Synfacts
Issue 11 · November 2011
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A100
SYNFORM
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Synthesis of Natural Products and Potential Drugs
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1149
Synthesis of Rho-Kinase Inhibitor Y-27632
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1150
Synthesis of (+)-Przewalskin B
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1151
Synthesis of a γ-Secretase Modulator
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1152
Formal Synthesis of Ezetimibe
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1153
Synthesis of Spirastrellolide F Methyl Ester
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PDF (81 kb)
1154
Synthesis of HSD-016
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1155
Synthesis of (+)-Brevisamide
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1156
Synthesis of (±)-Hapalindoles K, A, and G
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1157
Synthesis of (+)-Awajanomycin
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1158
Synthesis of Febuxostat, Tafamadis, and Texaline
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1159
Synthesis of Cholesterol Transporter NPC1L1 Inhibitor
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1160
Synthesis of (±)-Communiol E
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1161
Synthesis of Synechoxanthin
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Synthesis of Heterocycles
z1163
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1163
Concise Palladium-Catalyzed Synthesis of Dibenzodiazepines
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1164
Synthesis of 1-Aroxyisoquinolines from Phenols and 2-Alkynylbenzaldoximes
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1165
Ru-Catalyzed Heteroannulation to Indoles, Dihydroisoquinolines, and Dihydroquinolines
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1166
[3+2] Cycloaddition to Pyrido[1,2-
b
]indazoles
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1167
Ruthenium-Catalyzed Synthesis of Phthalides in Water via C-H Alkenylation
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1168
One-Pot Cu-Catalyzed C-N Coupling Approach to Pyrido[1,2-
a
]benzimidazoles
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PDF (73 kb)
1169
Efficient Zinc-Mediated Heteroannulation Route to 3-Amidoindoles
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PDF (67 kb)
1170
Base-Mediated Intramolecular Aryne-Ene Cyclization
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1171
Synthesis of Benzoxazinones via Palladium-Catalyzed Intramolecular C-O Coupling
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1172
Copper-Catalyzed Three-Component Synthesis of Polysubstituted Pyrroles
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1173
Sonogashira-Hydroamination Route to 1,2,4-Trisubstituted Pyrroles
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1174
Gold-Catalyzed [3+2]-Cycloaddition Approach to 2,4,5-Trisubstituted Oxazoles
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1175
Microwave-Facilitated Synthesis of Pyrimidinones
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1176
Iron-Mediated Heteroannulation Route to Isochromenones
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1177
Pd-Catalyzed Heteroannulation Route to 4-Aminoquinazolines via C-H Amidination
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Synthesis of Materials and Unnatural Products
z1179
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1179
A Stabilized Singlet Biradical Compound
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1180
Alkynes
en Route
to Porphyrinoides
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1181
Substitute This!
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1182
A Facile Route to Polycylic Aromatic Hydrocarbons
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1183
‘Ticktock’ Cyclopolymerization
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1184
Polyaryl Mesobenzanthrones
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1185
Expanded Cyclo[8]pyrroles Made Easy
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1186
C
3
-Symmetric Chromophores with 6,5,5-Fused Ring Systems
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1187
High-Yielding Thermal [2+2] Addition to Fullerene
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1188
Controlling Calixarene Size with Metal Salts: The First Brønsted-Free Synthesis
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1189
Ultra-Low Bandgap Donor-Acceptor Polymers Based on Pyromellitic Diimide
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1190
Conjugated Polymers via Aroyl Chloride-Alkyne Polymerization
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1191
Acenaphthene-Fused Phospholes with Enhanced Electronic Properties
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Metal-Catalyzed Asymmetric Synthesis and Stereoselective Reactions
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1193
Novel Ligand for Rh-Catalyzed Asymmetric Conjugate Addition
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1194
Ni-Catalyzed Reductive Cycloaddition
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1195
Gold-Catalyzed Enantioselective Protonation
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1196
Pd-Catalyzed Enantioselective Allylic Etherizations of Oximes
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1197
Tandem Catalytic Allylic Amination and [2,3]-Stevens Rearrangement of Tertiary Amines
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1198
A One-Pot Synthesis of Challenging Chiral Primary Amines
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1199
Copper-Catalyzed Asymmetric 1,3-Dipolar Cycloadditions
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1200
Iron-Catalyzed Oxidative Kinetic Resolution of Secondary Alcohols
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1201
Thermally-Induced Cycloadditions of Diazo Compounds and Alkenes
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1202
Combined C-H Functionalization/Cope Rearrangement with Vinyl Ethers
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1203
Enantioselective Alder-Ene Reactions towards Dihydrobenzofurans
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1204
Pd-Catalyzed Chemo- and Regioselective Allylic Alkylation
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1205
Silver-Catalyzed Enantioselective 1,3-Dipolar Cycloaddition
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1206
Iridium-Catalyzed Asymmetric Allylations
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1207
Palladium-Catalyzed Allylic C-H Oxidation
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1208
3-Aminochroman Derivatives via Ruthenium-Catalyzed Asymmetric Hydrogenation
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1209
New Ligands for Catalytic Asymmetric NHK Allylation of Aldehydes
