Synthesis

Issue 08 · April 2020

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table of contents
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review
1147
Zambroń, Bartosz K.:
Internal Chelation within Functionalized Organoindium Reagents: Prospects for Regio- and Stereocontrol in the Allylation, Propargylation and Allenylation of Carbonyl Compounds

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short review
1181
Zhu, Yannan; Huang, You:
Organocatalyzed [3+3] Annulations for the Construction of Heterocycles

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feature
1203
Li, Dong; Lv, Shujun; Qu, Jingping; Zhou, Yuhan:
Oxidation of 4-Aryl-1,1,1-trifluorobut-2-en-2-yl Trifluoromethanesulfonates by 4-Picoline-N-Oxide: A Novel Approach to β-Trifluoromethyl-α,β-enones

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psp
1211
Mulks, Florian F.; Heckershoff, Robin; Zimmer, Marc; Hashmi, A. Stephen K.:
Practical Preparation of Cyclopropenone 1,3-Propanediol Ketal

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special topic
1215
Connon, Robert; Carroll, Laura; Guiry, Patrick J.:
A Base-Promoted One-Pot Asymmetric Friedel–Crafts Alkylation/Michael Addition of 4-Substituted Indoles

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1223
Yang, Yuzhong; Zhou, Liwei; Yang, Xiumei; Luo, Xiai; Deng, Guobo; Yang, Yuan; Liang, Yun:
Synthesis of Phenanthrenes via Palladium-Catalyzed Three-Component Domino Reaction of Aryl Iodides, Internal Alkynes, and o-Bromobenzoic Acids

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1231
Henkel, Michael; Bach, Thorsten:
Annulation of Indoles with 1,n-Dibromoalkanes by a Pd(II)-Catalyzed and Norbornene-Mediated Reaction Cascade

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1239
Shen, Zican; Li, Chen; Mercado, Brandon Q.; Ellman, Jonathan A.:
Cobalt(III)-Catalyzed Diastereoselective Three-Component C–H Bond Addition to Butadiene and Activated Ketones
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1247
Lee, Sumin; Jang, Young Jin; Phipps, Erik J. T.; Lei, Honghui; Rovis, Tomislav:
Rhodium(III)-Catalyzed Three-Component 1,2-Diamination of Unactivated Terminal Alkenes

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1253
Sun, Manman; Li, Jinshan; Chen, Weida; Wu, Haijian; Yang, Jianguo; Wang, Zhiming:
Palladium-Catalyzed [4+2] Annulation of Aryl and Alkenyl Carboxamides with 1,3-Dienes via C–H Functionalization: Synthesis of 3,4-Dihydroisoquinolones and 5,6-Dihydropyridinones

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paper
1266
Dar’in, Dmitry; Khoroshilova, Olesya; Kantin, Grigory; Krasavin, Mikhail:
Realizing the Trifunctional Potential of Alkyl 4-Chloro-2-diazo-3-oxobutanoates: Convenient Assembly of 6,7-Dihydro-4H-[1,2,3]triazolo[5,1-c][1,4]thiazine Core

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1273
Choi, Anthony; Castle, Jemma; Saruengkhanphasit, Rungroj; Coldham, Iain:
Synthesis of Spirocyclic Amines by 1,3-Dipolar Cycloaddition of Azomethine Ylides and Azomethine Imines

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1279
Rajbongshi, Kamal K.; Ambala, Srinivas; Govender, Thavendran; Kruger, Hendrik G.; Arvidsson, Per I.; Naicker, Tricia:
Microwave-Accelerated N-Acylation of Sulfoximines with Aldehydes under Catalyst-Free Conditions
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1287
Dahlmann, Uwe; Vollhardt, K. Peter C.:
Oligoether-Substituted Derivatives of Carbon-Rich 1,4,7,10,13,16-Hexaethynyltribenzo[a,e,i]cyclododeca-5,11,17-triyne (C₃₆H₁₂) and 1,4,9,12-Tetrakis(ethynyl)dibenzo[a,g]cyclododeca-5,7,13,15-tetrayne (C₂₈H₈): Potential Precursors to the Circular [6]Phenylene (‘Antikekulene’) Frame

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1301
Qiu, Changfu; Yu, Heshui; Qiu, Chuanjiang; Li, Fangyi; Suo, Tongchuan; Wang, Chunhua; Bie, Songtao; Li, Zheng:
Metal-Free Halogenation of N-Substituted Enaminoesters and Enaminones: A Facile Access to Functionalized α,α-Dihaloimines

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