Synfacts

Issue 06 · June 2014

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Synthesis of (+)- and (–)-Frondosin B

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Synthesis of a Hepatitis C Replication Inhibitor

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Total Synthesis of Halichondrin A

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Synthesis of Atorvastatin Calcium

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Synthesis of GS-9669

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Total Synthesis of (±)-Picrinine

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0567
Synthesis of N-Heterocycles via Rhodium(III)-Catalyzed C–H Activation

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Cu- and Pd-Catalyzed Heteroannulation Route to Imidazo[4,5-c]pyridines

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Benzofurans via Gold-Catalyzed Intramolecular Alkoxyboration of Alkynes

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0570
Synthesis of β-Lactams via Intramolecular Oxidative Amidation

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Isoindolones via Intramolecular Amination of Benzylic C–H Bonds

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0572
Synthesis of Isoindolin-1-ones by sp³ C–H Bond Activation–Cyclization

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0573
Synthesis of Quinolinones via Aryne Insertion into C–S Bonds

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0574
Oxidative Coupling of Acrylic Acids and Amides with Alkynes

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Two-Stage Chemoselective Methylation Method for Heteroarenes

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Allylation–Radical Cyclization to Difluoromethylated Dihydrobenzoheteroles

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Pyrroles from Terminal Alkynes, N-Sulfonyl Azides, and Alkenyl Alkyl Ethers

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0578
Palladium-Catalyzed One-Pot Synthesis of Oxazolopyrazines by Heteroannulation

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0579
One-Pot Four-Step Regioselective Preparation of Pyrazoles and Isoxazoles

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0580
Copper-Catalyzed Route to Azido-Substituted Isoxazolines

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Efficient Three-Fold Symmetrical Nanographene Synthesis FREE ACCESS

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0582
‘A–zide’ You’ve Never Seen Before

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Poor Packing for Plentiful Pores

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Clar-ly Aromatic: A New Route to Tetrabenzo[8]circulene

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0585
A Mild Method to Access Functionalized Carboranes

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0586
Nucleophilic Substitution on Carbon Nanotubes

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A Creative Route to Tetracenes

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0588
A Good Way to Dye: A Modular Synthesis of Soluble, Unsymmetric TPDO Dyes

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0589
New Palladium Initiators for Living Polymerization of Isocyanides

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0590
Cyclopropanation of Norbornene Derivatives with Benzyl Bromides

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0591
Bottoms-up: Controlled Synthesis of BN-Heterosuperbenzenes

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0592
Poly(α-aminophosphonates) by MCR without Isocyanides

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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Copper(II)-Catalyzed Regioselective Acylations of Monosaccharides

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Asymmetric Addition of Propargylic Boron to Imines Catalyzed by NHC–Cu

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0595
C–C Bond Activation of Cyclobutanones by Rh(I) Catalysis

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0596
Ru(II)–Porphyrin-Catalyzed Carbene/Nitrene Transfer and Insertions

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Ferrocenes via a Desymmetrization Process Involving C−H Functionalization

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Asymmetric Dearomatization of Indoles Catalyzed by Iridium

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Copper-Catalyzed Asymmetric Hydroamination of Alkenes

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Rhodium-Catalyzed Enantioselective Synthesis of Dihydropyrroloindolones

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0601
Copper-Catalyzed Diastereoselective Synthesis of Unnatural Thiazoline Scaffolds

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Trimerization of Two Alkynes with Alkenes Catalyzed by a Rhodium Complex

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Enantioenriched P-Stereogenic Diarylphosphinites by Palladium Catalysis

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Synthesis of Chiral Organoboronates via Enantiotopic-Group-Selective Suzuki Reaction

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0605
Mannich Reaction Using a Silver Salt and Cinchona-Derived Aminophosphine

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Co(III)(salen)-Catalyzed Phenolic Kinetic Resolution of Epoxides

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0607
Asymmetric Allylic Alkylation Catalyzed by Molybdenum

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0608
Ruthenium-Catalyzed Stereocontrolled Synthesis of Aminodiols

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0609
Ruthenium-Catalyzed trans-Selective Hydrostannation of Alkynes

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0610
Iron–Iminium Catalyzed Enantioselective Synthesis of β-Amino α-Hydroxy Esters

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0611
Enantioselective Insertion of α-Diazoacetates into O–H Bonds

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0612
Kinetic Resolution of Cyclic Enol Ethers Catalyzed by Palladium

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0613
Copper-Catalyzed Enantioselective Synthesis of Substituted Pyrrolidines

