Synlett

Issue 03 · March 1998

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213
Guindon, Yvan; Jung, Grace; Guérin, Brigitte; Ogilvie, William W.:
Hydrogen and Allylation Transfer Reactions in Acyclic Free Radicals

PDF (242 kb)
221
Varvoglis, Anastasios; Spyroudis, Spyros:
Hypervalent Iodine Chemistry: 25 Years of Development at the University of Thessaloniki

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new tools in synthesis
233
Meier, C.:
Pro-Nucleotides - Recent Advances in the Design of Efficient Tools for the Delivery of Biologically Active Nucleoside Monophosphates
FREE ACCESS

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letter
243
Okano, Tamon; Iwahara, Masahiro; Kiji, Jitsuo:
Catalytic Cyanation of Aryl Halides with NaCN in the Presence of Crowned Phosphine Complexes of Palladium under Solid-liquid Two-phase Conditions

PDF (41 kb)
245
Wang, Fang; Zibuck, Regina:
Studies on α-Alkoxyalkylation of 2-Cyclohexen-1-one with Cyclic Acetals 1. Pyridiniosilylation

PDF (27 kb)
247
Olivo, Horacio F.; Hemenway, Michael S.; Hartwig, Amy C.; Chan, Raymond:
New Preparation of Activated 2-Vinylaziridines from 1,4-Aminoalcohols

PDF (28 kb)
249
Oyamada, Hidekazu; Kobayashi, Shu:
Rare Earth Triflate-Catalyzed Addition Reactions of Acylhydrazones with Silyl Enolates. A Facile Synthesis of Pyrazolone Derivatives

PDF (44 kb)
251
Cossy, Janine; Poitevin, Christophe; Pardo, Domingo Gomez:
Heck Reaction versus Free Radical Reaction for the Synthesis of Spiro[indoline-2,4′-piperidines]

PDF (34 kb)
253
Takai, Kazuhiko; Shinomiya, Norio; Ohta, Masako:
Generation of α-Boryl Radicals by Reduction of α-Haloalkylboronic Esters with CrCl₂

PDF (42 kb)
255
Kotsuki, Hiyoshizo; Oshisi, Takeshi; Inoue, Motoshi:
Scandium(III) Trifluoromethanesulfonate-Catalyzed Friedel-Crafts Alkylation of Aromatic Compounds with Secondary Alcohol Methanesulfonates

PDF (40 kb)
257
Sakai, Atsushi; Tani, Hideaki; Aoyama, Toyohiko; Shioiri, Takayuki:
Enantioselective Photosensitized Oxygenation. Its Application to N_b-Methoxycarbonyltryptamine and Determination of Absolute Configuration of the Product

PDF (33 kb)
259
Mori, Kenji; Audran, Gérard; Monti, Honoré:
The First Synthesis of Coniochaetones A and (±)-B: Two Benzopyranone Derivatives

PDF (39 kb)
261
Kim, Yong Hae; Park, Heui Sul:
A Convenient Coupling Reaction of Isocyanates with t-Alcohols with Catalytic Amount of SmI₂ in the Presence of HMPA

PDF (32 kb)
263
Girreser, Ulrich; Heber, Dieter; Schütt, Martin:
An Efficient and Facile Synthesis of Novel 3-Benzoyl-3,4-dihydro-2H-pyrido[1,2-a]pyrimidines

PDF (38 kb)
265
Nabeshima, Tatsuya; Hosoya, Toshiyuki; Yano, Yumihiko:
Preparation of Novel Polyethers Containing Bisbipyridines and Chiral Auxiliaries, and the Complexation with Cu(I)

PDF (45 kb)
267
Matsubara, Seijiro; Kawamoto, Kazunari; Utimoto, Kiitiro:
Preparation of 1,3-Diketones by the Reaction of Bis(iodozincio)methene with Acyl Cyanides or Palladium-Catalyzed Reaction with Acyl Chlorides

PDF (55 kb)
269
Okada, Yukihiro; Hagihara, Masatoshi; Mineo, Masatoshi; Nishimura, Jun:
A New Intermolecular Photochemical Approach to Calix[4]arene Synthesis

PDF (38 kb)
271
Miyata, Okiko; Muroya, Kanami; Koide, Junko; Naito, Takeaki:
A Concise Synthesis of Rigidified β-Amino Acids via Sulfanyl Radical Addition-Cyclization of Oxime Ethers and Hydrazones

PDF (34 kb)
273
Akiyama, Takahiko; Iwai, Junko:
Three-Component Synthesis of Homoallylamines by Scandium(III) Triflate-Mediated Allylation with Allylgermane: A Highly Imine Selective Allylation Reaction

PDF (34 kb)
275
Chataigner, Isabelle; Zammattio, Françoise; Lebreton, Jacques; Villiéras, Jean:
Enantioselective Synthesis of α-Methylene-γ-Lactams. Nucleophilic Addition of a Chirally Modified β-Functionalized Allylboronate Reagent to Imines