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1210
Yb-Catalyzed Asymmetric Conjugate Allylation of Coumarins
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1211
Domino Knovenagel/Pinner/Friedel-Crafts Synthesis of Chiral Chromenes
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1212
Hetero-Diels-Alder Reaction of Brassard’s Diene and Aliphatic Aldehydes
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1213
Novel Phosphorus Amidite-Olefin Ligands for Allylic Alkylation of Indoles
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1214
Co-Catalyzed Conjugate Addition of Alkynes to α,β-Unsaturated Ketones
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1215
Use of 1,2,4-Triazolyl-1,2,3-Triazoles as Carbene Precursors
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1216
Kinetic Resolution of Morita-Baylis-Hillman Adducts by 1,4-Addition
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1217
Zirconium-Catalyzed Enantioselective Friedel-Crafts Alkylation of Pyrroles
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1218
Tetradentate Amine Ligands for Asymmetric Friedel-Crafts Alkylations
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1219
Pd-Catalyzed Asymmetric Intramolecular Arylation of α-Keto Amides
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1220
One-Pot Domino Ring Opening/C-N Bond Formations
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1221
Rhodium-Catalyzed Asymmetric 1,4-Addition of Arylboronic Acids
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1222
Asymmetric Ene Reaction by La/Ag Heterobimetallic Cooperative Catalysis
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Metal-Mediated Synthesis
z1223
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1223
Pd-Catalyzed Direct Alkynylation of Aliphatic C-H Bonds
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1224
In-Promoted Approach to Synthetic Equivalents of Hydroxyacetone Enolates
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1225
One-Pot Synthesis of Functionalized Arylboronic Acids
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1226
CuCl-Catalyzed β-Boration of α,β-Unsaturated Carbonyl Compounds
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1227
Base-Mediated Transition-Metal-Free Alkynylation of Aryl Chlorides
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1228
Asymmetric Allylic Substitution
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1229
Chiral C(sp
³
) Boronate Building Blocks
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1230
γ-Selective Cross-Coupling of Allylic Silanolate Salts
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1231
Synthesis of Multialkylated Olefins through Carbozirconation and Coupling
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1232
Ti-Mediated Coupling of Amines with Grignard Reagents
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1233
Oxidation of Silyl Enol Ethers with Metal Nitrites
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1234
CuCl
2
-Mediated Chlorocyclization and Oxidative Aromatization Cascade
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1235
Lithium Cuprate Ion Pairs as a Key to Control Diastereoselectivity
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1236
CuCF
3
Aromatic Trifluoromethylating Agents
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1237
Ag-Mediated C
aryl
-OCF
3
Bond Formation
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1238
Trifluoromethylation of Aromatic Isoxazoles
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Organo- and Biocatalysis
z1239
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1239
Catalytic Enantioselective Oxaziridination
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1240
Asymmetric Synthesis of Spirooxindoles
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1241
Thiourea-Catalyzed Intramolecular [5+2] Cycloadditions
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1242
Desymmetrization of Cyclohexadienones via Cinchonine-Derived Thiourea
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1243
Synthesis of Aryl Alkyl Sulfides by γ-Addition of Aryl Thiols to Allenoates
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1244
α-Alkylation of Aldehydes by Oxidative Coupling with Molecular Oxygen
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1245
Phosphoramide-Catalyzed Michael Addition of Oxindoles to Nitroolefins
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1246
Electrophilic Reactivities of Photo-Generated α,β-Unsaturated Iminium Ions
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1247
Catalytic Enantioselective Desymmetrization of
meso
-Diamines
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Polymer-Supported Synthesis
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1249
Silane Oxidation Catalyzed by Carbon Nanotube-Gold Nanohybrids
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1250
Oxidation of Alcohols with PMO-Supported Oxo-Vanadium Schiff Base
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1251
Silica-Supported Polyimidazolium Pd Catalysts for Suzuki-Miyaura Coupling
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1252
Denitrogenative Deuteration of Solid-Supported Triazenes
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1253
Suzuki-Miyaura Coupling in Water with Pd@CSP
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1254
Synthesis of Unsymmetrical Sulfides with CuO Nanoparticles
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1255
Polyethylene Oligomer Supported Olefin Metathesis Catalysts
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1256
Reduction of Nitro Compounds with N
2
H
4
˙H
2
O Using Fe
3
O
4
Nanoparticles
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1257
A Recyclable Polystyrene-Supported Gold(I) Catalyst
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1258
Synthesis of 1,2,4,5-Tetrasubstituted Imidazoles with Silica-Bonded PPSA
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1259
Copper Nanoparticles on Activated Carbon for Click Chemistry
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1260
A Polymeric Bimetallic Catalyst for
N-Alkylation of Amines with Alcohols
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1261
Transfer Hydrogenation with Immobilized Wilkinson’s Catalyst
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1262
Borylation of Aryl Halides with Silica-SMAP/Pd
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Addenda and Errata
1263
Fe-Catalyzed Phenanthrene Synthesis via [4+2] Benzannulation
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1263
Palladium-Catalyzed C-H Activation Induced Enantioselective Route to Fused Indolines
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1264
Dysprosium(III) Triflate Catalyzed Aza-Piancatelli Rearrangement
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1264
Organocatalytic Enantioselective Fluorocyclizations
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