Synfacts

Issue 10 · October 2017

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A161
SYNFORM ISSUE 2017/10 FREE ACCESS

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Synthesis of Natural Products and Potential Drugs
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1005
Synthesis of Ciprofloxacin Hydrochloride in Continuous Flow

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1006
Synthesis of (+)-Dendrowardol C

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1007
Synthesis of (–)-Virosaine A FREE ACCESS

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1008
Synthesis of Pepluanol A

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1009
Total Synthesis of Dragonbloodins A1 and A2

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1010
Phase Separation Macrocyclization in the Synthesis of Vaniprevir

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1011
Enantioselective Synthesis of Polypyrrolo-indolines by Controlled Oligomerization

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1012
Synthesis of Protoilludane Natural Products

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1013
Biomimetic Total Synthesis of (±)-Naphthomevalin

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Synthesis of Heterocycles
z1015
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1015
Rhodium(III)-Catalyzed Indoline C–H Alkylation with Enones

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1016
Synthesis of Iodoquinolines from N-Tosyl-2-propynylamines

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1017
Borylketenimines in the Synthesis of Borylated Heterocycles

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1018
Synthesis of 1-Substituted 2-Azaspiro[3.3]-heptanes

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1019
Synthesis of Oxindoles Containing Trifluoromethyl Quaternary Carbon Centers

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1020
Synthesis of Fluoropyrrolidines by Using an Iodine/Hydrogen Fluoride Reagent

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1021
Click Synthesis of 1-Aza-2,3,4-triphospholenes

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1022
Synthesis of 3-Substituted Phthalides by Reductive Hydroiodination

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1023
Synthesis of the Tetracyclic Core of Secoyohimbane Alkaloids

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1024
Silver-Catalyzed Oxidative Decarboxylation Route to Diﬂuorooxindoles

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1025
Synthesis of Furan and Pyrrole Derivatives by Oxetane Ring Opening

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1026
One-Pot Synthesis of Thieno[3,2-b]pyridines

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Synthesis of Materials and Unnatural Products
z1027
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1027
Mission Accomplished: Synthesis of ‘Flexible’ Ladder Polymers FREE ACCESS

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1028
Two Steps to Loops

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1029
Coupling N-Trimethylsilyl-carbazole

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1030
A New Twist in Ladder Polymers

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1031
Flipping the Switch on Monomer Reactivity

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1032
Chiral Recognition with Hydrohelicenes

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1033
Silicon Makes Perylene Diimides See Red

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1034
Pioneering Electrophilic Alkyne Polyhydroamination

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1035
Salt-Free Polymerization Yields Fluorinated Poly(aryl thioether)s

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1036
Four-Membered Heterocycles from Ynamide

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1037
Indolyne Cyclotrimerization

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1038
Expanding Functionality of Indole and Pyrrole the Electrophilic Way

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
z1039
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1039
Enantioselective Functionalization of Internal Alkenes FREE ACCESS

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1040
A Nickel-Catalyzed Dearomative Reductive Heck Reaction of Indoles

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1041
Palladium-Catalyzed Synthesis of Alkylidenecyclobutanes FREE ACCESS

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1042
Enantioselective Oxytrifluoromethylation of Alkenes

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1043
Iridium-Catalyzed Asymmetric Synthesis of Allylated Aliphatic Esters

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1044
Enantioselective Palladium-Catalyzed Synthesis of Biaryl Atropisomers

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1045
Stereoselective Negishi Coupling of Oxiranyl Zincates Using Flow Chemistry

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1046
Palladium-Catalyzed Enantioselective Allylic Aminations of Vinylbenzoxazinones

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1047
Copper-Catalyzed Vinylogous Propargylation of Coumarins

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1048
Cobalt-Catalyzed Asymmetric Hydrosilylation of Alkenes

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1049
Dual Catalysis for Enantioselective Allylic Alkylation of Amino Acids

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1050
Asymmetric Nucleophilic Addition of Phosphites to 2H-Azirines

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1051
Yttrium-Catalyzed C(sp³)–H Addition to Cyclopropenes

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1052
Titanium-Catalyzed Enantioselective S-Oxidation of 1,5-Benzothiazepines

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1053
Divergent Synthesis of Tricyclic Ketals and Triarylmethanes

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1054
Nickel-Catalyzed Suzuki–Miyaura Coupling of CF₃O-Containing Benzyl Bromides

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1055
Generation of Allylboron Reagents in situ for the Synthesis of Chiral Oxaborenes

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1056
Palladium-Catalyzed Enantioselective Reaction of Allenyl Nitriles with Imines

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1057
Copper-Catalyzed Synthesis of Chiral Hydroxy Bis(boronates)

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1058
Asymmetric Nickel-Catalyzed Hydrogenation of β-Acylamino Nitroolefins