PDF (33 kb)
277
Baskaran, Subramanian; Aurich, Hans Günter:
Domino Reactions of a Double δ,ℇ-Unsaturated Dioxime: Competition between Two Intramolecular Cycloaddition Pathways

PDF (53 kb)
280
Pyne, Stephen G.; Ung, Alison T.:
Diastereoselective Synthesis of (1S,2S,3R)- and (1R,2R,3R)-2-Acetyl-5-(1,2,3,4-tetrahydroxybutyl)thiazole

PDF (49 kb)
283
Collingwood, Stephen P.; Taylor, Roger J.:
The Utilization of Secondary Phosphine Oxide Synthons for the Preparation of Novel Tertiary Phosphine Oxide Modified DNA

PDF (56 kb)
286
Muraki, Takahito; Togo, Hideo; Yokoyama, Masataka:
Synthetic Use of 1-(p-Toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one: Iodination of Aromatic Rings

PDF (46 kb)
289
Gauthier, Jacques Yves; Zajac, Nicolas; Mayhew, Darrin L.; Hughes, Gregory J.; Martins, Evelyn; Guay, Daniel; Young, Robert N.; Zamboni, Robert J.:
Heteroaromatic Dithioacetals Part I: The Preparation of Unsymmetrical Dithioacetals from Heteroaromatic Thiols

PDF (48 kb)
292
Kita, Yasuyuki; Iio, Kiyosei; Okajima, Akiko; Takeda, Yoshifumi; Kawaguchi, Ken-ichi; Whelan, Brendan A.; Akai, Shuji:
An Efficient Synthesis of peri-Hydroxy Aromatic Compounds: A Strong Base-Induced [4 + 2]Cycloaddition of 4-Phenylthio-Substituted Homophthalic Anhydrides with Various Sulfinyl-Substituted Dienophiles

PDF (54 kb)
295
Blettner, Carsten G.; König, Wilfried A.; Stenzel, Wolfgang; Schotten, Theo:
Poly(ethylene glycol) Supported Liquid Phase Synthesis of Biaryls

PDF (65 kb)
298
Noda, Takeshi; Ishiwata, Akihiro; Uemura, Satoshi; Sakamoto, Satoshi; Hirama, Masahiro:
Synthetic Study of Pinnatoxin A: Stereoselective Synthesis of the BCD-ring Unit, a Novel 6,5,6-Bis-spiroketal System

PDF (76 kb)
301
Haenel, Matthias W.; Oevers, Stephan; Bruckmann, Joachim; Kuhnigk, Jörg; Krüger, Carl:
Facile Syntheses of 1,8-Bis(diphenylphosphino)anthracene and 1,8-Bis(dimethylamino)anthracene by Nucleophilic Substitution of 1,8-Difluoroanthracene

PDF (46 kb)
304
Turner, Debra; Vogel, Pierre:
Synthesis of 4-Hydroxy-2,6-bis(hydroxymethyl)tetrahydropyran-2-carbaldehyde Derivatives

PDF (41 kb)
307
McAuliffe, Joseph C.; Hindsgaul, Ole:
The Synthesis of Disaccharides Terminating in D-Septanosyl Residues Using Acyclic Intermediates

PDF (59 kb)
310
Garg, Nupur; Lee, T. Randall:
Regioselective Bromomethylation of 1,2-Dialkylbenzenes

PDF (52 kb)
313
Matsubara, Seijiro; Sugihara, Masakazu; Utimoto, Kiitiro:
Methylenation of Carbonyl Compounds by Means of Nysted Reagent

PDF (67 kb)
316
Fernández, J. M. García; Mellet, C. Ortiz; Benito, J. M.; Fuentes, J.:
Synthesis of Calystegine B₂ Analogs by Tandem Tautomerization-Intramolecular Glycosylation of Thioureidosugars

PDF (40 kb)
319
Alpegiani, Marco; Bissolino, Pierluigi; D'Anello, Matteo; Perrone, Ettore:
Novel Preparation of 1,1-Dioxo-7α-methoxy-3-methyl-Δ³-cephem-4-yl Aryl Ketones

PDF (48 kb)
322
Alpegiani, Marco; Bissolino, Pierluigi; D'Anello, Matteo; Palladino, Massimiliano; Perrone, Ettore:
Expeditious Synthesis of 4-(tert-Butylcarbonyl)-7α-methoxy-3-methyl-Δ³-cephem 1,1-Dioxide. Convenient Access to 7-Substituted Analogues

PDF (59 kb)
325
Alami, M.; Ramiandrasoa, P.; Cahiez, G.:
Stereoselective Manganese-Catalyzed Coupling Reaction of Conjugated Chloroenynes and Chlorodienes with Grignard Reagents

PDF (65 kb)

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Synlett

Hydrogen and Allylation Transfer Reactions in Acyclic Free Radicals

Hypervalent Iodine Chemistry: 25 Years of Development at the University of Thessaloniki

