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Synlett 1999; 1999(9): 1471-1473
DOI: 10.1055/s-1999-2877
DOI: 10.1055/s-1999-2877
letter
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Structure and Reactivity of Bis(iodozincio)methane in Tetrahydrothiophene
Further Information
Publication History
Publication Date:
31 December 1999 (online)
Addition of tetrahydrothiophene (THT) to THF solution of bis(iodozincio)methane modified the stability and reactivity: EXAFS analysis indicated that THF stabilizes bis(iodozincio)methane in a monomeric structure; the species reacts with acyl chlorides to give 1,3-diketones.
zinc - 1,3-diketone - dimetal - THT - EXAFS