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Synlett 2000; 2000(7): 1043-1045
DOI: 10.1055/s-2000-6683
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Palladium-Catalyzed Cross-Coupling Reaction of Tributyltin Hydride with Aryl Iodides: Formation of A Tin-Carbon Bond

Miki Murata* , Shinji Watanabe, Yuzuru Masuda
  • *Department of Materials Science, Kitami Institute of Technology, Kitami, 090-8507, Japan; Fax +81-1 57-26-49 73; E-mail: MASUDA-Yuzuru/mtrl@king.cc.kitami-it.ac.jp
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Publication Date:
31 December 2000 (online)

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Various aryl iodides were coupled with 2 equiv of tributyltin hydride (and/or 1.5 equiv of hexabutylditin) in the presence of potassium acetate and a catalytic amount of PdCl2(PMePh2)2 to afford the corresponding arylstannanes under mild conditions.

tin - hydrides - palladium - halides - Cross-coupling

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