Pro-Nucleotides - Recent Advances in the Design of Efficient Tools for the Delivery of Biologically Active Nucleoside Monophosphates

Catalytic Cyanation of Aryl Halides with NaCN in the Presence of Crowned Phosphine Complexes of Palladium under Solid-liquid Two-phase Conditions

Studies on α-Alkoxyalkylation of 2-Cyclohexen-1-one with Cyclic Acetals 1. Pyridiniosilylation

New Preparation of Activated 2-Vinylaziridines from 1,4-Aminoalcohols

Rare Earth Triflate-Catalyzed Addition Reactions of Acylhydrazones with Silyl Enolates. A Facile Synthesis of Pyrazolone Derivatives

Heck Reaction versus Free Radical Reaction for the Synthesis of Spiro[indoline-2,4′-piperidines]

Generation of α-Boryl Radicals by Reduction of α-Haloalkylboronic Esters with CrCl₂

Scandium(III) Trifluoromethanesulfonate-Catalyzed Friedel-Crafts Alkylation of Aromatic Compounds with Secondary Alcohol Methanesulfonates

Enantioselective Photosensitized Oxygenation. Its Application to N_b-Methoxycarbonyltryptamine and Determination of Absolute Configuration of the Product

The First Synthesis of Coniochaetones A and (±)-B: Two Benzopyranone Derivatives

A Convenient Coupling Reaction of Isocyanates with t-Alcohols with Catalytic Amount of SmI₂ in the Presence of HMPA

An Efficient and Facile Synthesis of Novel 3-Benzoyl-3,4-dihydro-2H-pyrido[1,2-a]pyrimidines

Preparation of Novel Polyethers Containing Bisbipyridines and Chiral Auxiliaries, and the Complexation with Cu(I)

Preparation of 1,3-Diketones by the Reaction of Bis(iodozincio)methene with Acyl Cyanides or Palladium-Catalyzed Reaction with Acyl Chlorides

A New Intermolecular Photochemical Approach to Calix[4]arene Synthesis

A Concise Synthesis of Rigidified β-Amino Acids via Sulfanyl Radical Addition-Cyclization of Oxime Ethers and Hydrazones

Three-Component Synthesis of Homoallylamines by Scandium(III) Triflate-Mediated Allylation with Allylgermane: A Highly Imine Selective Allylation Reaction

Enantioselective Synthesis of α-Methylene-γ-Lactams. Nucleophilic Addition of a Chirally Modified β-Functionalized Allylboronate Reagent to Imines

Domino Reactions of a Double δ,ℇ-Unsaturated Dioxime: Competition between Two Intramolecular Cycloaddition Pathways

Diastereoselective Synthesis of (1S,2S,3R)- and (1R,2R,3R)-2-Acetyl-5-(1,2,3,4-tetrahydroxybutyl)thiazole

The Utilization of Secondary Phosphine Oxide Synthons for the Preparation of Novel Tertiary Phosphine Oxide Modified DNA

Synthetic Use of 1-(p-Toluenesulfonyloxy)-1,2-benziodoxol-3(1H)-one: Iodination of Aromatic Rings

Heteroaromatic Dithioacetals Part I: The Preparation of Unsymmetrical Dithioacetals from Heteroaromatic Thiols

An Efficient Synthesis of peri-Hydroxy Aromatic Compounds: A Strong Base-Induced [4 + 2]Cycloaddition of 4-Phenylthio-Substituted Homophthalic Anhydrides with Various Sulfinyl-Substituted Dienophiles

Poly(ethylene glycol) Supported Liquid Phase Synthesis of Biaryls

Synthetic Study of Pinnatoxin A: Stereoselective Synthesis of the BCD-ring Unit, a Novel 6,5,6-Bis-spiroketal System

Facile Syntheses of 1,8-Bis(diphenylphosphino)anthracene and 1,8-Bis(dimethylamino)anthracene by Nucleophilic Substitution of 1,8-Difluoroanthracene

Synthesis of 4-Hydroxy-2,6-bis(hydroxymethyl)tetrahydropyran-2-carbaldehyde Derivatives

The Synthesis of Disaccharides Terminating in D-Septanosyl Residues Using Acyclic Intermediates

Regioselective Bromomethylation of 1,2-Dialkylbenzenes

Methylenation of Carbonyl Compounds by Means of Nysted Reagent

Synthesis of Calystegine B₂ Analogs by Tandem Tautomerization-Intramolecular Glycosylation of Thioureidosugars

Novel Preparation of 1,1-Dioxo-7α-methoxy-3-methyl-Δ³-cephem-4-yl Aryl Ketones

Expeditious Synthesis of 4-(tert-Butylcarbonyl)-7α-methoxy-3-methyl-Δ³-cephem 1,1-Dioxide. Convenient Access to 7-Substituted Analogues

Stereoselective Manganese-Catalyzed Coupling Reaction of Conjugated Chloroenynes and Chlorodienes with Grignard Reagents