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0614
Rhodium-Catalyzed Sequential Allylic Amination and Olefin Hydroacylation

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Cu-Catalyzed Enantioselective Allylic Cross-Coupling with Alkylboranes

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0616
Ruthenium-Catalyzed Diastereoselective Cyclization of Enediynes

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0617
Enantioselective Fluoroarylation Catalyzed by Palladium FREE ACCESS

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0618
Nickel-Catalyzed Asymmetric Michael–Henry Reaction

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0619
Palladium-Catalyzed Cyclative Diacetoxy-lation of Alkynyl Cyclohexadienones

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0620
Synthesis of Planar Chiral Metallocenes via an Asymmetric C−H Functionalization

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0621
Asymmetric Hydrogenation of α-Acetamidocinnamates by Rhodium Catalysis

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0622
Asymmetric Negishi Cross-Coupling en route to Chiral Tertiary Alkyl Fluorides

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Metal-Mediated Synthesis
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0623
Enantioselective Allene Addition to Aryl and Alkyl Imines FREE ACCESS

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0624
Copper-Promoted, Three-Component Access to Trifloromethylketoximes

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0625
Copper-Catalyzed Cross-Coupling and Application to Carboboration

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0626
Synthesis of Phenylcyclopropanes from Allylic Alcohols

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0627
MnO₂-Mediated Aroylation of N-Chlorosulfoximines Using Methyl Arenes

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0628
Synthesis of α-Amino Ketones via Aminocyanation of Cyclic Enones

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0629
Copper-Mediated Perfluoroalkylation of Heteroaryl Bromides Using (phen)CuR_F

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0630
1,4-Conjugate Addition of Grignard Reagents Catalyzed by Zinc(II) Salts

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0631
Lithiation–Borylation for the Conversion of Alcohols into Pinacol Boronic Esters

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0632
Metal Alkoxide Promoted Condensation of 2,3-Allenoates with Aldehydes

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0633
Geminal Silicon/Zinc Reagents as CF₂Bis-carbanion Synthons

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0634
Preparation of 2-Methyl-1,2-dihydro-naphthalen-1-ols

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0635
Addition of Grignard and Organolithium Reagents to N-Carboxyanhydrides

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0636
Transfer of Chirality in the Cycloisomerization of Enediynes

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0637
Chemo- and Regioselective C(sp³)–H Arylation of Unactivated Allylarenes

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Organo- and Biocatalysis
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0639
A Novel Chiral NHC Catalyst: Application to an Intramolecular Stetter Reaction

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0640
Organocascade Olefin Isomerization/Diels–Alder Reaction

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0641
Bifunctional Urea Catalyzed Synthesis of β-Amino Thioesters

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0642
Bromoetherification and Desymmetrization Using a Sulfide Organocatalyst

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0643
Organocatalytic Asymmetric Fluorination of α-Substituted Cyclohexanones

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0644
Catalytic Enantioselective Synthesis of Bridged Tricyclic Benzopyrans

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0645
A Route to Chiral Spirocycles via Organocatalytic Bromoetherification

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0646
Insights on Asymmetric Sulfoxidation Catalyzed by Imidodiphosphoric Acids

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0647
Aminothiourea-Catalyzed Asymmetric Isomerization

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Polymer-Supported Synthesis
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0649
Adhesive Immobilization of Polymer-Stabilized Pd Nanoparticles on Cellulose FREE ACCESS

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0650
Asymmetric Aldol Reaction Using Zirconium Phosphonate Supported l-Proline

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0651
Direct Borylation of Arenes Catalyzed by Ir(I)-bpy-PMO

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0652
Synthesis of Sulfones Using CuFe₂O₄ Magnetic Nanoparticles

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0653
Synthesis of Trisphenols with Tungstosilicic Acid in Water

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S-Arylation of Malononitrile–CS₂ Adduct Using CuO Nanoparticles

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0655
Asymmetric Henry Reaction with Block Copolymer Supported Copper(II)

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0656
Suzuki Coupling Using a Polystyrene-Supported Oxime Palladacycle

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Coupling of Epoxides and CO₂ with a Copper Azamacrocycle Based MOF

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0658
Reductive Amination of Nitriles with Platinum Nanowires

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0659
Regioselective Hydroaminomethylation of Styrenes Catalyzed by Rhodium

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0660
Aerobic Oxidation of Amines with Pd₃Pb/Al₂O₃

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0661
Biginelli Reaction Using Mn@PMO-IL

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