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1059
Spirofused Phenols by Enantioselective Dearomatization Using Silver Carbenes

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1060
Copper-Catalyzed Asymmetric exo-Selective [3+2] Cycloaddition Reaction

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1061
Chiral Rhodium-Catalyzed Asymmetric [2+2] Photocycloaddition

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1062
Rhodium-Catalyzed Asymmetric Synthesis of Seven-Membered Cyclic Amines

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1063
Synthesis of Chiral Homoallylic Alcohols by a Palladium-Catalyzed Cascade Reaction

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1064
Stereoselective Formation of Tertiary Alcohols and Ethers by Opening of Vinylic Carbonates

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1065
Manganese-Catalyzed Asymmetric Reduction of Ketones

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1066
Copper-Catalyzed Dearomatic Enantioelective Propargylation of Phenols

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1067
Zinc-Catalyzed Addition of Terminal Alkynes to α-Keto Esters

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1068
Palladium-Catalyzed Conjugate Addition of Arylboronic Acids

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Metal-Mediated Synthesis
z1069
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1069
Intermolecular Carbosulfonylation of Terminal Alkynes

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1070
Cobalt-Catalyzed Cross-Coupling of Alkyl Fluorides

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1071
Cross-Coupling of Tertiary Organoboron Nucleophiles

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1072
Selective Nickel/Photoredox Cross-Coupling

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1073
A Boron Alkylidene–Alkene Cycloaddition

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1074
Organometallic Additions to Imines and Nitriles Using Water Catalysis

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1075
Diastereo- and Enantioselective Synthesis of β-Aminoboronate Esters

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1076
Oxidative [1,2]-Brook Rearrangements via Hypervalent Silicon Intermediates

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1077
Selective Additions of Allyl Groups to N–H Ketimines

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1078
Coupling of Arylboronic Acids with Isocyanides

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1079
Synthesis of Unsymmetrical Tertiary Phosphine Oxides

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1080
Monofluoromethylthiolation with S-(Fluoromethyl) Benzenesulfonothioate

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1081
Enantiospecific Couplings of Boronic Esters with ortho-Lithiated Benzylamines

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1082
Trifluoromethylation of Alkyl Halides

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1083
Suzuki–Miyaura Coupling of Nitroarenes

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Organo- and Biocatalysis
z1085
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1085
Highly Enantioselective Organocatalysis with a Mechanically Interlocked Molecule FREE ACCESS

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1086
A Light-Driven Organocatalytic Aldol Desymmetrization Strategy

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1087
Organocatalytic Enantioselective Intramolecular Povarov Reaction of Anilines

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1088
Enzyme-Catalyzed Direct Alkylation of Amines with Alcohols

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1089
Regioselective Organocatalytic Hydroformylation of Aryl Alkenes

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1090
Biocatalytic Access to Challenging Tryptophan Analogues

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1091
Amine-Catalyzed Mannich Reactions with Activated Ketimines

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1092
Asymmetric Cycloadditions of Nitrile Oxides to o-Hydroxystyrenes

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1093
Oxidative [4+3] Cycloaddition of Allenamides and Furans

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1094
Biocatalyzed Formal Anti-Markovnikov Alkene Hydroamination and Hydration

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Polymer-Supported Synthesis
z1095
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1095
Chemoselective Hydrogenation of Functionalized Nitroarenes to Anilines FREE ACCESS

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1096
Photocatalytic Suzuki–Miyaura Coupling under Near-Infrared Light

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1097
Palladium Nanoparticle Catalyzed Chemoselective Reduction of β-Nitro Enones

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1098
Alkylation of Quinolines on Carbon-Supported Cobalt Oxide Nanocatalysts

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1099
Asymmetric Reduction of Imines on a Polystyrene-Supported Organocatalyst

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1100
Nanoporous Gold Catalyzed 1,2-Reduction of α,β-Unsaturated Aldehydes

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1101
Polymer-Supported Photosensitizers for Aerobic Photooxidations by LED Light

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1102
C–H Arylation of 2-Phenylpyridines on Carbon Nanotube Supported Pd Nanoparticles

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1103
Stille and Mizoroki–Heck Reactions on a C@Fe₃O₄ Nanosphere Supported Pd Catalyst

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1104
Dehydrogenative Coupling on Organic Sponge Supported Rose Bengal

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1105
Cycloaddition of 2-Vinylphenols on a Metal–Organic Framework Catalyst

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1106
Porphyrin-Based Metal–Organic Framework Copper Catalyst for C–N Bond Formation

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1107
Decarboxylative Cross-Coupling on Supported Copper(I) Iodide

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1108
Palladium-Catalyzed Suzuki–Miyaura Coupling and Hydrogenation

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1109
Niobic Acid Catalyzed Cyclization of Dicarboxylic Acids

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