Synfacts

Ausgabe 09 · September 2021

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Ausgabe
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A139
SYNFORM ISSUE 2021/09 FREIER ZUGRIFF

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Synthesis of Natural Products and Potential Drugs
z959
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0959
Total Synthesis of (+)-Fortalpinoid A and (+)-Cephinoid H FREIER ZUGRIFF

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0960
Synthesis of (±)-Jujuyane

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0961
Synthesis of PF-06873600 FREIER ZUGRIFF

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0962
Divergent Synthesis of Pentacyclic Cytochalasans

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0963
2-Sulfinyl-Diazabicyclooctane Derivatives as β-Lactamase Inhibitors

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0964
Synthesis of BACE1 Inhibitor PF-06751979

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0965
Total Synthesis (+)-Samroiyotmycin A

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0966
Total Synthesis of (–)-Spiroxins A, C, and D

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0967
Synthesis of (–)-Halichondrin B

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0968
Synthesis of (±)-Paeoniflorigenin FREIER ZUGRIFF

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Synthesis of Heterocycles
z0969
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0969
Radical Azidation of Cyclopropenes

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0970
One-Pot, Two-Step Synthesis of Indole-Fused Diazepanones

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0971
Regioselective C–H Borylation via Minisci-Type Reaction

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0972
Synthesis of Fluoroalkylated Isoquinolinones via Cobalt-Catalyzed C–H Activation/Annulation

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0973
Synthesis of Multisubstituted Pyridines via Nickel Catalysis

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0974
One-Pot Knoevenagel Condensation–Reduction Reaction of 2,4-Dihydroxy Quinolines and Pyridines

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0975
Umpolung Strategy to Functionalize Pyridines/Quinolines via Phosphonium Intermediates

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0976
Rhodium(III)-Catalyzed Synthesis of Functionalized Dihydrobenzofurans

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0977
Catalyst-Free Amination of Quinoxalin-2-ones and Benzo[1,4]oxazin-2-ones by Visible Light

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0978
Heterogeneous Nickel Catalyst Promotes Indole Formation via Dehydrogenative Coupling

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0979
Eight-Membered Cyclic Amines via Morpholine Intermediates

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0980
Room-Temperature C–N Coupling with Aryl Chlorides

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Synthesis of Materials and Unnatural Products
z0981
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0981
May the ‘London Dispersion Force’ Be with You

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0982
Triple Oxa[7]Helicene With High Dissymmetry Factor

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0983
A Family of Benzothienothienothienoindoles

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0984
Mimicking Flavin in Polyaromatic Hydrocarbons

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0985
An Enantioselective Host for Carbohelicenes

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0986
Chemoselectivity of Nucleophilic Addition Controlled by Triple Helicene Geometry

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0987
Borane-Catalyzed Block Copolymerization and Selective Polycarbonate Degradation

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0988
Mild Synthesis of (E)-β-Amidovinyl Sulfones

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0989
Building the Cyclothianthrenes Family

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0990
Avoiding Cyanide in Cyanoformate Synthesis

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0991
Air Tautomerism Yielding Quinoidal Compounds

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0992
Pre-Polymerization Fluorine Functionalization of Polymers of Intrinsic Microporosity (PIMs)

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Metals in Synthesis
z993
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0993
Enamide Synthesis from Amides Using Tf₂O for Electrophilic Activation FREIER ZUGRIFF

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0994
Photocatalyzed Sulfinylation of Strong, Unactivated Aliphatic C(sp³)–H Bonds

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0995
Enantioconvergent Photoinduced Copper-Catalyzed Synthesis of Chiral Secondary Amides FREIER ZUGRIFF

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0996
Cobalt-Catalyzed Enantioselective Desymmetritive Cycloaddition Generating Pyridines

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0997
Iridium-Catalyzed Enantioselective Hydrocarbonation of Alkenes

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0998
Catalytic Asymmetric α-Arylation of Aldehydes

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0999
Aluminum-Catalyzed Borylation of Alkynes

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1000
Switchable endo/exo-Selectivity in a Nickel-Catalyzed Domino Heck Cyclization

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1001
[5+2] Annulation of 1-Indanones and Alkynes via Rhodium-Catalyzed C–C Activation

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1002
Pd/Cu Dual-Catalyzed Directed Carbonylative Arylborylation of Unactivated Alkenes

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1003
Selective Difluoroallylations with 3,3-Difluoroallyl Ammonium Salts

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1004
Allylation of 2-Azaallyls with Allyl Ethers

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1005
Electroreductive Nozaki–Hiyama–Kishi Reaction

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1006
Synthesis of Congested β-Stereogenic Amines via Asymmetric Iridium-Catalyzed Allylation of Nitroalkanes

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1007
Co-Catalyzed C–H Activation and Diastereoselective Annulation Cascade Towards the Synthesis of Indanes

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1008
Difluoromethylation of Alkenes

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1009
Photoinduced 1,2-Dicarbofunctionalization of Alkenes

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1010
Ligand Design for the Palladium-Catalyzed Cross-Coupling of Nitroarenes and Phenols

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1011
Enantioselective Dearomative Alkylation of 4-Methoxypyridinium Ions

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1012
Asymmetric [3+2] Cycloaddition via Rh/Pd Synergistic Catalysis

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1013
Difunctionalization of Alkenes via Copper Catalysis Generated Oxocarbenium Ion

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1014
Arylation and Alkenylation of Cyclopropanols

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1015
Enantioselective Reverse Hydroboration of α,β-Unsaturated Amides

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1016
Rhodium-Catalyzed Reactions of Boronic Acids with Cyclobutenes

