Synlett

Issue 14 · November 2004

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2449
Achari, Basudeb; Mandal, Sukhendu B.; Dutta, Pradeep K.; Chowdhury, Chinmay:
Perspectives on 1,4-Benzodioxins, 1,4-Benzoxazines and their 2,3-Dihydro Derivatives

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2468
Gabriele, Bartolo; Salerno, Giuseppe; Costa, Mirco:
PdI₂-Catalyzed Synthesis of Heterocycles

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letter
2484
Chakraborty, Tushar K.; Tapadar, Subhasish; Raju, T. Venugopal; Annapurna, J.; Singh, Harjinder:
Cyclic Trimers of Chiral Furan Amino Acids

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PDF (402 kb)
2489
Allwein, Shawn P.; Secord, Elizabeth A.; Martins, Andrew; Mitten, Jeffrey V.; Nelson, Todd D.; Kress, Michael H.; Dolling, Ulf H.:
Convenient Synthesis and Isolation of 1-Aminocyclopropane-1-carboxylic Acid (ACC) and N-Protected ACC Derivatives

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PDF (138 kb)
2493
Tsuchiya, Yasunori; Kanazawa, Yoshinori; Shiomi, Takushi; Kobayashi, Kazuki; Nishiyama, Hisao:
Asymmetric Conjugate Reduction of α,β-Unsaturated Esters with Chiral Rhodium(bisoxazolinylphenyl) Catalysts

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2497
Fuwa, Haruhiko; Kobayashi, Toshitake; Tokitoh, Takashi; Torii, Yukiko; Natsugari, Hideaki:
Intramolecular Nucleophilic Aromatic Substitution Reaction of 2-Carboxamido-3-arylquinazolin-4-ones and its Application to the Synthesis of Secondary Aryl Amines

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PDF (147 kb)
2501
Sakuma, Daisuke; Togo, Hideo:
Facile and Environmentally Benign Zn-Mediated Cyclopropanation of Electron-Deficient 2-Iodoethyl-Substituted Olefins via Radical 3-exo-trig Manner

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2505
Yamagishi, Takehiro; Fujii, Keiichi; Shibuya, Shiroshi; Yokomatsu, Tsutomu:
Synthesis of Chiral γ-Amino-β-hydroxyphosphonate Derivatives from Unsaturated Phosphonates

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2509
Shibata, Norio; Ishimaru, Takehisa; Nakamura, Mai; Toru, Takeshi:
20-Deoxy-20-fluorocamptothecin: Design and Synthesis of Camptothecin Isostere

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2513
Kashiwagi, Yoshitomo; Chiba, Shinya; Ikezoe, Hiroshi; Anzai, Jun-ichi:
Polypyrrole-Supported Graphite Felt for Acetylene Coupling Reaction in Solid Phase

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PDF (143 kb)
2517
Toftered, Jörgen; Nilsson, Ulf J.:
Synthesis of Chiral Macrocycles by Cyclodimerization of Diamines with Stepwise Nucleophilic Aromatic Substitution of 1,5-Difluoro-2,4-dinitrobenzene

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PDF (137 kb)
2521
Braddock, D. Christopher; Matsuno, Ai:
A Silicon-Centred Tetrafunctionalised Reagent for the Cyclopropylmethylsilane-Terminated Prins Reaction and a Concise Synthesis of Lyngbic Acid

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2525
Ficht, Simon; Röglin, Lars; Ziehe, Matthias; Breyer, David; Seitz, Oliver:
Direct Carbodiimide-Mediated Conjugation of Carboxylates Using Pyridinium p-Toluenesulfonate and Tertiary Amines as Additives

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2529
Valsecchi, Elena; Tacchi, Alessio; Prosperi, Davide; Compostella, Federica; Panza, Luigi:
An Efficient Transformation of (-)-Quinic Acid into Carba-l-rhamnose

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2533
Kamal, Ahmed; Reddy, K. Laxma; Devaiah, V.; Shankaraiah, N.:
Synthesis of DNA-Interactive Pyrrolo[2,1-c][1,4]benzodiazepines by Employing Polymer-Supported Reagents: Preparation of DC-81

