Synthesis

Issue 11 · July 2005

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review
1727
Rendler, Sebastian; Oestreich, Martin:
Hypervalent Silicon as a Reactive Site in Selective Bond-Forming Processes

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short paper
1748
De, Surya K.; Gibbs, Richard A.:
Ruthenium(III) Chloride-Catalyzed One-Pot Synthesis of 3,4-Dihydropyrimidin-2-(1H)-ones under Solvent-Free Conditions

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paper
1751
Frick, Jeffrey A.; Klassen, John B.; Rapoport, Henry:
Diastereo- and Enantioselective Synthesis of 2-Substituted 1-Aminocyclopropane-1-Carboxylic Acids. Application to the Synthesis of Protected 2,3-Methano Analogs of Ornithine and Glutamic Acid

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1757
Zhang, Suhong; Xu, Liang; Trudell, Mark L.:
Selective Oxidation of Benzylic Alcohols and TBDMS Ethers to Carbonyl Compounds with CrO₃-H₅IO₆

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1761
Yavari, Issa; Souri, Sanaz; Sirouspour, Mehdi; Djahaniani, Hoorieh; Nasiri, Farough:
Synthesis of Alkyl 3-Aryloxypropenoates and Alkyl 2-Arylacrylates through Nucleophilic Addition to Alkyl Propiolates

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1765
Norlin, Rikard; Juhlin, Lars; Lind, Per; Trogen, Lars:
α-Haloenamines as Reagents for the Conversion of Phosphorus Oxyacids to Their Halogenated Analogues

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1771
Mallegol, Thomas; Gmouh, Said; Meziane, Mohamed Aït Amer; Blanchard-Desce, Mireille; Mongin, Olivier:
Practical and Efficient Synthesis of Tris(4-formylphenyl)amine, a Key Building Block in Materials Chemistry

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1775
Akhlaghinia, Batool; Tavakoli, Sedigheh:
An Efficient Method for the Protection of Alcohols and Phenols by Using Hexamethyldisilazane in the Presence of Cupric Sulfate Pentahydrate under Neutral Reaction Conditions

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1779
Pradhan, Prasun K.; Dey, Sumit; Giri, Venkatachalam Sesha; Jaisankar, Parasuraman:
InCl₃-HMTA as a Methylene Donor: One-Pot Synthesis of Diindolylmethane (DIM) and Its Derivatives

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1783
Sherman, Andrei A.; Yudina, Olga N.; Komarova, Bozhena S.; Tsvetkov, Yury E.; Iacobelli, Stefano; Nifantiev, Nikolay E.:
Preparative Route to Per-O-acetylated N-Acetyl- and N-(tert-Butoxycarbonyl)neuraminyl-α-(2→3)-galactosyl Disaccharide Glycosyl Donors by Regioselective Acetolysis of Sialyl-α-(2→3′)-lactose

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1789
ter Wiel, Matthijs K. J.; Feringa, Ben L.:
Synthesis of Functionalized Molecular Motors

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1797
Hofmann, Tatjana; Zweig, Karin; Engels, Joachim W.:
A New Synthetic Approach for the Synthesis of N²-Modified Guanosines

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1801
Das, Jagattaran; Patil, Santoshkumar N.; Awasthi, Riti; Narasimhulu, C. Prasad; Trehan, Sanjay:
An Easy Access to Aryl Azides from Aryl Amines under Neutral Conditions

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1807
Enders, Dieter; Moll, Alexander:
Asymmetric Synthesis of cis-3,4-Disubstituted β-Sultams

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1817
Dousson, Cyril B.; Heron, Nicola M.; Hill, George B.:
Valuable Synthetic Building Blocks: Useful 2-Substituted 5-Aminopyrimidines from a Stable Precursor

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1822
Frangin, Yves; Montigny, Frédéric:
Synthesis of Symmetrical Polyenes by Allylzincation

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1829
Stončius, Arvydas; Nahrwold, Markus; Sewald, Norbert:
Chiral Succinate: A Precursor for Enantiomerically Pure β²-Amino Acids

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1838
Metten, Bert; Smet, Mario; Boens, Noël; Dehaen, Wim:
Synthesis of APTRA Derivatives as Building Blocks for Low-Affinity Fluorescent Ca²⁺ Indicators

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1845
Ghosh, Tarun; Saha, Satyajit; Bandyopadhyay, Chandrakanta:
Synthesis of 2,2′-Diaminobischromones Using a Modified Procedure for the Rearrangement of 5-(2-Hydroxyphenyl)isoxazole to 2-Aminochromone