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1017
1,4-Hydroboration of CF₃-Substituted Dienes via Copper Catalysis

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1018
Decarbonylative Sonogashira Cross-Couplings

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1019
The Hosomi–Sakurai Reaction FREIER ZUGRIFF

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1020
A Bifunctional Tautomeric Ligand for Pd-Catalyzed C(sp²)–H Hydroxylation Using Oxygen as the Oxidant

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Polymer-Supported Synthesis
z1021
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1021
C–H Oxidation of Hydrocarbons Catalyzed by Iron Immobilized on COF Nanospheres and NanoFilms

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1022
Asymmetric Ring-Opening and Hetero-Diels–Alder Reactions on a Supported Chiral Salen–Cr Complex

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1023
Aromatic Substitution in Water by Using a Polymeric Amphiphilic Additive FREIER ZUGRIFF

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1024
C–N and C–O Cross-Couplings of Aryl Iodides Catalyzed by Reusable Copper Nanoparticles

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1025
Hydrogenation and Tandem Reactions of Nitroarenes on N-Doped Carbon−Coated Cobalt Nanoclusters

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1026
Dynamic Kinetic Resolution with a Palladium Nanoparticle–Lipase Hybrid Catalyst

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1027
Catalyst-Free Electrochemical C-3 Formylation of Indoles in an Aqueous Biphasic System

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1028
Copper-Catalyzed Dehydrogenative Coupling of Primary Amines: Preparation of Amides and Imines

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1029
Transfer Vinylation of Alcohols by Butyl Vinyl Ether on DMF-stabilized Palladium Nanoparticles

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1030
Synthesis of Carboxylic Acids from Styrene Derivatives and Fatty Acids through Oxidative C=C Bond Cleavage

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1031
Heterogenized Photocatalyst for Condensation of 4-Hydroxycoumarin, Dimedones, and Benzaldehydes

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Organo- and Biocatalysis
z1033
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1033
Enzymatic Intra- and Intermolecular Hydroalkylations of Alkenes through Ground-State Electron Transfer FREIER ZUGRIFF

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1034
Tripeptide-Catalyzed N-Oxidation Enables Enantioselective Desymmetrization of Sulfoximines

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1035
Aminocatalytic α-Enantioselective Etherification of Branched Aldehydes

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1036
Efficient Access to Contiguously Substituted Tetrahydronaphthols through Dienamine Catalysis

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1037
Atropisomeric Multiaxis Aldehyde Permits Epoxidation of Nonactivated Olefins with H₂O₂ as the Oxidant

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1038
Prolinol-Derived Catalysts Mediate Route Towards Functionalized trans-Diels–Alder Products

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1039
Chiral N-Heterocyclic Carbene Bifunctional Organocatalyst for Aza-Michael Addition Reactions

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1040
Organophotocatalytic Hydroxymethylation of Secondary Alkyl Iodides

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1041
Enantioselective [2+2] Photocycloaddition Catalyzed by Sensitizer-Modified Chiral Phosphoric Acid

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1042
Organophotocatalytic Strict Temporally Controlled Cationic Polymerization of Vinyl Ethers

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Chemistry in Medicine and Biology
z1043
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1043
X-ray Irradiation Promoted Activation of Prodrugs FREIER ZUGRIFF

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1044
Go Bi-Steric for Selectivity

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1045
Goyazensolide, a Covalent Importin‑5 (IPO5) Inhibitor

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1046
Truncated Mycalolide B Analog to Prevent Cancer Metastasis

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1047
Macrodiolide Library Synthesis of cGAS-STING Inhibitors

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1048
Spiro-Trycyclic Alkaloids as nAChR Antagonists

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1049
Targeting Transcription Factors for Degradation

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1050
Fighting Malaria with Endoperoxides

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1051
Cyclic Disulfides as Selective Thioredoxin Probes

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1052
Total Synthesis of Pyrrolylpyrromethane Alkaloids with Antimalarial Activity

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1053
Total Synthesis and Configurational Assignment of Mutanobactin D

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1054
Total Synthesis and Structure-Activity Studies of Geodiamolide H

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1055
Drugging the Undruggable using Irreversible Covalent K-Ras G12C Inhibitors FREIER ZUGRIFF

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Peptide Chemistry
z1057
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1057
Solar Radiation-Assisted Peptide-Bond Formation FREIER ZUGRIFF

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1058
C(sp³)–H Functionalization for Modification of Peptides with Alanine at the C-Terminus

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1059
Nickel-Catalyzed Synthesis of α-Amino Acid Derivatives

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1060
Photocatalytic Phosphotyrosine Mimetic Functionalization of Peptides

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1061
Enantioselective Synthesis of α-Amino Acid Esters by Rhodium/Copper Catalysis

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1062
Photoredox Amidation of Tryptophan in Peptides

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1063
Late-Stage Palladium-Mediated N-Arylation of p-Aminophenylalanine in Unprotected Peptides

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1064
Hybrid Peptide Synthesis by Radical–Radical Coupling

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1065
Trimethylaluminum-Mediated Peptide Synthesis FREIER ZUGRIFF

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1066
Palladium(II)-Catalyzed C(sp²)–H Functionalization of Tryptophan and Tryptophan-Containing Peptides

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Flow Chemistry
z1067
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1067
Electrochemical Fluorination Reactions in Continuous Flow Using (Difluoroiodo)arene Mediators

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1068
Synthesis of α-Amino Acids by Electrochemical Carboxylation of Aldimines in a Flow System

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1069
Copper-Catalyzed Hydrosilylation of Alkynes and Alkenes under Blue LED Irradiation

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1070
Z-Selective Olefin Metathesis in Continuous Flow

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