Synthesis

Issue 23 · December 2019

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table of contents
V
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Synform
A184
Zanda, Matteo:
SYNFORM ISSUE 2019/12
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review
4311
Dénès, Fabrice; Farard, Julien; Lebreton, Jacques:
Synthesis of ¹³C-Labeled Steroids

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short review
4338
Rakitin, Oleg A.:
Recent Developments in the Synthesis of 1,2,5-Thiadiazoles and 2,1,3-Benzothiadiazoles

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PDF (341 kb)
feature
4348
Li, Fang; He, Feifei; Koenigs, Rene M.:
Catalyst-Free [2,3]-Sigmatropic Rearrangement Reactions of Photochemically Generated Ammonium Ylides

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psp
4359
Zilate, Bouthayna; Fischer, Christian; Schneider, Lukas; Sparr, Christof:
Scalable Synthesis of Acridinium Catalysts for Photoredox Deuterations

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special topic
4366
Special Topic Cover Page

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4368
Sutherland, Andrew:
Radiohalogenation of Organic Compounds: Practical Considerations and Challenges for Molecular Imaging

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PDF (330 kb)
4374
Milicevic Sephton, Selena; Zhou, Xiaoyun; Thompson, Stephen; Aigbirhio, Franklin I.:
Preparation of the Serotonin Transporter PET Radiotracer 2-({2-[(Dimethylamino)methyl]phenyl}thio)-5-[¹⁸F]fluoroaniline (4-[¹⁸F]ADAM): Probing Synthetic and Radiosynthetic Methods

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PDF (219 kb)

Supplementary Material

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4385
Kitahara, Kazumasa; Mizutani, Haruna; Iwasa, Seiji; Shibatomi, Kazutaka:
Asymmetric Synthesis of α-Chloro-α-halo Ketones by Decarboxylative Chlorination of α-Halo-β-ketocarboxylic Acids

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4393
Dubost, Emmanuelle; Babin, Victor; Benoist, Florian; Hébert, Alexandra; Pigrée, Gilbert; Bouillon, Jean-Philippe; Fabis, Frédéric; Cailly, Thomas:
Improvements of C–H Radio-Iodination of N-Acylsulfonamides toward Implementation in Clinics

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4401
Thompson, Stephen; Lee, So Jeong; Jackson, Isaac M.; Ichiishi, Naoko; Brooks, Allen F.; Sanford, Melanie S.; Scott, Peter J. H.:
Synthesis of [¹⁸F]-γ-Fluoro-α,β-unsaturated Esters and Ketones via Vinylogous ¹⁸F-Fluorination of α-Diazoacetates with [¹⁸F]AgF

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4408
Sarie, Jérôme C.; Neufeld, Jessica; Daniliuc, Constantin G.; Gilmour, Ryan:
Willgerodt-Type Dichloro(aryl)-λ³-Iodanes: A Structural Study

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paper
4417
Wimberger, Laura; Kratz, Thilo; Bach, Thorsten:
Photochemical Deracemization of Chiral Sulfoxides Catalyzed by a Hydrogen-Bonding Xanthone Sensitizer

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PDF (911 kb)

Supplementary Material

Supporting Information (PDF)

Primary Data
Primary Data (ZIP)
4425
Jian, Yong; Chen, Ming; Yang, Chao; Xia, Wujiong:
Nitroacenaphthene as a New Photocatalyst for the Synthesis of Sulfonyl Amidines

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Supplementary Material

Supporting Information (PDF)
4434
Roy, Deblina; Panda, Gautam:
Base-Mediated 1,6-Aza-Michael Addition of Heterocyclic Amines and Amides to para-Quinone Methides Leading to Meclizine-, Hydroxyzine- and Cetirizine-like Architectures
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4443
Mendoza, Manuel; Eom, Ryan; Salas, Celeste; Haynes-Smith, Jeremy; Billingsley, Kelvin L.:
The Synthesis and Biological Evaluation of Indolactam Alkaloids

