Synfacts

Issue 12 · December 2006

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Synthesis of Natural Products and Potential Drugs
1193
Synthesis of Ciguatoxin (CTX1B)
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1194
Synthesis of (-)-Nigellamine A₂

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1195
Synthesis of Hepatitis C Polymerase Inhibitor

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1196
Synthesis of Amphidinolide X and Y

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1197
Syntheses of Guanacastepene E

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1198
Synthesis of (S)-Brevicolline

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1199
Synthesis of (+)-Streptazolin

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1200
Synthesis of (-)-Merrilactone A

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1201
Synthesis of Galbulimima Alkaloid 13

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1202
Synthesis of (+)-Lactacystin

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1203
Synthetic Approach to Otamixaban

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1204
Synthesis of (S)-Venlafaxine

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1205
Synthesis of Lu AA20465

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1206
Synthesis of (±)-Nominine

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1207
Synthesis of (±)-Salviasperanol

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Synthesis of Heterocycles
1209
Indolizinone and Quinolizinone via Asymmetric [2+2+2] Cycloaddition

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1210
Synthesis of Cyclic Amidines via Ru-Catalyzed Hydroamination

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1211
Synthesis of Tetracyclic ABCD Ring Cores of Camptothecins
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1212
Pyridazines by Acetylenic 1,2,4-Triazole Cyclization/Fragmentation

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1213
Rhenium-Catalyzed Synthesis of Isobenzofurans

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1214
Heteroring Annulation Using TandemN-Acylamide Methylenation-RCM

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1215
Organocatalytic and Stereoselective Synthesis of Bipyrazolidin-3-ones

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1216
Synthesis of Trifluoromethyl Pyrroles

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1217
Phenethylamine Trimerization to Pyrroles

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1218
A Regioselective Cycloaddition Route to Pyrazoles

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1219
Regiospecific 3-Arylation of Imidazo[1,2-a]pyrimidines

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1220
Pyrano- and Oxepinopyridines by RCM

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1221
Benzyne-Mediated Route to Benzoxazinones

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1222
Synthesis of Dihydrobenzoindazoles and Dihydrobenzoquinazolines

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1223
Titanium-Mediated Synthesis of N-Substituted 2-Arylpyrroles

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Synthesis of Materials and Unnatural Products
1225
A Squaramide-Based Citrate Receptor

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1226
Synthesis of Fluorescent Dialkynylboradiazaindacenes

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1227
Organopalladium Nanodroplets with Fluorous-Phase Core

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1228
A Precursor Detour Makes Processing Trouble-Free

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1229
Synthesis and Biradicaloid Character of Doubly Linked Corrole Dimers

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1230
Increasing Molecular Weight of a Helical Polymer through Polymerization in a Chiral Solvent

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1231
Insertion Polymerization of Cyclobutenes by Detouring Pericyclic Opening

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1232
Overcoming the Cationic Route

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1233
Preparation of N-Substituted Diaza[12]annulenes

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1234
Anion-Templated Macrocycle Synthesis

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1235
Copolymer Hosts for Selective Protein Recognition

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1236
Polymers for Light-Emitting Devices with Integrated Hole-Transporting Elements

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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
1237
Gold-Catalyzed Carboalkoxylation of Alkynes

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1238
Pd-Catalyzed Allylic Alkylation of Nitromethane and its Application

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1239
Catalytic Enantioselective Decarboxylation-Protonation
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1240
Bismuth-Catalyzed Synthesis of 2,6-Disubstituted Dihydropyrans

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1241
Cycloisomerizations of Ene-Ynamides Mediated by Gold

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1242
Spirophosphonites as Chiral Ligands for Enamine Hydrogenation

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1243
Cu(I)-Catalyzed Enantioselective Hydrosilylation of Aromatic Ketones

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1244
New Phosphine-Phosphoramidite Ligands for Hydrogenations

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1245
Diastereoselective Synthesis of Pyrrolidines and Prolines
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1246
Preparation of syn-1,2-Diols via Tandem Wittig Rearrangement/Aldol Reaction

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1247
Rh-Catalyzed One-Pot Conjugate Addition and Indium-Mediated Allylation

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1248
Stereoselective Gold-Catalyzed Sila-Cope Rearrangement

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1249
Cascade Radical Addition-Cyclization-Trapping Reactions

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1250
(H₈-BINOLate)Ti-Based Catalyzed Asymmetric Methallylation of Ketones