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1850
Wegert, Anita; Miethchen, Ralf; Hein, Martin; Reinke, Helmut:
Organofluorine Compounds and Fluorinating Agents, Part 33: Regioselective Chlorodifluoromethylations in the 1-Position of 1,2-Unsaturated Monosaccharide Derivatives

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1859
Boltukhina, Ekaterina V.; Zubkov, Fedor I.; Nikitina, Eugenia V.; Varlamov, Alexey V.:
Novel Approach to Isoindolo[2,1-a]quinolines: Synthesis of 1- and 3-Halo-Substituted 11-Oxo-5,6,6a,11-tetrahydroisoindolo[2,1-a]quinoline-10-carboxylic Acids

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1876
Koshkin, A. V.; Lokshin, V.; Samat, A.; Gromov, S. P.; Fedorova, O. A.:
One-Pot Synthesis of 6′-Amino-Substituted Spirooxazines

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1881
Mishra, Jitendra Kumar; Panda, Gautam:
A Convenient Two-Step Synthesis of Amino Acid Derived Chiral 3-Substituted [1,4]Benzodiazepin-2-ones

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feature article
1888
Lesch, Bernhard; Toräng, Jakob; Nieger, Martin; Bräse, Stefan:
The Diels-Alder Approach towards Cannabinoids

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practical synthetic procedures
1901
Paquet, Valérie; Lebel, Hélène:
Rhodium-Catalyzed Synthesis of Terminal Alkenes

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book review
1906
Waldvogel, Siegfried R.:
Synthesis of Biaryls
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Synthesis

Hypervalent Silicon as a Reactive Site in Selective Bond-Forming Processes

Ruthenium(III) Chloride-Catalyzed One-Pot Synthesis of 3,4-Dihydropyrimidin-2-(1H)-ones under Solvent-Free Conditions

Diastereo- and Enantioselective Synthesis of 2-Substituted 1-Aminocyclopropane-1-Carboxylic Acids. Application to the Synthesis of Protected 2,3-Methano Analogs of Ornithine and Glutamic Acid

Selective Oxidation of Benzylic Alcohols and TBDMS Ethers to Carbonyl Compounds with CrO₃-H₅IO₆

Synthesis of Alkyl 3-Aryloxypropenoates and Alkyl 2-Arylacrylates through Nucleophilic Addition to Alkyl Propiolates

α-Haloenamines as Reagents for the Conversion of Phosphorus Oxyacids to Their Halogenated Analogues

Practical and Efficient Synthesis of Tris(4-formylphenyl)amine, a Key Building Block in Materials Chemistry

An Efficient Method for the Protection of Alcohols and Phenols by Using Hexamethyldisilazane in the Presence of Cupric Sulfate Pentahydrate under Neutral Reaction Conditions

InCl₃-HMTA as a Methylene Donor: One-Pot Synthesis of Diindolylmethane (DIM) and Its Derivatives

Preparative Route to Per-O-acetylated N-Acetyl- and N-(tert-Butoxycarbonyl)neuraminyl-α-(2→3)-galactosyl Disaccharide Glycosyl Donors by Regioselective Acetolysis of Sialyl-α-(2→3′)-lactose

Synthesis of Functionalized Molecular Motors

A New Synthetic Approach for the Synthesis of N²-Modified Guanosines

An Easy Access to Aryl Azides from Aryl Amines under Neutral Conditions

Asymmetric Synthesis of cis-3,4-Disubstituted β-Sultams

Valuable Synthetic Building Blocks: Useful 2-Substituted 5-Aminopyrimidines from a Stable Precursor

Synthesis of Symmetrical Polyenes by Allylzincation

Chiral Succinate: A Precursor for Enantiomerically Pure β²-Amino Acids

Synthesis of APTRA Derivatives as Building Blocks for Low-Affinity Fluorescent Ca²⁺ Indicators

Synthesis of 2,2′-Diaminobischromones Using a Modified Procedure for the Rearrangement of 5-(2-Hydroxyphenyl)isoxazole to 2-Aminochromone

Organofluorine Compounds and Fluorinating Agents, Part 33: Regioselective Chlorodifluoromethylations in the 1-Position of 1,2-Unsaturated Monosaccharide Derivatives

Novel Approach to Isoindolo[2,1-a]quinolines: Synthesis of 1- and 3-Halo-Substituted 11-Oxo-5,6,6a,11-tetrahydroisoindolo[2,1-a]quinoline-10-carboxylic Acids

One-Pot Synthesis of 6′-Amino-Substituted Spirooxazines

A Convenient Two-Step Synthesis of Amino Acid Derived Chiral 3-Substituted [1,4]Benzodiazepin-2-ones

The Diels-Alder Approach towards Cannabinoids

Rhodium-Catalyzed Synthesis of Terminal Alkenes

Synthesis of Biaryls