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Synlett 1993; 1993(8): 587-588
DOI: 10.1055/s-1993-22540
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Synthesis of 1-Halo-1-fluoroalkanes

A. García Martínez* , J. Osío Barcina, A. Z. Rys, L. R. Subramanian
  • *Departamento de Química Orgánica, Facultad de Ciencias Químicas, Universidad Complutense, Ciudad Universitaria, E-28040 Madrid, Spain
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Publication History

Publication Date:
19 March 2002 (online)

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1-Halo-1-fluoroalkanes 4 (X= Cl, Br, I) can be straightforward prepared from aldehydes 1 by succcessive reaction of the corresponding gem-bistriflates 2 with tetrabutylammonium difluorotriphenylstannate at 0°C and then with tetrabutylammonium halides at room temperature.

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