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1251
Stereoselective Allylic Alkylation with Azlactones Using Triphenylarsine

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1252
Rh(I)-Catalyzed Asymmetric Allylic Substitution with Boronic Acids

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1253
Asymmetric Preparation of anti-β-Hydroxyα-amino Acid Esters

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1254
Chiral 1,2-Diols via One-Pot Diboration/Hydroboration/Cross-Coupling

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1255
Enantioselective Lanthanoid-Catalyzed Cycloaddition Reactions

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1256
Aminophosphines with Axial Chirality for Asymmetric Catalysis

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1257
Pd(0)/Ir(I)-Catalyzed Sequential Allylic Isomerization and Substitution

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1258
Asymmetric Addition of in situ Formed Alkynylzincs to Ketones

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1259
Rhodium-Catalyzed Synthesis of Chiral Aryl Glycines

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1260
Rh(I)-Catalyzed Isomerization ofN-Allylaziridines to Z-Enamines

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1261
Iridium-Catalyzed Enantioselective Synthesis of Allylic Alcohols

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1262
Hydroformylation of Internal Alkenes by Encapsulated Rhodium

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1263
Synthesis of Enantiopure α-Trifluoromethyl Amine Derivatives

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1264
Enantioselective Conjugate Radical Addition

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Metal-Mediated Synthesis
1265
Highly Efficient Al-Catalyzed Alcohol Oxidation via Oppenauer Reaction
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1266
Stereoselectivity Reversal in Allylation ofN-tert-Butanesulfinyl Imines

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1267
Cr(II)-Mediated Cascade Reactions of tert-Trihalomethylcarbinols

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1268
Cu/Ag-Promoted Oxidative Amidation of Aldehydes with Amine Hydrochlorides

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1269
Metallation of Aryl Bromides Bearing a Potassium Trifluoroborate Moiety

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1270
Pd/Cu-Mediated Cyanation of Boronic Acids with Benzylthiocyanate

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1271
Diastereoselective Synthesis of anti-1,2-Diols from α-Silyloxyaldehydes

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1272
Synthesis of Chiral-β-Amino Esters via Titanium Ester Enolates

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1273
Hydroindation of 1,3-Dienes and One-Pot Allylation of Carbonyl Compounds

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1274
Asymmetric Allylboration of Ketones Catalyzed by Chiral Diols

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1275
Simple Lithiation of α,ω-Dihaloalkanes

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1276
Direct C-H Arylation of (Hetero)arenes with Aryl Iodides via Rhodium Catalysis

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1277
Arylation and Oxidative Esterification of Aldehydes with Siloxanes

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Organo- and Biocatalysis
1279
Theoretical Studies on the Bifunctionality of Thiourea-Based Organocatalysts
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1280
Brønsted Acid Catalyzed Aza-Diels-Alder Reaction

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1281
Ball-Milling Organocatalysis

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1282
l-Prolinamide-Catalyzed Enantioselective Synthesis of α-Hydroxyphosphonates

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1283
Organocatalytic Kinetic Resolution of Propargylic Alcohols

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1284
Enantioselective Ene Reaction Catalyzed by a Diphenylprolinol Silyl Ether

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1285
Bulky Cinchonine Derivatives as Phase-Transfer Catalysts in Vinylic Substitution Reactions

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Polymer-Supported Synthesis
1287
Polymer-Supported Synthesis of Hydroxamic Acids

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1288
scCO₂-Flow Asymmetric Hydrogenation

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1289
Solid-Phase Synthesis of PBD Dimers

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1290
Novel 3D Coordination Palladium-Network Complex

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1291
SBA-15-Supported Acid-Base Catalyst for Aldol Reaction

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1292
N-Heterocyclic Carbene-Au(I) Complexes Immobilized on Solid Supports

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1293
Polymer-Supported Non-Chiral and Homochiral Schrock Catalysts

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1294
Sulfonic Acid Functionalized Silica Catalyst for the Boc Protection of Amines

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1295
A Combinatorial Approach to Heterogeneous Asymmetric Aquacatalysis

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1296
Ring Opening and Expansion of Aziridines Using Silica-Water System

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1297
Polymer-Assisted Strategy for Deprotection of Protected Sugars

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1298
Asymmetric Aldol Reaction in Water Using Polystyrene-Supported Proline

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1299
A New Route to Polymer-Supported Allyltin Reagents

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