition of Borylalkenes to α,β-Unsaturated Diesters

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0416
Asymmetric Heck–Matsuda Reaction for the Preparation of β-Chiral Ketones

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0417
Enantioselective Sulfimidation of Pyridones and Quinolones via Silver Catalysis

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0418
Copper-Catalyzed Asymmetric Alkylamination of Unactivated Alkenes Generating β-Lactams

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0419
Generation of Secondary and Tertiary Alcohols via Anaerobic Mukaiyama-Type Hydration

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0420
meta-Selective C–H Functionalization of Phenols

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0421
Palladium-Catalyzed Carbonylation of 1,3-Dienes

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0422
Asymmetric Synthesis of 4-Aryl-3,4-dihydrocoumarins by Palladium-Catalyzed Hydroesterification

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0423
Hydrofuctionalization of Styrene via a Photoredox Process Catalyzed by a Decatungstate Complex

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0424
Nickel-Catalyzed Enantioselective Hydroalkylation of Enecarbamates

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PDF (87 kb)
0425
Copper-Catalyzed Enantioselective Vinylogous Aldol Reaction of Allylazaarenes

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0426
Asymmetric Conjugate Addition of 1,1-Diborylmethane

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0427
Directed ortho-Lithiation of Benzamides
FREIER ZUGRIFF

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Polymer-Supported Synthesis
z0429
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PDF (404 kb)
0429
Synthesis of Alkynylcyclopentenols on a Foam-Supported Palladium Catalyst
FREIER ZUGRIFF

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0430
Dehydrogenative Condensation of Anilines with Dioles on Platinum/Alumina

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0431
One-Step Deoxydehydration–Transfer Hydrogenation of Sugar Acids with a Pt–Re Oxide Catalyst

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PDF (85 kb)
0432
Supported Cobalt Phosphide Nanoalloy Catalysts for Hydrogenation of Furfurals

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PDF (99 kb)
0433
Synthesis of Spiro-4-thiazolidinones on a Porous Polymeric Ionic Liquid Containing Co₃O₄

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PDF (80 kb)
0434
Hydrocarboxylation of Alkenes Catalyzed by Rhodium Supported on Porous Organic Polymer

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PDF (72 kb)
0435
Heterogeneous Gold-Nanoparticle-Catalyzed Stille Coupling of Benzylic Bromides and Allylstannanes

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PDF (297 kb)
0436
Cobalt-Catalyzed Reductive Alkylation of Nitriles with Aldehydes or Ketones

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PDF (70 kb)
0437
Selective Oxidation of Alcohols with TEMPO Supported on Hollow Porous Aromatic Frameworks

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0438
Gold/Titania-Catalyzed Borylation of Allylic, Propargylic, and Benzylic Esters

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Organo- and Biocatalysis
z0439
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0439
Photoenzymatic Intermolecular Hydroalkylation of Alkenes
FREIER ZUGRIFF

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PDF (160 kb)
0440
Asymmetric Photoredox Dearomatization of Indoles by Neutral α-Amino Radicals

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0441
Photoenzymatic Reduction of α,β-Unsaturated Amides with Ene-Reductases

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PDF (103 kb)
0442
BINOL-Derived Photoswitchable Phase-Transfer Catalysts

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PDF (95 kb)
0443
Synthesis of a Chiral Pentafluorinated Isopropyl Group by Aryl Iodide Catalyzed Difluorination of Styrenes

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PDF (87 kb)
0444
N-Fluorosulfonyl Carbamate and Organoiodine Catalysis: Vicinal Heterodifunctionalization of Olefins

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0445
Synergistic Dual Organocatalysis for Highly Selective Michael Additions

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PDF (85 kb)
0446
Catalytic Asymmetric Chloroamidation of Allylic Amides

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PDF (88 kb)
0447
High Lewis Acidity of Bidentate Iodine(III)-Based Halogen-Bond Donors

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PDF (96 kb)
0448
Photocatalytic Minisci Alkylation of Azaarenes

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PDF (83 kb)
0449
Room-Temperature Carbon Isotope Exchange of Carboxylic Acids Through Photoredox Catalysis

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PDF (94 kb)
Chemistry in Medicine and Biology
z0451
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PDF (460 kb)
0451
Sucrose Analogues for Real-Time Imaging of Intracellular Plant Metabolism

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PDF (65 kb)
0452
Total Synthesis of Cephalosporin C
FREIER ZUGRIFF

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PDF (141 kb)
0453
Optical Control of the Cannabinoid Receptor 2
FREIER ZUGRIFF

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PDF (130 kb)
0454
Novel Prodrugs for Targeted Cancer Therapy

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PDF (191 kb)
0455
Light-Induced Cell Cycle Arrest and Apoptosis

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PDF (83 kb)
0456
A Potent Preclinical Plasmodium Proteasome Inhibitor

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PDF (80 kb)
0457
Modular Chemoenzymatic Synthesis of GE81112 B1

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PDF (86 kb)
0458
Diversity-Focused Semisynthesis of Polyether Ionophores with New Antibacterial Selectivity

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PDF (82 kb)
0459
Evaluation of C2−C2′ Bond Stereochemistry Influence on Cytotoxicity of (–)-Lomaiviticin A

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Peptide Chemistry
z0461
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PDF (326 kb)
0461
Ball-Milling Strategy for Epimerization-Free Peptide Synthesis
FREIER ZUGRIFF

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PDF (113 kb)
0462
Rhodium-Catalyzed Synthesis of β²/γ²/δ²-Amino Acid Derivatives

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PDF (87 kb)
0463
Synthesis of All-Alkyl α-Tertiary Amino Acid Derivatives under Visible-Light Irradiation

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PDF (82 kb)
0464
β-Seleno-α-Amino Acids Synthesis by Seleno-Michael Additions to Bicyclic Dehydroalanine

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PDF (89 kb)
0465
Photocatalyzed Modification for Tryptophane-Containing Peptides

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PDF (76 kb)
0466
Triflic Acid Catalyzed N–H Insertion Reaction for the Synthesis Unnatural α-Amino Esters

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PDF (91 kb)
0467
Synergistic Brønsted Acid/Photoredox Catalysis for the Synthesis of α-Amino Acids

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PDF (91 kb)
0468
Rhodium-Catalyzed Formation of Proline Analogues

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PDF (76 kb)
0469
Peptide Bond Formation by Using 2-Pyridyl Thio Esters
FREIER ZUGRIFF

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Flow Chemistry
z0471
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PDF (170 kb)
0471
Halogen–Lithium Exchange on Isothiocyanate-Substituted Aryl Halides

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PDF (77 kb)
0472
Safer Handling of Diazomethane through Continuous Generation and Consumption

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PDF (85 kb)
0473
Oxidative Debenzylation of Protected Carbohydrates under Flow Conditions

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PDF (70 kb)
0474
Synthesis of Aminoimidazo Heterocycles under Flow Conditions

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PDF (72 kb)
0475
Generation and Use of Lithiated 1-Azabicyclo[1.1.0]butanes in Flow Microreactors

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PDF (80 kb)
0476
Selective Oxidation of Alcohols under Flow Conditions

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