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2537
Loog, Olavi; Mäeorg, Uno:
Cu-Catalysed N-Arylation of Hydrazines with Bismuthanes: Synthesis and Pinacol or Imino-Pinacol Coupling of 4-Formylphenylhydrazines and their Phenylimine Derivatives

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PDF (138 kb)
2541
Park, Kang Hyun; Jung, Il Gu; Chung, Young Keun:
Synthesis of Coumarins Catalyzed by Heterobimetallic Co/Rh Nanoparticles

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2545
Kang, Hyun Jung; Kim, Sang Hee; Pae, Ae Nim; Koh, Hun Yeong; Chang, Moon Ho; Choi, Kyung il; Han, So-Yeop; Cho, Yong Seo:
Diastereoselective Synthesis of Seven- and Eight-Membered Oxabicycles via Prins-Type Cyclization

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PDF (138 kb)
2549
Nettekoven, Ulrike; Naud, Frédéric; Schnyder, Anita; Blaser, Hans-Ulrich:
A New Efficient Palladium Catalyst for the Amination of Aryl Chlorides

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2553
Fernández-Mateos, A.; Mateos Burón, L.; Martín de la Nava, E. M.; Rabanedo Clemente, R.; Rubio González, R.; Sanz González, F.:
Effect of Tether Length on Ti(III)-Mediated Cyclization of Epoxyalkenes and Unsaturated Epoxyketones

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PDF (185 kb)
2558
Gilbert, Michael W.; Galkina, Anna; Mulzer, Johann:
Toward the Total Syntheses of Pepluanin A and Euphosalicin: Concise Route to a Highly Oxygenated Cyclopentane as a Common Intermediate

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PDF (220 kb)
2563
Gogonas, Efstathios P.; Nyxas, Ioannis; Hadjiarapoglou, Lazaros P.:
The Reaction of Phenyliodonium Bis(phenylsulfonyl)methylide with Alkyl Iodides

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2566
Gabrilidis, Dimitris; Kalogiros, Christos; Hadjiarapoglou, Lazaros P.:
Diels-Alder Reactions of Substituted Cyclohexa-2,4-dienones with Alkenes and Alkynes

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2570
De Luca, Lidia; Giacomelli, Giampaolo; Porcheddu, Andrea; Salaris, Margherita:
A New, Simple Procedure for the Synthesis of Formyl Amides

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2573
Chappellet, Sabrina; Müller, Paul:
Ru-Catalyzed Enantioselective Dipolar Cycloadditions of Ethyl Diazopyruvate

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PDF (87 kb)
2576
Kazmaier, Uli; Ackermann, Stefanie:
An Improved Protocol for the Synthesis of Allylated Isonitriles

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2579
McIntosh, Caitlin E.; Martínez, Isamir; Ovaska, Timo V.:
Microwave Enhanced Tandem 5-exo Cyclization/Claisen Rearrangement Reactions: A Convenient Route to Cycloheptanoid Ring Systems

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2582
Kobayashi, Yuichi; Yagi, Kaori; Ainai, Takayuki:
Synthesis of Δ²-OPC-8:0 and OPC-6:0

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2585
Zheng, Hongchao; Cheng, Changmei; Wang, Hua; Xu, Shanshan; Zhao, Yufen:
Study on Disulfur-Backboned Nucleic Acid: Part 1, Efficient Synthesis of 3′,5′-Dithio-2′-Deoxyadenosine

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PDF (115 kb)
2588
Brandes, Sebastian; Selig, Philipp; Bach, Thorsten:
Stereoselective Intra- and Intermolecular [2+2] Photocycloaddition Reactions of 4-(2′-Aminoethyl)quinolones

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PDF (131 kb)
2591
Balog, Mária; Kálai, Tamás; Jekő, József; Steinhoff, Heinz-Jürgen; Engelhard, Martin; Hideg, Kálmán:
Synthesis of New 2,2,5,5-Tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl Radicals and 2-Substituted-2,5,5-trimethylpyrrolidin-1-yloxyl Radicals Based α-Amino Acids

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PDF (101 kb)
2594
Wu, Zicheng; Kong, Fanzuo:
Synthesis of 6-Branched Cyclo-(1→3)-glucohexaose and Glucooctaose

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PDF (131 kb)
2597
Miyabe, Hideto; Yamaoka, Yousuke; Takemoto, Yoshiji:
Aqueous Medium Radical Addition to Ketimines with a Phenolic Hydroxyl Group