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4452
Heinz, Benjamin; Balkenhohl, Moritz; Knochel, Paul:
Thiolation of Pyridine-2-sulfonamides using Magnesium Thiolates

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4463
Isbera, Mostafa; Bognár, Balázs; Gulyás-Fekete, Gergely; Kish, Krisztina; Kálai, Tamás:
Syntheses of Pyrazine-, Quinoxaline-, and Imidazole-Fused Pyrroline Nitroxides
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4473
Mangaonkar, Saeesh R.; Singh, Fateh V.:
Hypervalent Iodine(III)-Catalyzed Epoxidation of β-Cyanostyrenes

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4487
Jiang, Gan; Lin, Yang; Cai, Mingzhong; Zhao, Hong:
Recyclable Heterogeneous Copper(II)-Catalyzed Oxidative Cyclization of 2-Pyridine Ketone Hydrazones Towards [1,2,3]Triazolo[1,5-a]pyridines

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4498
Rodrigues, Shirley M. M.; Previdi, Daniel; Baviera, Giovanni S.; Matias, Alexandre A.; Donate, Paulo M.:
Niobium Pentachloride Mediated (Hetero)aromatic Aldehyde Friedel–Crafts Hydroxyalkylation with Arenes: An Efficient Strategy to Synthesize Triarylmethanes

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Synthesis

Linked PDF of Table of Contents

SYNFORM ISSUE 2019/12

Synthesis of ¹³C-Labeled Steroids

Recent Developments in the Synthesis of 1,2,5-Thiadiazoles and 2,1,3-Benzothiadiazoles

Catalyst-Free [2,3]-Sigmatropic Rearrangement Reactions of Photochemically Generated Ammonium Ylides

Scalable Synthesis of Acridinium Catalysts for Photoredox Deuterations

Special Topic Cover Page

Radiohalogenation of Organic Compounds: Practical Considerations and Challenges for Molecular Imaging

Preparation of the Serotonin Transporter PET Radiotracer 2-({2-[(Dimethylamino)methyl]phenyl}thio)-5-[¹⁸F]fluoroaniline (4-[¹⁸F]ADAM): Probing Synthetic and Radiosynthetic Methods

Asymmetric Synthesis of α-Chloro-α-halo Ketones by Decarboxylative Chlorination of α-Halo-β-ketocarboxylic Acids

Improvements of C–H Radio-Iodination of N-Acylsulfonamides toward Implementation in Clinics

Synthesis of [¹⁸F]-γ-Fluoro-α,β-unsaturated Esters and Ketones via Vinylogous ¹⁸F-Fluorination of α-Diazoacetates with [¹⁸F]AgF

Willgerodt-Type Dichloro(aryl)-λ³-Iodanes: A Structural Study

Photochemical Deracemization of Chiral Sulfoxides Catalyzed by a Hydrogen-Bonding Xanthone Sensitizer

Nitroacenaphthene as a New Photocatalyst for the Synthesis of Sulfonyl Amidines

Base-Mediated 1,6-Aza-Michael Addition of Heterocyclic Amines and Amides to para-Quinone Methides Leading to Meclizine-, Hydroxyzine- and Cetirizine-like Architectures

The Synthesis and Biological Evaluation of Indolactam Alkaloids

Thiolation of Pyridine-2-sulfonamides using Magnesium Thiolates

Syntheses of Pyrazine-, Quinoxaline-, and Imidazole-Fused Pyrroline Nitroxides

Hypervalent Iodine(III)-Catalyzed Epoxidation of β-Cyanostyrenes

Recyclable Heterogeneous Copper(II)-Catalyzed Oxidative Cyclization of 2-Pyridine Ketone Hydrazones Towards [1,2,3]Triazolo[1,5-a]pyridines

Niobium Pentachloride Mediated (Hetero)aromatic Aldehyde Friedel–Crafts Hydroxyalkylation with Arenes: An Efficient Strategy to Synthesize Triarylmethanes