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2600
Li, Xueshu; Fu, Hua; Jiang, Yuyang; Zhao, Yufen; Liu, Jinyong:
New and Efficient Approach to Aryl Phosphoramidate Derivatives of AZT/d4T as Anti-HIV Prodrugs

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PDF (91 kb)
2603
Sheng, Shou-Ri; Huang, Pei-Gang; Zhou, Wei; Luo, Hai-Rong; Lin, Shu-Ying; Liu, Xiao-Ling:
A Facile Solid-Phase Synthesis of Substituted 2(5H)-Furanones with Sulfone Traceless Linker

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PDF (134 kb)
2606
Page, Philip C. Bulman; Chan, Yohan; Heaney, Harry; McGrath, Matthew J.; Moreno, Eduardo:
The Efficient Synthesis of Alkoxy-esters from Hydroxy Carboxylic Acids Using Dimsyllithium in Dimethylsulfoxide Followed by Alkylation with an Alkyl Halide

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2609
Hilton, Stephen T.; Motherwell, William B.; Selwood, David L.:
An Expedient Entry into the α-Mercaptodiketopiperazine Nucleus

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2612
Sissouma, Drissa; Collet, Sylvain C.; Guingant, André Y.:
A Synthesis of Calothrixin B

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2615
Bagley, Mark C.; Chapaneri, Krishna; Glover, Christian; Merritt, Eleanor A.:
Simple Microwave-Assisted Method for the Synthesis of Primary Thioamides from Nitriles

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PDF (79 kb)
2618
Ballini, Roberto; Barboni, Luciano; Fiorini, Dennis; Palmieri, Alessandro:
Anionic Domino Process for the One-Pot, Diastereoselective Synthesis of Dihydropyranols from β-Nitroalcohols

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2621
Blanrue, Amélie; Wilhelm, René:
Imidazolinium-Carbodithioate Zwitterions as Organocatalysts for the Cyanosilylation of Aldehydes

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PDF (70 kb)
2624
Tsogoeva, Svetlana B.; Jagtap, Sunil B.:
Dual Catalyst Control in the Chiral Diamine-Dipeptide-Catalyzed Asymmetric Michael Addition

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PDF (87 kb)
2627
Zhao, Gang; Castro, Peter P.; Gutierrez-Tunstad, Linda M.:
Hexacarboxylic Acid Biscavitands

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2630
Basu, Basudeb; Das, Pralay; Hossain, Ismail:
Synthesis of β-Amino Esters via Aza-Michael Addition of Amines to Alkenes Promoted on Silica: A Useful and Recyclable Surface

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2633
Procopio, Antonio; Dalpozzo, Renato; De Nino, Antonio; Nardi, Monica; Sindona, Giovanni; Tagarelli, Antonio:
Erbium(III) Triflate: A Valuable Catalyst for the Rearrangement of Epoxides to Aldehydes and Ketones

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2636
Bartels, Marc; Zapico, Julian; Gallagher, Timothy:
C(6)-Alkylation of 3-Hydroxypiperidine via Reductive and Homolytic Cleavage of N,S-Acetals

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2639
Horino, Yoshikazu; Livinghouse, Tom; Stan, Magdalena:
Alkene-Pinacolborane Hydroborations Catalyzed by Lanthanum Tris[bis(trimethylsilyl)amide]

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PDF (76 kb)
spotlight
2642
Wang, Shun-Yi:
Molecular Iodine
FREE ACCESS

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2644
Malaubier, Jean-Baptiste:
p-Toluenesulfonyl Isocyanate
FREE ACCESS

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PDF (117 kb)
addenda and errata
2646
Bernotas, Ronald C.:
A Short, Novel Approach to 2,3,4a,5-Tetrahydro-1H-pyrazino[1,2-a]quinoline-4,6-diones
FREE ACCESS

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PDF (12 kb)
2646
Hara, Osamu; Sugimoto, Kazuhiko; Makino, Kazuishi; Hamada, Yasumasa:
New Synthesis of a Pyrroloquinoline Skeleton, the Martinelline Core, Using a Tandem Michael-Aldol Strategy
FREE ACCESS

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PDF (8 kb)